• Title/Summary/Keyword: Grain shape

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Controllable Growth of Single Layer MoS2 and Resistance Switching Effect in Polymer/MoS2 Structure

  • Park, Sung Jae;Chu, Dongil;Kim, Eun Kyu
    • Applied Science and Convergence Technology
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    • v.26 no.5
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    • pp.129-132
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    • 2017
  • We report a chemical vapor deposition approach and optimized growth condition to the synthesis of single layer molybdenum disulfide ($MoS_2$). Obtaining large grain size with continuous $MoS_2$ atomically thin films is highly responsible to the growth distance between molybdenum trioxide source and receiving silicon substrate. Experimental results indicate that triangular shape $MoS_2$ grain size could be enlarged up to > 80um with the precisely controlled the source-to-substrate distance under 7.5 mm. Furthermore, we demonstrate fabrication of a memory device by employing poly(methyl methacrylate) (PMMA) as insulating layer. The fabricated devices have a PMMA-$MoS_2$/metal configuration and exhibit a bistable resistance switching behavior with high/low-current ratio around $10^3$.

A Study of Forging Equipment for One Body Crankshaft of Medium Sized Marine Engine (선박 중형엔진용 일체형 Crankshaft 단조장치에 관한 연구)

  • 박승희;윤성만;신상엽;박래원;박종국;이응기;김대두
    • Transactions of Materials Processing
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    • v.8 no.3
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    • pp.237-244
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    • 1999
  • The purpose of this research is for the development of a new type forging equipment. H.C.G.(Hyundai Continuous Grain-Flow), by using two virtual build-up tools, rigid viscoplastic FEM and downsized plasticine experiment. This forging method consists of only vertical pressuree. Therefore, high quality crankshafts can be forged with this method as it can maintain a continuous grain flow. The factors considered in the development of equipment are die geometry for flawless deformed shape, die reaction forces, stress/strain distributions and continuous material flow. We carried out several numerical simulations and downsized plasticine experiments for the proper design of the forging equipment. The validity of those simulation results is confirmed by checking with the actual test results. Based on these simulation results, the proper design of the H.C.G. forging equipment is enabled.

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SERKOWSKI'S EMPIRICAL RELATION FOR INTERSTELLAR LINEAR POLARIZATION VIEWED FROM DAVIS-GREENSTEIN ALIGNMENT MECHANISM

  • Hong, Seung-Soo;Lee, Hyung-Mok
    • Journal of The Korean Astronomical Society
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    • v.11 no.1
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    • pp.31-36
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    • 1978
  • Although Serkowski used a single value K=1.15 in representing all the observed interstellar linear polarization curves by his empirical relation $p({\lambda})/P_{max}$=exp (-K $1n^2({\lambda}_{max}/{\lambda})$), where $p_{max}$ is the maximum polarization at wavelength ${\lambda}_{max}$, we have noticed a meaningful variation in K from observations of 72 stars. By comparing K's with $P_{max}/E_{B-V}\;and\;with\;{\lambda}_{max}$, we have examined how the shape of the polarization curve is related with the degree of grain alignment on one hand, and with grain sizes on the other. We have shown that correlations between K, $P_{max}/E_{B-V}\;and\;with\;{\lambda}_{max}$, are consistent with the idea of Davis-Greenstein mechanism for grain alignment.

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Toughening of $Al_2$O$_3$/LaAl$_{11}$O$_{18}$ Composites (Al$_2$O$_3$/LaAl$_{11}$O$_{18}$ 복합재료의 인성증진)

  • 장병국;우상국
    • Journal of the Korean Ceramic Society
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    • v.35 no.12
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    • pp.1266-1273
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    • 1998
  • Al2O3/(5~20vol%)LaAl11O18 composites in which the second phase was dispersed with a elongated grain shape were fabricated using Al2O3 and La2O3 composition by hot-pressing. In order investigate the in-fluence of LaAl11O18 on the toughening of LaAl11O18 on the toughening of Al2O3 matrix composites AE(acoustic emission) analysis was con-ducted together with an evaluation of fracture toughness using of SEPB technique. The degree of AE events occurred in composites were more than those in monolithic alumina. The occurrences of AE event increased with increasing the amount of LaAl11O18 phase in the Al2O3/LaAl11O18 composite is two times higher compared to monolithic alu-mina. The main toughening mechanism was attributed to the bridging of LaAl11O18 grains at tip of pro-pagating crack.

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The electrochromic properties of nickel oxide films (니켈산화물 박막의 전기적착색특성)

  • 이길동
    • Journal of the Korean Vacuum Society
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    • v.8 no.2
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    • pp.127-135
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    • 1999
  • Nickel oxide films were prepard by using the electron beam evaporation technique. Coloring and bleaching experiments for cyclic durability were repeated in KOH electrolyte by cyclic voltammetry. Visible spectrophtometry was used to assess the stability of the transmittance in the degraded films. X-ray photoelectron spectroscopy results showed that the grain surface are oxygen-rich compared to the grain interiors in a NiO film. Open circuit memory of colored films is about 400hours in lN KOH. The rate of self discharge was evaluated by measuring the transmittance at 550nm of a fully oxidized NiO film. The rate of self discharge was increased polynomially with time and the film is nearly bleached after about 400hours. It was also found that the degraded film by repeated cycles in the KOH solution changed the grain shape of film surface The film prepared under a vacuum pressure of $3\times10^{-4}$ mbar was found to be rather stable when subjected to the repeated coloring and bleaching cycles in KOH electrolyte. Band theory applied to explain the electrochromic mechanism was discussed.

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Dependence of Microstructure of Sintered $Y_3$Fe$_5$O$_{12}$ in Addition of CuO (CuO 첨가에 따른 $Y_3$Fe$_5$O$_{12}$ 소결체의 미세구조 변화)

  • 이재동;김광석;김성재;김태옥
    • Journal of the Korean Ceramic Society
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    • v.35 no.10
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    • pp.1014-1019
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    • 1998
  • As results of the study on the sinterbility of YIG at the low temperature using CuO as additive CuO com-pound which contain {{{{ { {Fe }_{2 }O }_{3 } }} was shown liquid in sintering process. YIG crystal dissolved into CuO compound liquid phase and then Y element which is considered no solubility in solid CuO compound moved to the grain during cooling. The abnormal grain growth up to 150${\mu}{\textrm}{m}$ at CuO 8.6mole% was shown due to shape accomdation reaction and local liquid distribution. The apparent density of YIG shows minimum at CuO 8.6 mole% due to abnormal grain growth and the saturation magnetization decrease dramatically at 32.5mole% due to orthoferrite formation.

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Study the effects of grain shape on the erosive burning (그레인 형상에 따른 침식연소 효과 연구)

  • Cho, Min-Gyung;Kim, Jin-Yong;Kwon, Tae-Hoon
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2011.04a
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    • pp.232-235
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    • 2011
  • A typical unsteady internal ballistic analysis model was developed to take account the erosive burning of a solid rocket motor. The variance of local velocity and pressure along grain surface were analyzed by using the continuity and momentum equation. The coefficients of erosive burning were drew from comparing experiment data with analysis. It was investigated that the grain shapes of propellant affect the erosive burning.

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Varietal Variations in Absolute Density of Rice Grain and Its Relations with Other Grain Characters (미립 절대밀도의 품종간 변이 및 몇가지 미립형질과의 관계)

  • Hee Jong, Koh;Mun Hue, Heu;Cheng Mo, Jiang
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.37 no.3
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    • pp.244-249
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    • 1992
  • To investigate the varietal variations in absolute density of milled rice grain and its relations with other grain characters, the 235 rice varieties which consist of 30 Tongil type rices, 72 Japonica rices and 133 Indica rices were tested on grain size, volume, hardness, chalkiness and 1000 grains weight of brown rice, ADV, amylose content, starch composition on SEM and absolute density of milled rice grain using completely ripened grains. Average absolute density of milled rice grain was 1.496g / cm$^3$ in Tongil type rices, 1.506g / em in Japonica rices, and 1.500g / cm$^3$ in Indica rices. It was correlated positively with days to heading and grain hardness, and negatively with chalkiness, volume, grain weight and grain length of brown rice. Regression analysis indicated that grain volume and weight were the major characters affecting the density. However, since the absolute density of milled rice grain did not show great varietal variations it might not seem important as one of the characters contributing to the grain yield, while it could be a factor affecting the grain quality because there were definite varietal differences even though small. The microscopic feature of starch composition on SEM revealed differences between clear and chalky parts of the grain in shape and compactness of starch composition but did not discriminate between high and low-density grains.

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Resistance to Airflow of Grain as Affected by Grain Moisture Content (곡물(穀物)의 함수율(含水率) 변화(變化)에 따른 송풍저항(送風抵抗)에 관(關)한 연구(硏究))

  • Kim, M.S.;Kim, S.R.
    • Journal of Biosystems Engineering
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    • v.11 no.2
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    • pp.55-65
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    • 1986
  • The resistance to the passage of airflow through various agricultural products is an important consideration in the design of an aeration or drying system. The amount of resistance to airflow varied widely from one kind of grain to another, and depended upon airflow rate, surface texture and shape of the particles, the size and configuration of voids, and foreign and fine material in the grain bed. The airflow rate was the major factor considered on this kind of study in the early stages. But these days, the studies on the resistance to airflow of grain affected by grain moisture content and foreign and fine material have been widely carried out. However the foreign an fine material in the grain bed could not be a major factor on the study in Korea because there were only a few grain process procedure after harvesting it. The objectives of this study were to investigate the effect of moisture content and airflow rate on airflow resistance to grain, and to develop a model to predict the static pressure drop across the grain bed as a function of moisture content and airflow rate. The rough rice varieties, Akibare, Milyang 15 (Japonica types), Samkwang, Backyang (Indica types)and covered barley variety, Olbori, which were harvested in 1985 were used in the experiment after cleaning them. Resistances to airflow of grain were investigated at four levels of moisture content (13-25%, wb.) for ten different airflow rates($0.01-0.15m^3/sm^2$). The results of this study are summarized as follows; 1. Theaverage bulk densities were $585.3kg/m^3$ for rough rice and $691.6kg/m^3$ for barley at the loose fill, and were $648.8kg/m^3$ for rough rice and $758.2kg/m^3$ for barley at the packed fill. The pressure drops at the packed fill beds were approximately 1.4 to 1.8 times higher than those at the loose fill beds. 2. The pressure drops across grain beds deceased with the increase of moisture content and increased with airflow rate. The decreasing rates of pressure drop across grain beds according to the moisture contents at the lower airflow rates were higher than those at the higher airflow rates, and the increasing rates of pressure drop according to the airflow rates at the lower moisture contents were higher those at higher moisture contents. 3. The pressure drop across barley bed were much higher than rough rice beds and the pressure drops across Japonica type rough rice beds were a little higher than Indica type. 4. The mathematical models to predict the pressure drop across grain beds as a function of moisture content and airflow rate were developed from these experiments.

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Transient Liquid Phase Bonding of Directionally Solidified Ni Base Superalloy, GTD-111(II) -Microstructural Change of Base Metal during Bonding Process - (일방향응고 Ni기초내열합금 GTD-111의 천이액상확산접합(II) -접합공정에서 모재조직의 변화-)

  • 강정윤;황형철;김인배;김대업;우인수
    • Journal of Welding and Joining
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    • v.21 no.2
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    • pp.89-96
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    • 2003
  • The change of microstructures in the base metal during transient liquid phase bonding process of directionally Ni base superalloy, GTD-111 was investigated. Bonds were fabricated using a series of holding times(0-7.2ks) at three different temperatures(1403, 1418 and 1453K) under a vacuum of 13.3mPa. In raw material, ${\gamma}$- ${\gamma}$' eutectic phases, platelet η phases, MC carbide and PFZ were seen in interdendritic regions or near grain boundary and size of primary ${\gamma}$' precipitates near interdendritic regions were bigger than core region. The primary ${\gamma}$' precipitates in dendrite core were dissolved early in bonding process, but ${\gamma}$' precipitates near interdendritic regions were dissolved partially and shape changed. The dissolution rate increased with increasing temperature. Phases in interdendritic regions or near pain boundary continually changed with time at the bonding temperature. In the bonding temperature of 1403K, eutectic phases had not significantly changed, but η phases had transformed from platelet shape to needle morphology and PFZ region had widened with time. The interdendritic region and near pain boundary were liquated partially at 1423k and fully at 1453k by reaction of η phases and PFZ. In the bonding temperature of 1453K, interdendritic region and near pain boundary were liquated and then new phases which mixed with η phases, PFZ and MC carbide crystallized during cooling. Crystallized η phases transformed from rod shape to platelet shape with increasing holding time.