• Korean Journal of Materials Research
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• v.29 no.1
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• pp.30-36
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• 2019

We evaluate the properties of friction welded STK400 steel tube in terms of the relationship between microstructures and mechanical properties. Friction welding is conducted at a rotation speed of 1,600 rpm and upset time of 3-7 sec for different thicknesses of STK 400 tubes. To analyse the grain boundary characteristic distributions(GBCDs) in the welded zone, electron backscattering diffraction(EBSD) method is introduced. The results show that a decrease in welding time (3 sec.) creates a notable increase grain refinement so that the average grain size decreases from $15.1{\mu}m$ in the base material to $4.5{\mu}m$ in the welded zone. These refined grains achieve significantly enhanced microhardness and a slightly higher yield and higher tensile strengths than those of the base material. In particular, all the tensile tested specimens experience a fracture aspect at the base material zone but not at the welded zone, which means a soundly welded state for all conditions.

• Korean Journal of Materials Research
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• v.12 no.6
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• pp.436-441
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• 2002

Effect of Sn addition on the stress corrosion cracking(SCC) resistance of the Al-Cu-Mn cast alley was investigated by C-ring teat and electrical conductivity measurement, The electrical conductivity and SCC resistance increased by Sn addition. The alley containing 0,10%Sn showed maximum electrical conductivity and the best SCC resistance. At the same composition, the electrical conductivity and SCC resistance increased from peak aged condition to ever aged condition. The PFZ and coarse precipitates along the grain boundary were observed from TEM micrographs. The fracture mode of the alloy was confirmed as intergranular type and showed brittle fracture surface. The SCC mechanism of the alloy was concluded as the anodic dissolution model, The maximum hardness was increased from 130Hv in the Sn-free alloy to 156Hv in the 0.10%Sn added alloy.

• Korean Journal of Materials Research
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• v.11 no.4
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• pp.266-271
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• 2001

Effect of Cd addition on the stress corrosion cracking(SCC) resistance of Al-Cu-Mn cast alloy was investigated by C-ring test and electrical conductivity measurement. With increasing Cd contents, the electrical conductivity and the SCC resistance were increased. The PFZ and coarse precipitates along the grain boundary were observed from TEM micrographs. The fracture made of the alloys was confirmed as intergranular type and showed brittle fracture surface. As a result, it was concluded that the SCC mechanism of these alloys is the anodic dissolution model. The maximum hardness was increased from 127Hv in the Cd-free alloy to 138∼145Hv in the Cd addition alloys.

• Journal of the Korean Society of Safety
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• v.12 no.2
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• pp.45-56
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• 1997

Fracture behavior of ex-serviced 1Cr-0.5Mo steel was measured at room($24^{\circ}C$) and elevated($538^{\circ}C$) temperature and compared with that measured with virgin 1Cr-0.5Mo steel. Compact C(T) specimens were machined from the base and welded test materials. In case of the C(T) specimens of the weld, fatigue precrack was introduced along the fusion line so that following crack growth should occurs along the region of heat affected zone. It was observed that the J-R curve of the serviced material was significantly lower than that of the virgin material at room temperature. Brittle fracture was observed in the serviced material. On the other hand, at elevated temperature no noticeable difference was found between the J-R curves of the virgin and the serviced material. The measured J-R curves were also compared with those of the 1.25Cr-0.5Mo steel obtained from the other literatures. Optical microscopy and SEM examination of the serviced material reveal the carbide in/along the grain boundary which shows material degradation due to long-term usage. An example of application of the measured J-R curves is shown.

• Korean Journal of Metals and Materials
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• v.48 no.7
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• pp.683-689
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• 2010

In this study, FeAl based intermetallic matrix composites reinforced with in-situ synthesized TiC particles were fabricated by an in-situ liquid mixing process. The microstructures, mechanical properties and fracture behaviors of the in-situ liquid mixing processed composite were investigated and compared with the vacuum suction casting processed composite. The results showed that the in-situ formed TiC particles exhibited fine and uniform dispersion in the liquid mixing processed composite, while significant grain boundary clustering and coarsening of TiC particles were obtained by the vacuum suction process. It was also shown in both types of composites that the hardness and bending strength were increased with the increase of the TiC volume fractions. Through the study of fractography in the bending test, it was considered that the TiC particles prohibited brittle intergranular fracture of FeAl intermetallic matrix by crack deflections. Because of the uniformly distributed fine TiC particles, the bending strength of the liquid mixing processed composite was superior to that of the casting processed composite.

• Journal of the Korean Society for Heat Treatment
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• v.5 no.1
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• pp.41-49
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• 1992

The effects of alloying elements on the superplastic properties of Al-Li based alloys had been investigated. The intermediate thermo-mechanical treated (ITMT) Al-2.0wt%Li, Al-2.0wt%Li-1.0wt%Mg, Al-2.0wt%Li-0.12wt%Zr and Al-2.0wt%Li-1.2wt%Cu-1.0wt%Mg-0.12wt%Zr alloys were tested in tension at various temperature (400, 450, 500 and $550^{\circ}C$) and strain rate($6.7{\times}10^{-3}$, $1.0{\times}10^{-2}$, $1.6{\times}10^{-2}$ and $5.0{\times}10^{-2}/sec$). The results were as follows : The superplasticity in binary, ternary and pentanary alloys appeared at 500 to $550^{\circ}C$, and good strain rate for superplasticity. $1.6{\times}10^{-2}/sec{\sim}1.0{\times}10^{-2}/sec$ for a binary alloy and $1.0{\times}10^{-2}/sec{\sim}6.7{\times}10^{-3}/sec$ for ternary and pentanary alloys. A Zr-added ternary alloy had best value of elongation (730%) in four alloys at $550^{\circ}C$ of tension temperature and $1.0{\times}10^{-2}/sec$ of strain rate. The strain rate was greatly dependent on tension temperature and true strain rate was more than 1.0 at all test temperature and strain rate. In binary and Mg-added teranry alloys. the necks were slightly formed and their fracture surface had lips shape, but Zr-added ternary and pentanary alloy fractured along the grain boundary without necking. Their dislocations moved to grain boundary during superplasticity deformation and arranged perpendicular to grain boundary. Super plastic deformation was made by grain boundary slip of dislocation slip creep and model of core and mantle.

• Journal of Powder Materials
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• v.5 no.1
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• pp.42-49
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• 1998

A study on the improvement of the impact energy in 93W heavy alloy with a Ni/Fe ratio of 9/1 has been carried out as a function of heat treatment temperature. The obtained results were compared to that of the traditional alloy system in which the Ni/Fe ratio is 7/3 or 8/2. With increasing heat treatment temperature from 1150 to 125$0^{\circ}C$, the impact energy of the alloy with the Ni/Fe ratio of 9/1 is remarkably increased from 42 to 72 J, which is higher than that of traditional alloy, up to 118$0^{\circ}C$ and then saturated. Fracture mode was also changed from brittle W/W boundary failure to W cleavage. The temperature showing the dramatic shrinkage by dilatometric anaysis of the heavy alloy with Ni/Fe ratio of 9/1 was found to be 1483 $^{\circ}C$, which is higher than that (146$0^{\circ}C$) of the heavy alloy with Ni/Fe ratio of 7/3. Auger Electron Spectroscopy showed that the segregation of impurities, such as S, P, and C in W/W grain boundary was considerably decreased with increasing heat treatment temperature from 1150 to l18$0^{\circ}C$. From the above results, it was found that the impurity segregation in W/W grain boundary played an important role on the decrease of impact properties, and the heat treatment temperature should be appropriately chosen, as considering the Ni/Fe ratio of the alloy, in order to get good impact properties.

• Transactions of the Korean Society of Mechanical Engineers
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• v.9 no.1
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• pp.40-46
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• 1985

Some problems such as toughness decrement and stess relief cracking (SRC), many occur when post weld heat treatment (PWHT) is applied to remove residual stress adn hydrogen. In this paper PWHT was carried out under the stress of 0, 98, 196 and 294 MPa (0, 10, 20 and 30kgf/mm$^{2}$ each) to simulate residual stress in HAZ of Cr-Mo steel. The effect of applied stress during PWHT on fracture toughness was evaluated by COD fracture toughness test, micro-hardnes test and observation of SEM. The experimental results are as follows; (1) Fracture toughness of weld HAZ was improved by PWHT, but it decreased as heat treated under the stress. (2)Hardness ratio under the stress of 294MPa (30kg/mm$^{2}$) was lower and fracture toughness was decreased than that of the no stress. (3) Applied stress in weld HAZ during PWHT assisted precipitation of over saturated alloying elements in the structure, so fracture surface at the stress of 294MPa (30kg/mm$_{2}$) appeared the grain boundary failure possibly one of the reasons for PWHT embrittlenment.

• Advances in nano research
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• v.13 no.4
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• pp.407-416
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• 2022

In this study, the gravitating mechanical stir casting method was used to fabricating the Nb₂O₅/AZ31 magnesium matrix nanocomposites. Niobium pentoxide (Nb₂O₅) used as reinforcement with two different weight percentages (3 wt % and 6 wt %). The influence of Nb₂O₅ on microstructure and mechanical properties has been investigated. The microstructure analysis showed that the composites are mainly composed of the primary α-magnesium phase and phase β-Mg₁₇Al₁₂ secondary phase. The secondary phase was dispersed evenly along the grain boundary of the Mg phase. The Nb₂O₅/AZ31 nanocomposites revealed that the grain size and its lamellar shape (β-Mg₁₇Al₁₂) were gradually refined. Different strengthening mechanisms were assessed in terms of their contributions. Results showed that composite material properties of hardness, yield strength, and fracture study were directly related to Nb₂O₅ as a reinforcement. The maximum values of the mechanical properties were achieved with the addition of 3 wt% Nb₂O₅ on the AZ31 alloy.

• Proceedings of the KWS Conference
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• 1997.05a
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• pp.65-68
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• 1997

Fracture behavior of ex-serviced 1Cr-0.5Mo steel was measured at room(24$^{\circ}C$) and elevated(538$^{\circ}C$) temperature and compared with that measured with virgin 1Cr-0.5Mo steel. Compact C(T) specimens were machined from the base and welded test materials. In case of the C(T) specimens of the weld, fatigue precrack was introduced along the fusion line so that a crack growth should occur along the region of heat affected zone. It was observed that the J-R curve of the serviced material was significantly lower than that of the virgin material at room temperature. Brittle fracture was observed in the serviced material. On the other hand at elevated temperature no noticeable difference was found between the J-R curves of the virgin and the serviced material. The measured J-R curves were also compared with those of the 1.25Cr-0.5Mo steel from other literatures. Optical microscopy and SEM examination of the serviced material reveal the carbide in/along the grain boundary which shows material degradation due to long-term usage.