• Title/Summary/Keyword: Grain Size

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Effect of Ti and C Contents on Prior Austenite Grain Size in Ti Added Steels (Ti 첨가강의 Ti와 C 함량에 따른 초기 오스테나이트 입도 변화)

  • Kim, Woo-Jin;Kang, Nam-Hyun;Kim, Sung-Ju;Do, Hyung-Hyup;Nam, Dae-Geun;Cho, Kyung-Mox
    • Korean Journal of Materials Research
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    • v.21 no.4
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    • pp.187-191
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    • 2011
  • Prior austenite grain size plays an important role in the production of high strength hot-rolled steel. This study investigated the effect of Ti and C contents on the precipitates and prior austenite grain size. Steel with no Ti solutes had prior austenite grain size of about 620 ${\mu}m$. The addition of Ti ~ 0.03 wt.% and 0.11 wt.% reduced the prior austenite grain size to 180 ${\mu}m$ and 120 ${\mu}m$, respectively. The amount of Ti required to significantly decrease the prior austenite grain size was in the range of 0.03 wt.%. However, the amount of carbon required to significantly decrease the prior austenite grain size was not present from 0.04 wt.% to 0.12 wt.%. Oxides of Ti ($Ti_2O_3$) were observed as the Ti content increased to 0.03 wt.%. The specimen containing 0.11 wt.% of Ti exhibited the complex carbides of (Ti, Nb) C. The formation of Ti precipitates was critical to reduce the prior austenite grain size. Furthermore, the consistency of prior austenite grain size increased as the carbon and Ti contents increased. During the reheating process of hot-rolled steel, the most critical factor for controlling the prior austenite grain size seems to be the presence of Ti precipitates.

Prediction for the Dynamically Recrystallized Grain Size of AISI 304 (AISI 304 스테인리스강의 동적 재결정립 예측)

  • Kim S. I.;Yoo Y. C.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2001.05a
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    • pp.143-146
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    • 2001
  • The evolution of dynamic recrystallization (DRX) was studied with torsion test for AISI 304 stainless steel in the temperature range of $900-1000^{\circ}C$ and strain rate range of 0.05-5/sec. The evolution of DRX was investigated with microstructural analysis and change of flow stress curve slope. The investigation of serrated grain boundaries using electron back scattered diffraction (EBSD) analysis indicated that the nucleated new DRX grain size was similar to the size of bulging part. Before the steady state, the dynamically recrystallizing grains do not remain a constant size and gradually grow to the size of fully DRX grain at steady state. The calculation of grain size was based on $X_{DRX}$ and the assumption, which the nucleated DRX grains are growing to the steady state, continuously. It was found that the calculated results agreed with the microstructure of the alloy.

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Grain Size Refinement in CuAlNi Shape Memory Alloy using Melt-spun Ribbon (급냉응고된 Ribbon을 이용한 CuAINi 형상기억합금의 결정미세화)

  • Choe, Yeong-Taek
    • 연구논문집
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    • s.22
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    • pp.127-139
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    • 1992
  • The mechnial properties such as fracture strength, ductility and fatigue strength of Cu shape memory alloy are lower than those of Ti-Ni SMA, because of their high elastic anisotropy and large grain size. And in order to improve the mechanical property of Cu SMA, some techniques such as casting method by addition of refining element, powder metallurgy and rapid solidification process have been studied on the refinement of the grain size of Cu SMA. This study was carried out to refine the grain size of CuAlNi SMA by applying the melt spinning method. According to this study, the conclusions are as follows; - grain size of the melt-spun ribbon was about $1\mum$ - there was not change in grain size, although increasing of hot pressing temperature -grain size of the hot-extruded specimen was about $30-40\mum$, it is more refiner than that of castings

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Abnormal Grain Growth Behaviors of $BaTiO_3$ Ceramics with Controlling of Particle Size Distributjion of Calcined Powder (하소분체의 입도조절에 따른 $BaTiO_3$ 요업체의 비정상 입성장거동)

  • 이태헌;김정주;김남경;조상희
    • Journal of the Korean Ceramic Society
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    • v.32 no.2
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    • pp.147-154
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    • 1995
  • Abnormal grain growth behavior of BaTiO3 ceramics with controlling of particle size distribution of calcined powder was investigated. The particle size distribution was controlled by changing the calcining temperature or by using of classification and regrinding process. With broadening of the normallized size distribution in calcined powder, it showeda normal grain growth behavior in sintered body due to an increase of volume fraction of seed grain in the calcined powder. It was supposed that the seed grains could easily contact each other for the rapid grain growth during sintering process and resulted in fast switching-over from abnormal to normal grain growth stage.

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Analysis of the effect on the whisker growth as grain size of plating and base metal (Plating 및 Base metal의 Grain size에 따른 Whisker 성장 영향 분석)

  • Kim, Su-Jin;Chang, Mi-Soon;Kwack, Kae-Dal
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.1337-1342
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    • 2008
  • The whisker grows at the plating of a lead frame so that it causes the serious problem like the short. To prove this case, many people have studied the cause and influence of the tin whisker growth. This study explains the grain size affects the growth of the whisker in the lead frame. By these studies about the whisker, the whisker growth is discovered by stresses generated by the intermetallic compound and CTE mismatch in both plating and base metal. The stresses or lattice defect generated in the plating process changes grain structure of plating. Consequently, these various stresses are stabilized by forming unspecified whiskers through lots of grain boundaries. Because the grain boundary is the path of the whisker growth, the smaller grain size exists, the more whiskers grow.

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A Study on the Grain Size Dependence of Hardness in Nanocrystalline Metals (나노결정금속의 경도의 결정립도의존성에 관한 연구)

  • 김형섭;조성식;원창환
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1997.03a
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    • pp.73-76
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    • 1997
  • Nanocrystalline materials have been modeled as a mixture of the crystallite and the grain boundary phases. The mechanical property has been calculated using the rule of mixtures based on the volume fractions. The critical grain size concept suggested by Nieh and Wadsworth and porous material model suggested by Lee and Kim were applied to the calculation. The theoretical results fit very well with the experimental values

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Relation of Grain Size with Magnetic Domain Wall for Tertiary Recrystallized 3% Si-Fe Strip (3차 재결정에 의한 극박 방향성 규소강판의 결정립 크기와 자벽수와의 관계)

  • ;K. I. Arai
    • Journal of the Korean Magnetics Society
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    • v.6 no.3
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    • pp.165-169
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    • 1996
  • The relationship between grain size and number of magnetic domain walls for tertiary recrystallized ultra thin 3 % Si-Fe strips was investigated. It was found that the strips with different grain size can be produced by controlling the inserting speed of sample in annealing furnace. Though grain size of the stirip became smaller than 1mm, $B_{8}$ of high value above 1.95T was obtained. But $H_{c}$ increased with decaying the grain size. The magnetic domains and losses of the ultra thin grain oriented silicon steel with smaller grian size were observed. The eddy current losses of the strips were decreased with decreasing the grain size in high frequency range because strips with smaller grain have narrower magnetic domain wall spacings. But Hysteresis losses of the strips with smaller grain have high value in low frequency range. Therefore the iron loss of ultra thin grain oriented silicon steel could be controlled by the grain size. It was clarified that the minumum tatal loses depended on the exciting frequency and grain size.

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Development of the breeding materials with diverse grain size and shape in japonica rice

  • Park, Hyun-Su;Shin, Woon-Chul;Baek, Man-Kee;Nam, Jeong-Kwon;Jeong, Jong-Min;Park, Seul-Gi;Kim, Choon-Song;Cho, Young-Chan;Kim, Bo-Kyeong
    • Proceedings of the Korean Society of Crop Science Conference
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    • 2017.06a
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    • pp.67-67
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    • 2017
  • We developed the breeding materials with diverse grain size and shape in japonica rice. Grain size and shape are important factors affecting consumer preference and choice. However, most of Korean japonica rice cultivars have small, short, and round grain. To diversify the grain size and shape of japonica rice, we conducted the breeding program using donor parents, Jizi1560 and Jizi1581. Jizi1560 and Jizi1581 are japonica germplasm with extremely large grain. Four crosses between the each donor parents and high yielding japonica rice cultivars, Deuraechan and Boramchan, were constructed and then anther culture method was applied. We obtained 290 doubled-haploid (DH) lines with appropriated morphological traits and selected 91 DH lines with diverse grain size and shape. The grain related-traits of the selected DH lines showed a higher diversity when compared with 319 cultivars developed by NICS (264 japonica, 13 black, and 32 Tongil type cultivars). We designated the selected DH lines, four parents, and Daeripbyeo 1, large grain japonica cultivar, as the breeding materials for further analysis. The breeding materials were classified into five groups, A to E, based on the grain-related traits. Group A (including Jizi1581) and Group B (including Daeripbyeo 1) showed similar grain width, whereas Group A exhibited longer grain length and heavier grain weight. Group C (including Deuraechan and Boramchan) showed shorter and rounder grain shape and smaller grain size than any other groups. Group D including solely Jizi1560 had extremely large grain, such as the longest grain length, width, and thickness and heaviest grain weight. Group E including only two DH lines had long and slender grain shape, so that showed the highest ratio of length to width. The grain size and shape of the breeding materials exhibited beyond the characteristics of previously developed Korean japonica cultivars. The breeding materials will be applied in the breeding programs to diversify the grain size and shape of japonica rice.

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Grain size effects on the dielectric phase transition in PZT ceramics (PZT 요업체에서 입자 크기가 상전이에 미치는 영향)

  • 정훈택;김호기
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1989.06a
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    • pp.107-109
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    • 1989
  • Based on the ferroelectric microstructural residual stress model, the relation between grain size and residual elastic energy was proposed. It was found that the residual elastic energy increased with decreasing grain size by modeling and DSC results. This residual elastic energy change with grain size which induce the phase transituion mode change was the cause of a diffuse phase transition in small grain size.

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A Study on the Room Temperature Properties of Molding Sand with different Sand Grain Size (규사(硅砂)의 입도(粒度)에 따른 주물사(鑄物砂)의 상온성질(常溫性質)에 관(關)한 연구(硏究))

  • Choi, Dong-Soo;Lee, Kye-Won
    • Journal of Korea Foundry Society
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    • v.3 no.3
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    • pp.167-173
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    • 1983
  • The effect of sand grain size on the various properties of mold is not only basic but important interest which we have to deal with.And the relation among the various properties of mold (strength, permeability, flowability, compactability, hardness, deformation, toughness etc.) is very complicated and inaccurate, so we can delineate the behavior of mixture (sand+water+bentonite) with experience only. Within recent years a so-called rigid-water theory has been accepted as a means of advancing logical explanations for the research aimed at delineating sand-clay-water relationships. By changing grain size or mesh no. of grain, specimens have been subjected to green compressive strength, permeability, deformation, flowability, compactablity, toughness at room temperature. Under constant mulling energy and ratio of water/bentonite, the results obtained were as follows: 1. With decreasing grain size green compressive strength of the specimen increased. 2. With decreasing grain size permeability decreased. 3. With decreasing grain size flowability and bulk density decreased but compactability increased. 4. With decreasing grain size deformation decreased but toughness increased. 5. At 60 mesh no., the properties of specimen are conspicuously changed. The reason is that the total surface area of sand grain which affects the type of bonding between sand grains is more changed at 60 mesh number.

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