• Title/Summary/Keyword: Gas-Phase

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고농도 Out Gas 정량 분석법 개발

  • Kim, Min-Ju;Kim, Jong-Yun;Jeong, Gi-Ho;Park, Chang-Sik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.11a
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    • pp.13-13
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    • 2009
  • 본 연구는 MLCC 구성성분의 증발/비등에 의한 저분자물질의 제거가 bar 수축에 미치는 영향도를 평가하기 위해, 압착 bar에서 발생하는 고농도의 out gas를 정량하기 위한 최적 system을 구축하고자 하였다. gas 포집에 범용적으로 사용하는 Purge & Trap sampler 대신 Heating block를 사용하여 gas를 발생시키고 동시에 solvent에 용해시킴으로써 고농도의 시료가 희석될 수 있는 전처리 장치를 디자인하였다. 그 결과 고농도 gas 주입에 의한 장비오염과 peak saturation 문제가 해결되었고, gas phase의 시료를 liquid phase로 상전이 시켜 autosampler를 이용한 정확한 량의 시료 주입이 가능하였다. System의 Gage Linearity와 Bias는 각각 1.7%와 1.3%로 개선이 필요없는 수준의 정확도를 가졌다.

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Gas 자동제어시스템을 이용하여 다양한 gas 조성이 Aloe Saponaria 세포배양계에 미치는 영향 연구

  • Park, Tae-Yeong;Heo, Won;Kim, Dong-Il;Jo, Gyu-Heon
    • 한국생물공학회:학술대회논문집
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    • 2000.11a
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    • pp.398-401
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    • 2000
  • The effect of volatile components on cell growth and polysaccharide production in suspension cultures of Aloe saponaria was investigated using an intelligent on-line gas control system which enabled to control the concentrations of oxygen, carbon dioxide and ethylene simultaneously. Aloe production was enhanced in the presence of exogenous ethylene in the concentration range of 5ppm and 15ppm. Maintaining high tension of carbon dioxide (5% v/v) was found to enhance polysaccharide production significantly.

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The Effects of Oral Activity With Sensory Integration Intervention on Eating of a Child With Oral Defensiveness: A Single-Subject Research Design (구강 활동을 병행한 감각통합중재가 구강 방어 아동의 먹기에 미치는 효과: 단일 실험 설계 연구)

  • Kim, Yoon-Sung;Son, Cho-Rok;Kim, Kyeong-Mi
    • The Journal of Korean Academy of Sensory Integration
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    • v.16 no.1
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    • pp.1-13
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    • 2018
  • Objective : The purpose of this study was to investigate the effects of sensory integration intervention combined with oral activity on eating of child with sensitive oral senses. Methods : The study subject was 6 years old boy and diagnosed with developmental disorder. The experiment period was 15 sessions from April 21, 2017 to June 2, 2017. Experimental design used AB design in single-subject design, baseline (A) phase (sensory integration therapy) was 5 sessions and intervention phase (B) (sensory integration therapy combined oral activity) was 10 sessions. During the experiment, the child used the Goal Attainment Scale (GAS) to measure behavioral changes in eating. Results : The GAS score of voluntary eating of favorite foods was 0 on the baseline phase and increased to 1.9 on the intervention phase. The GAS score of voluntary eating of disliking foods was 0 on average during the baseline phase and increased to 1.7 on average during the intervention phase. Conclusion : This study suggests that sensory integration intervention combined with oral activity program may have a positive effect on eating of children with sensitive oral senses and limited food intake.

Zero-Offset VSP Data Processing for Gas Hydrate-Bearing Sediments in East Sea (동해 가스하이드레이트 부존지역 제로오프셋 VSP 탐사 자료의 자료처리)

  • Kim, Myung-Sun;Byun, Joong-Moo;Yoo, Dong-Geun
    • Geophysics and Geophysical Exploration
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    • v.12 no.3
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    • pp.255-262
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    • 2009
  • Conventionally, vertical-seismic-profiling (VSP) survey that provides high-resolution information has mainly performed to obtain the exact depth of the gas hydrate-bearing sediment, which is one of the key factors in the development of the gas hydrate. In this study, we extracted interval velocities and created corridor stacks from the first domestic zero-offset VSP data, which were acquired with three component receivers at UBGH09 borehole in Ulleung Basin where gas hydrate exists. Then we compared the corridor stacks with a CMP stacked section from surface seismic data. First of all, we converted the signals recorded with three component receivers to true vertical and horizontal components by phase rotation, and divided the data into direct waves and reflected waves by wavefield separation processing. The trend of the interval velocity extracted from the zero-offset VSP was similar to that of the sonic log obtained at the same borehole. Because the interval velocity of the gas hydrate-bearing sediment above the BSR was high, and it decreased suddenly through the BSR, we could infer that free gas is accumulated below the BSR. The results of comparing the corridor stacks to the CMP stacked section of the surface seismic data showed that most reflection events agreed well with those in the surface CMP stacked section and that the phase-rotated VSP data corresponded better with the surface seismic data than the VSP data without phase rotation. In addition, by comparing a corridor stack produced from the transverse component with the CMP stacked section of the surface seismic data, we could identify PS mode-converted reflections in the CMP stacked section.

Complex Analyses for Gas Hydrate Seismic Reflection Data (가스하이드레이트 탄성파 자료의 복소분석)

  • Hien, D.H.;Jang, Seong-Hyung;Kim, Young-Wan;Suh, Sang-Yong
    • 한국신재생에너지학회:학술대회논문집
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    • 2008.10a
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    • pp.208-212
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    • 2008
  • Gas hydrate has been paid attention to study for because: 1) it can be considered as a new energy resources; 2) one of reasons causing the instability of sea floor slope and 3) a factor to the climate change. Bottom simulating reflector (BSR) defined as seismic boundary between the gas hydrate and free gas zone has been considered as the most common evidence in the seismic reflection data for the gas hydrate exploration. BSR has several characteristics such as parallel to the sea bottom, high amplitude, reducing interval velocity between above and below BSR and reversing phase to the sea bottom. Moreover, instantaneous attribute properties such as amplitude envelop, instantaneous frequency, phase and first derivative of amplitude of seismic data from the complex analysis could be used to analyze properties of BSR those would be added to the certain properties of BSR in order to effectively find out the existence of BSR of the gas hydrate stability zone. The output of conventional seismic data processing for gas hydrate data set in Ulleung basin in the East sea of Korea will be used for complex analyses to indicate better BSR in the seismic reflection data. This result of this analysis implies that the BSR of the analyzed seismic profile is clearly located at the two ways time (TWT) of around 3.1 seconds.

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Synthesis of Nano-sized Tungsten Carbide Powders by Vapor Phase Reaction of Tungsten Ethoxide (텅스텐 에톡사이드의 기상 반응을 이용한 초미립 WC 분말의 합성)

  • 가미다;하국현;김병기
    • Journal of Powder Materials
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    • v.10 no.1
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    • pp.1-5
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    • 2003
  • Nano-sized WC powders were synthesized by vapor phase reaction using the precusor of tungsten ethoxide under helium and hydrogen atmosphere. The phases of the powder were varied with reaction Bone and gas flow rate. The powder size was about 30nm in diameter, and the tungsten carbide powder was coated by carbon layer. The synthesis of nano-sized WC powders was promoted as the hydrogen gas flow rate became higher. Inversely, tungsten oxide was formed by increasing the flow rate of helium gas. The synthesized powders were analyzed by XRD, FE-SEM, carbon analyzer etc.

Visualization of Gas/liquid Ejector Flow and Void Fraction Measurement using Fiber Optic Probe (기체-액체 이젝터 유동의 가시화와 광섬유 탐침에 의한 기포분율 측정)

  • Choi, Sung Hwan;Ji, Ho Seong;Kim, Kyung Chun
    • Journal of the Korean Society of Visualization
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    • v.11 no.1
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    • pp.34-40
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    • 2013
  • Gas/liquid two-phase ejector is a device without moving parts, in which liquid is used to drive gas of a low-pressure source. In this paper, the hydrodynamic characteristics of a vertical down type two-phase ejector were studied using an air-water loop system. Entrained air flow rates were measured with inlet and outlet pressures of the ejector with varying water flow rate. Homogeneous bubbly flows in the discharge pipe were confirmed by the high speed flow visualization method. Quantitative measurements of void fraction were made using a newly developed fiber optic probe system.

Surface Micromachining of TEOS Sacrificial Layers by HF Gas Phase Etching (HF 기상식각에 의한 TEOS 희생층의 표면 미세가공)

  • 장원익;이창승;이종현;유형준
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1996.11a
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    • pp.725-730
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    • 1996
  • The key process in silicon surface micromachining is the selective etching of a sacrificial layer to release the silicon microstructure. The newly developed anhydrous HF/$CH_3$OH gas phase etching of TEOS (teraethylorthosilicate) sacrificial layers onto the polysilicon and the nitride substrates was employed to release the polysilicon microstructures. A residual product after TEOS etching onto the nitride substrate was observed on the surface, since a SiOxNy layer is formed on the TEOS/nitride interface. The polysilicon microstructures are stuck to the underlying substrate because SiOxNy layer does not vaporize. We found that the only sacrificial etching without any residual product and stiction is TEOS etching onto the polysilicon substrate.

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Simplifying Analysis of Nitric Oxide in Gas Phase Cigarette Smoke (담배연기중 일산화질소의 신속분석)

  • Rhee, Mun-Su;Jang, Gi-Cheol;Ji, Sang-Un
    • Journal of the Korean Society of Tobacco Science
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    • v.15 no.1
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    • pp.49-56
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    • 1993
  • Nitric oxide of gas phase in cigarette smoke was conveniently determined by Chemiluminescence NO analyzer with 20 ports rotary type smoking machine Data are presented to support this observation. On the basis of this method the amount of NO in the smoke from nonblended and commercial cigarettes were estimated. Gas phase NO concentration in main stream smoke was correlated well with the nitrate levels in tobacco leaves, but there was no correlation with the tar yields. In consequence, it would be considered that the methodology in this study provided simple and rapid quantification for NO in cigarette smoke.

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Analysis of Residual Furan in Human Blood Using Solid Phase Microextraction-Gas Chromatography/Mass Spectrometry (SPME-GC/MS)

  • Lee, Yun-Kyung;Jung, Seung-Won;Lee, Sung-Joon;Lee, Kwang-Geun
    • Food Science and Biotechnology
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    • v.18 no.2
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    • pp.379-383
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    • 2009
  • For an accurate risk assessment of furan, a potential human carcinogen, levels must be determined in human blood plasma using a simple and robust assay. In this study, solid phase microextraction-gas chromatography/mass spectrometry (SPME-GC/MS) was used to analyze blood plasma levels of furan in 100 healthy individuals who consumed a normal diet. The subjects were 30 to 70 years of age and 51% were women. Ultimately, an analytical method was established for analyzing furan in human blood. The limit of quantification (LOQ) and furan recovery rate in blood were 1.0 ppb and 104%, respectively. Finally, furan was detected in 21 individuals (13 males, 8 females) with levels ranging up to 17.86 ppb (ng furan/g food).