• 제목/요약/키워드: GLC

검색결과 449건 처리시간 0.026초

왕둥굴레의 생약학적연구(生藥學的硏究) (Pharmacognostical Studies on the Rhizome of Polygonum robustum Nakai)

  • 김정규;이용주
    • 생약학회지
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    • 제11권2호
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    • pp.69-74
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    • 1980
  • The rhizome of Polygonatum robustum Nakai (Liliaceae) has been used as a crude drug for the purpose of tonic and thirst cure in Korea. The dried rhizomes were extracted with hot ether, then the residue was extracted with hot alcohol. 1) The three kinds of chemical constituents, substance, I, II and III were isolated by silicagel column chromatography from ether and alcohol extracts of the rhizomes. Substance I was confirmed as ${\beta}-sitosterol$, $C_{29}H_{50}O$ by mass and IR spectroscopy. Substance II was identified as stigmasterol by GLC. 2) Substance III was obtained by crystallization from the column chromatography of alcohol fraction. It was suggested as diosgenin based on chemical and spectral discussions. 3) The concentration of blood sugar was significantly decreased in the group administered the ether extract with 20% dextrose and adrenaline in comparison to that of 20% dextrose and adrenaline along.

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인삼의 Sterol 성분에 관한 연구(I) -중성지질 분획의 Sterol함량 조사- (Studies on the Sterols of Korean Ginseng(I) -On the Contents of Sterols in Neutral Lipid Fraction-)

  • 김만욱;노길봉;위재준
    • Journal of Ginseng Research
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    • 제9권1호
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    • pp.64-71
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    • 1985
  • Free and esterified sterols in neutral lipid fractionated from the free lipid of Korean white ginseng (Panax ginseng C.A. Meyer) were analyzed by TLC and GLC to investigate the contents and composition ratios. Content of each sterol was as follows: ${\beta}$-sitosterol was about 51.60 mg%, stigmasterol, 8.93mg% and campesterol, 2.17mg%. Fine root tended to have slightly higher contents of sterols than main root. Linoleic and palmitic acid as the major fatty acids in esterified sterols occupied 70% of the total composition.

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추출시간에 따른 돼지 족의 지방산과 칼슘, 마그테슘 함량 변화에 관한연구 (Studies on the Content of fatty Acid Calcium and Magnesium of Pig s Shank According to Extraction Time by Water)

  • 이미경;노기환
    • 한국식품영양과학회지
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    • 제19권1호
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    • pp.61-64
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    • 1990
  • The influence of extraction time on the fatty acid profile and the contents of calcium and magnesium in pig's shank were examined. The 9 kinds of fatty acid were identified in water extracts from pig's shank by GLC. The profiles of fatty acids from different extraction were similer to each other,. The content of linolenic acid was increased after two-hours extraction however the amounts of MUFA, PUFA and p/s ratio were decreased by the longer extraction time. The amount of calcium was 124.7mg% in raw materials but water extracts and bone powder samples showed higher values. in case of magnesium it was 138.4mg% in raw materials, but the extracts showed lower amount and bone powder exhibited higher values.

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한국산(韓國産) 고등(高等) 균류(菌類)의 성분(成分) 연구(硏究)(XXI) - 긴말징버섯의 스테롤 성분(成分) - (Studies on the Constituents of Higher Fungi of Korea(XXI) - A Sterol from Calvatia saccatum (Vahl.) Fr. -)

  • 권태준;이정옥;강창율;김병각;박동우
    • 한국균학회지
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    • 제8권1호
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    • pp.25-28
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    • 1980
  • Attempts were made to investigate sterol components of Calvatia saccatum (Vahl.) Fr. which grows wildly in Korea. Its carpophores were collected in Gyeong Gi Province and extracted with chloroform and methanol. Two compounds were isolated from the extract and one of these compounds was identified as ergosterol by TLC, GLC and chemical tests.

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밀감 쥬스 향기(香氣) 성분(成分)의 정량(定量) (Quantitative Determination of Flavor Constituents of Korean Milgam (Citrus unshiu) Juice)

  • 김호;조도현;박연희;이춘영;이양희
    • Applied Biological Chemistry
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    • 제23권2호
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    • pp.106-114
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    • 1980
  • 제주산 밀감 juice의 향기성분을 질소 gas로 추출하여 gas liquid chromatography로 동정하였고 각 성분의 extraction coefficient를 사용하여 함량을 구하였다. 50여개의 peak중 26성분을 동정하였다. 향기성분중 ethanol이 140ppm이며 limonene이 120ppm으로 이 두 성분이 가장 중요한 성분으로 밝혀졌다.

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포도주 효모에 의한 중간크기의 지방산 생성 (Formation of Medium Chain Fatty Acid by Wine Yeasts)

  • 이수오
    • 한국식품과학회지
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    • 제21권6호
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    • pp.832-837
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    • 1989
  • 포도주 발효에 사용되는 호모균주 12종을 Murphy배지에 배양하여 중간크기의 지방산(MCFA)의 생성을 분석하였고 발효조건에 따라 그 생성량을 관찰하였다. 특히 발효력이 강한 Saccharomyces cerevisiae에 속하는 균주들은 발효초기에 decanoic acid를 약 21-26mg/1 생성하였고 발효 후기에는 약 5-10mg/1로 감소하였다. 발효조건에서 볼 때 MCFA의 생성은 온도가 높을수록 감소하였고 당함량이 클수록 증가하였으며 또한 탄산가스의 존재 하에서도 증가하였다.

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한국산(韓國産) 고등(高等) 균류(菌類)의 성분(成分) 연구(硏究)(XII) - 치마버섯의 스테롤 성분 - (Studies on the Constituents of Higher Fungi of Korea(XII) - A Sterol from Schizophyllum commune Fr. -)

  • 이송애;정경수;김병각;민홍기
    • 한국균학회지
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    • 제7권2호
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    • pp.87-90
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    • 1979
  • Attempts were made to investigate sterol components of Schizophyllum commune Fr. which is one of medicinal fungi and grows wildly in Korea. Its carpophores were collected in Mountain Gwanak and extracted with chloroform and methanol. A sterol was isolated and identified as ergosterol by TLC, GLC and chemical tests.

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한국산(韓國産) 고등(高等) 균류(菌類)의 성분(成分) 연구(硏究)(XV) - 병둥이 산그물버섯의 스테롤 성분(成分) - (Studies on the Constituents of the Higher Fungi of Korea(XV) - Sterols of Xerocomus badius (Fr.) Kuhner ex Gilbert -)

  • 김병각;이정옥;한성순;이동규
    • 한국균학회지
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    • 제7권2호
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    • pp.83-85
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    • 1979
  • Attempts were made to investigate the sterol components of Xerocomus badius Fr. Kuhner ex Gilbert which grows wildly in Korea. Its carpophores were collected in Gyeong-Gi Province and extracted with chloroform and methanol. Two compounds were isolated from the extract and one of these compounds was identified as ergosterol by TLC, GLC and chemical tests.

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