• 제목/요약/키워드: Free standing

검색결과 252건 처리시간 0.022초

Fabrication and Characterization of Free-Standing DBR Porous Silicon Film

  • Um, Sungyong;Sohn, Honglae
    • 통합자연과학논문집
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    • 제7권1호
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    • pp.1-4
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    • 2014
  • Distributed Bragg reflector porous silicon of different characteristics were formed to determine their optical constants in the visible wavelength range using a periodic square wave current between low and high current densities. The surface and cross-sectional SEM images of distributed Bragg reflector porous silicon were obtained using a cold field emission scanning electron microscope. The surface image of distributed Bragg reflector porous silicon indicates that the distributions of pores are even. The cross-sectional image illustrates that the multilayer of distributed Bragg reflector porous silicon exhibits a depth of few microns and applying of square current density during the etching process results two distinct refractive indices in the contrast. Distributed Bragg reflector porous silicon exhibited a porosity depth profile that related directly to the current-time profile used in etch. Its free-standing film was obtained by applying an electro-polishing current.

열화학기상증착법을 이용한 프리스탠딩 ZnO/Zn 코어셀 마이크로 다면체 구조물의 합성 (Synthesis of free-standing ZnO/Zn core-shell micro-polyhedrons using thermal chemical vapor deposition)

  • 최민열;박현규;정순욱;김상우
    • 한국결정성장학회지
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    • 제18권4호
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    • pp.155-159
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    • 2008
  • 본 연구에서는 금속 Zn 팰렛을 원료 물질로 이용하여 열화학기상증착법으로 마이크로 크기의 프리스탠딩 ZnO/Zn 코어셀 다면체 구조물을 합성하였다. 마이크로 크기로 성장된 ZnO/Zn 코어셀 다면체의 형태와 구조적인 특성을 분석하기 위해서 주사전자현미경과 투과전자현미경을 이용하였다. 성장된 마이크로 크기의 다면체는 단결정 ZnO 나노막대 배열에 의해 둘러싸인 단결정 금속 Zn로 구성되어 있음을 확인할 수 있었다. 마이크로 크기의 단결정 Zn는 육방정 결정구조로 이루어져 있으며, 표면을 구성하고 있는 c-축 배향된 ZnO 나노막대가 10 nm와 100 nm 이하의 직경과 높이를 각각 가지며 육방정 결정구조의 단결정임을 확인하였다.

수소 플라즈마 에칭과 탄소 확산법에 의한 다이아몬드막 표면의 평탄화 (Planarization of the Diamond Film Surface by Using the Hydrogen Plasma Etching with Carbon Diffusion Process)

  • 김성훈
    • 대한화학회지
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    • 제45권4호
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    • pp.351-356
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    • 2001
  • 철, 코발트, 니켈 합금을 이용한 탄소확산-수소플라즈마 에칭법으로 다이아몬드 자체막의 표면을 매우 평탄하게 할 수 있었다. 이 방법에서의 다이아몬드 자체막을 합금과 몰리브데늄 기판 사이에 위치시켜 금속-다이아몬드-몰리브데늄(MDM) 샌드위치 형태의 샘플 세 트를 이루게 하였다. 이 샘플세트를 마이크로 웨이브 플라즈마 장치에 장착하여 수소 플라즈마를 발생시켜서 기판온도가 섭씨 1,000 이상이 되도록 하였다. 이와 같은 과정들은 탄소확산-수소플라즈마 방법이라고 하였다. 다이아몬드 자체막 표면을 에칭한 후 표면 거칠기, 표면형상, 에칭한 다이아몬드 표면속의 불순물의 침투를 조사하였다. 결론적으로, 탄소 확산-수소 플라즈마 에칭법은 전자 디바이스에 응용할 수 있는 매우 평탄한 다이아몬드 표면을 형성시키는 방법임을 알 수 있다.

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Charge Neutral Quasi-Free-Standing Graphene on 6H-SiC(0001) Surface by Pd Silicidation and Intercalation

  • 송인경;신하철;박종윤;안종렬
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2012년도 제42회 동계 정기 학술대회 초록집
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    • pp.128-128
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    • 2012
  • We investigated the atomic and electronic properties of graphene grown by Pd silicidation and intercalation using LEED, STM, and ARPES. Pd was deposited on the 6H-SiC(0001) surface at RT. The formation of Pd silicide gives rise to breaking of Si-C bonds of the SiC crystal, which enables to release C atoms at low temperature. The C atoms are transformed into graphene from $860^{\circ}C$ according to the LEED patterns as a function of annealing temperature. Even though the graphene spots were observed in the LEED pattern and the Fourier transformed STM images after annealing at $870^{\circ}C$, the topography images showed various superstructures so that graphene is covered with Pd silicide residue. After annealing at $950^{\circ}C$, monolayer graphene was revealed at the surface. The growth of graphene is not limited by surface obstacles such as steps and defects. In addition, we observed that six protrusions consisting of the honeycomb network of graphene has same intensity meaning non-broken AB-symmetry of graphene. The ARPES results in the vicinity of K point showed the non-doped linear ${\pi}$ band structure indicating monolayer graphene decoupled from the SiC substrate electronically. Note that the charge neutrality of graphene grown by Pd silicidation and intercalation was sustained regardless of annealing temperature in contrast with quasi-free- standing graphene induced by H and Au intercalation. Further annealing above $1,000^{\circ}C$ accelerates sublimation of the Pd silicide layer underneath graphene. This results in appearance of the $(6r3x6r3)R30^{\circ}$ structure and dissolution of the ${\pi}$ bands for quasi-free-standing graphene.

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Freestanding GaN 기판의 Ga-polar 면에 기계적 연마 방법을 적용한 Bow 제어 및 그 특성 연구 (Effect of the Control of Bowing in Free-standing GaN by Mechanical Polishing)

  • 김진원;손호기;임태영;이미재;김진호;전대우;황종희;정정영;오해곤;김진훈;최영준;이혜용;윤대호
    • 한국전기전자재료학회논문지
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    • 제28권12호
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    • pp.776-780
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    • 2015
  • In this paper, we have studied the effect of mechanical polishing to Ga-polar face for reducing the wafer bowing and strain in free-standing GaN. After the mechanical polishing to Ga-polar face, the bowing of the free-standing GaN substrate significantly decreased with increasing the size of diamond slurry, and eventually changed the bowing direction from concave to convex. Furthermore, the full width at half maximum (FWHM) of high-resolution X-ray diffraction (HR-XRD) were decreased, especially the FWHM of (1 0 2) reflection for $1.0{\mu}m$ size of diamond slurry was significantly decreased from 630 to 203 arcsec. In the case, we confirmed that the compressive strain in Ga-polar face was fully released by Raman measurement.

Effect of pile group geometry on bearing capacity of piled raft foundations

  • Fattah, Mohammed Y.;Yousif, Mustafa A.;Al-Tameemi, Sarmad M.K.
    • Structural Engineering and Mechanics
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    • 제54권5호
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    • pp.829-853
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    • 2015
  • This is an experimental study to investigate the behaviour of piled raft system in different types of sandy soil. A small scale "prototype" model was tested in a sand box with load applied to the foundation through a compression jack and measured by means of load cell. The settlement was measured at the raft by means of dial gauges, three strain gauges were attached on piles to measure the strains and calculate the load carried by each pile in the group. Nine configurations of group ($1{\times}2$, $1{\times}3$, $1{\times}4$, $2{\times}2$, $2{\times}3$, $2{\times}4$, $3{\times}3$, $3{\times}4$ and $4{\times}4$) were tested in the laboratory as a free standing pile group (the raft not in contact with the soil) and as a piled raft (the raft in contact with the soil), in addition to tests for raft (unpiled) with different sizes. It is found that when the number of piles within the group is small (less than 4), there is no evident contribution of the raft to the load carrying capacity. The failure load for a piled raft consisting of 9 piles is approximately 100% greater than free standing pile group containing the same number of piles. This difference increases to about 4 times for 16 pile group. The piles work as settlement reducers effectively when the number of piles is greater than 6 than when the number of piles is less than 6. The settlement can be increased by about 8 times in ($1{\times}2$) free standing pile group compared to the piled raft of the same size. The effect of piled raft in reducing the settlement vanishes when the number of piles exceeds 6.

Seismic responses of a free-standing two-story steel moment frame equipped with a cast iron-mortar sliding base

  • Chung, Yu-Lin;Kuo, Kuan-Ting;Nagae, Takuya;Kajiwara, Koichi
    • Earthquakes and Structures
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    • 제17권3호
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    • pp.245-256
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    • 2019
  • An experimental study was conducted to evaluate the dynamic behavior of a free-standing frame equipped with a movable base system using cast iron and mortar as the bearing materials. The preliminary friction test indicated that a graphite layer developed on the interface and exhibited stable friction behavior. The friction coefficient ranged from 0.33 to 0.36 when the applied normal compression stress ranged from 2.6 to 5.2 MPa. The effect of the variation of normal compression stress would be small. Shaking table tests on the free-standing frame showed that rock, slide, and rock-slide responses occurred. The cumulative slide distance reached 381 mm under JMA Kobe wave excitation; however, only a few cyclic slides occurred at the same locations along the moving track. Most surfaces sustained single slides. Similar results can be observed in other shaking conditions. The insufficient cyclic sliding and significant rocking resulted in a few graphite layers on the mortar surfaces. Friction coefficients were generally similar to those obtained in the preliminary friction tests; however, the values fluctuated when the rocking became significant. The collisions due to rocking caused strong horizontal acceleration responses and resulted in high friction coefficient. In addition, the strong horizontal acceleration responses caused by the collisions made the freestanding specimen unable to reduce the input horizontal acceleration notably, even when slippage occurred. Compared with the counterpart fixed-base specimen, the specimen equipped with the iron-mortar base could reduce the horizontal acceleration amplification response and the structural deformation, whereas the vertical acceleration response was doubled due to collisions from rocking.

Binder-free and Full Electrical-Addressing Free-standing Nanosheets with Carbon Nanotube Fabrics for Electrochemical Applications

  • 이태일;제갈종필;최지혁;최원진;이민정;오진영;김광범;백홍구;;명재민
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2011년도 춘계학술발표대회
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    • pp.40.2-40.2
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    • 2011
  • As the old saying 'nothing is complete unless you put it in final shape', although nanosheets (NSs) are a promising functional building block for various electrochemical applications, their true value cannot be realized until they are well woven into electrical conducting materials. As an effort to determine their ideal shape, in this study, a unique manufacturing route to build a layer-by-layer (LBL) structure of two-dimensionally ordered, free-standing ${\beta}$-nickel hydroxide nanosheets (${\beta}$-NHNSs) that are fully electrically addressed with single-wall carbon nanotube fabrics was demonstrated, and its capabilities were verified through a comparative study on the differences between a simple bulky and LBL-structured electrochemical cathode, representing two extreme cases. The LBL-structured cathode showed a discharging current peak that was 25 times larger than the bulky structured one measured in cyclic voltammetry, which implies that the LBL structure is near an ideal electrode configuration for NS-based electrochemical applications.

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