• 제목/요약/키워드: Free Si

검색결과 892건 처리시간 0.031초

한의학과 문학의 교섭 양상 연구 -약명시(藥名詩)를 중심으로- (A Study on Reciprocal Relationship between TKM and Literature : Centering on Medicinal Name Verses(YakMyeongSi))

  • 이정현
    • 한국한의학연구원논문집
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    • 제16권3호
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    • pp.77-84
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    • 2010
  • In this study, YakMyeongSi were considered to define relations of Tradional Korean Medicine(TKM) and literature. In the introduction, present related studies were searched to clarify YakMyeongSi are completely different from medical property songs(YakSeongGa). Related data about YakMyeongSi and YakSeongGa were extracted for the initial findings. In chapter 2, medical name verse was defined as 'a type of free verses with one or more medical names in each verse to be interpreted ordinarily' based on records and examples of YakMyeongSi. In China, it originated from "Book of Odes" and "Songs of Chu", and it was most popular in the Song-China. Medical names actually referred to medical names in the early forms of the Warring States Period, but the complete form of YakMyeongSi started to appear in the Tang-China. In chapter 3, 34 YakMyeongSi and 5 related data were suggested in tables as the present conditions of Korean YakMyeongSi. With actual examples, better comprehension of YakMyeongSi were intended. Also, the fact that Korean YakMyeongSi were completed in forms at the end of Goryeo and beginning of Joseon dynasty. The motivations of writing YakMyeongSi were also studied. Medical names were put into verses because they well expressed landscapes and emotions. Propagation of medical knowledge was the basis of YakMyeongSi. There are limits in defining the relations of TKM and literature with some YakMyeongSi. More studies must be carried out on YakMyeongSi in various records with details and interests. Also, study to define general relations of TKM and literature must be carried out together by examining TKM in literary forms such as medical introductions or medical property songs and literature pieces that expressed principles and materials of TKM.

보강재에 도금된 Cu층이 Al/SiC복합재료의 젖음성에 미치는 영향 (Wetting improvement of SiC/Al Metal Matrix Composite by Cu Surface Treatment)

  • 이경구;조규종;이도재
    • 한국재료학회지
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    • 제11권5호
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    • pp.398-404
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    • 2001
  • SiC 보강재 표면에 도금된 Cu금속층이 Al/SiC복합재료의 젖음성에 미치는 영향을 검토하였다. 보강재에 대한 금속층의 도금은 무전해도금법을 이용하였으며, Al/SiC 복합재료의 제조는 텅스텐 발열체 진공로의$ 670^{\circ}C$~$900^{\circ}C$에서 제조하여 보강재와 기지간의 접촉부위를 촬영하여 젖음성을 측정하였다 젖음성 측정 결과 보강재에 도금된 Cu층은 젖음성을 향상시켰고, 젖음성의 개선은 보강재에 도금된 금속층과 기지간의 반응에 의해 계면에너지를 변화시킴으로서 나타난 결과이며. 반응을 통한 산화피막의 배제도 영향을 미친 것으로 판단된다

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솔-젤법에 의한 $SiO_2-ZrO_2$계 무반사 박막의 제조 (Fabrication of Sol-Gel derived Antireflective Thin Films of $SiO_2-ZrO_2$ System)

  • 김병호;홍권;남궁장
    • 한국세라믹학회지
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    • 제32권5호
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    • pp.617-625
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    • 1995
  • In order to reduce reflectance of soda-lime glass having average reflectance of 7.35% and refractive index of 1.53, single (SiO2), double (SiO2/20SiO2-80ZrO2), and triple (SiO2/ZrO2/75SiO2-25ZrO2) layers were designed and fabricated on the glass substrate by Sol-Gel method. Stble sols of SiO2-ZrO2 binary system for antireflective (AR) coatings were synthesized with tetraethyl orthosilicate (TEOS) and zirconium n-butoxide as precursors and ethylacetoacetate (EAcAc) as a chelating agent in an atmosphere environment. Films were deposited on soda-lime glass at the withdrawal rates of 3~11 cm/min using the prepared polymeric sols by dip-coating and they were heat-treated at 45$0^{\circ}C$ for 10 min to obtain homogeneous, amorphous and crack-free films. In case of SiO2-ZrO2 binary system, refractive index of film increased with an increase of ZrO2 mol%. Designed optical constant of films could be obtained through varying the withdrawal rate. In the visible region (380~780nm), reflectance was measured with UV/VIS/NIR Spectrophotometer. Average reflectances of the prepared single-layer [SiO2 (n=1.46, t=103nm)], double-layer [SiO2 (n=1.46, t=1-4nm)/20SiO2-80ZrO2 (n=1.81, t=82nm)], and triple-layer [SiO2 (n=1.46, t=104nm)/ZrO2 (n=1.90, t=80nm)/75SiO2-25ZrO2 (n=1.61, t=94 nm)] were 4.74%, 0.75% and 0.38%, respectively.

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폴리카보네이트 특성 향상을 위한 Al-Si-N 박막의 제작 및 크랙 방지

  • 송인설;안세훈;이근혁;장성우;김동환;한승희
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2015년도 제49회 하계 정기학술대회 초록집
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    • pp.168.1-168.1
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    • 2015
  • 자동차 산업분야에서 차량 경량화의 한 수단으로, 자동차용 유리를 무게가 가볍고 고강도 투명 고분자 소재인 폴리카보네이트로 대체하고자 하는 연구가 이루어지고 있다. 하지만, 폴리카보네이트의 낮은 내 마모 특성과 자외선에 의한 열화 및 변색 현상은 해결해야 할 문제점으로 지적되고 있다. 본 연구에서는, 폴리카보네이트의 내마모 특성을 향상시키기 위해 HIPIMS+ (High Power Impulse Magnetron Sputtering+) 방법을 이용하여 투과율이 확보되고, 고경도 특성을 갖는 Al-Si-N 박막을 증착하였다. 고속증착을 하기 위해 Target에 인가되는 Power를 올리게 되었는데, 열팽창 계수가 큰 고분자 물질인 폴리카보네이트 시료의 온도가 상승하여 증착된 박막과의 열팽창 계수 차이에 의해 박막에 Crack이 형성되는 문제가 발생하였다. 증착되는 Al-Si-N 박막의 공정 압력에 따른 Stress 제어 방법 및 폴리카보네이트 시료의 온도 상승을 막기 위한 알루미늄 구조체를 이용함으로써 박막의 Crack 형성을 억제하고자 하였다. 박막의 Stress를 확인하기 위하여 AFM (Atomic Force Microscope)과 OM (Optical Microscope)을 이용하여 분석하였고, 박막의 경도는 Knoop ${\mu}$-hardness tester를 사용하여 측정하였다. Al-Si-N 박막 경도는 Si at.%/(Al at.% + Si at.%) 비율이 16%에서 33 GPa의 경도를 갖는 것을 확인하였다. UV-Vis Spectrometer를 이용하여 투과율을 측정한 결과, 400-700 nm 파장의 가시광 영역 평균 투과율은 80%로 측정되었다.

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ANTICORROSION PROPERTIES OF SIOC COATED SUS-316

  • 김수룡;권우택;김정주;김종일;김영희;김정일;우창현
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2009년도 추계학술발표대회
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    • pp.34.2-34.2
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    • 2009
  • The ceramic coatings on metallic materials have attracted by many researchers due to the chemical inertness of ceramic materials. In such aspect, SiOC is a promising material tobe used as protective coating layer on metallic materials due to its outstanding thermal stability and chemical inertness. In this research, SiOC coating was carried out onto SuS-316 substrate using Cl free preceramic polymers such aspolyphenylcarbosilane. 20% of polymethylphenylsilane in cyclohexane solution was coated onto metal surface by dip coating method. Thermal oxidation was carried out at $200^{\circ}C$ for crosslink of the preceramic polymer and the sample was pyrolysized at $800^{\circ}C$ under argon to convert the preceramic polymer to amorphous SiOCx state. The microstructure of the SiOCx film after pyrolysis was investigated using FE-SEM. Corrosion resistance of SiOC coated SuS-316 substrate has been investigated using 5% HCl solution at 25, 40, 60 and $80^{\circ}C$ for 7days. The data revealed that the corrosion resistance increased with SiOC coating on SuS-316 substrate.

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Method and mechanism of dispersing agent free dispersion of short carbon fibers in silicon carbide powder

  • Raunija, Thakur Sudesh Kumar;Mathew, Mariamma;Sharma, Sharad Chandra
    • Carbon letters
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    • 제15권3호
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    • pp.180-186
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    • 2014
  • This study highlights a novel method and mechanism for the rapid and effective milling of carbon fibers (CFs) in silicon carbide (SiC) powder, and also the dispersion of CFs in SiC powder. The composite powders were prepared by chopping and exfoliation of CFs, and ball milling of CFs and SiC powder in isopropyl alcohol. A wide range of CFs loading, from 10 to 50 vol%, was studied. The milling of CFs and SiC powder was checked by measuring the average particle size of the composite powders. The dispersivity of CFs in SiC powder was checked through scanning electron microscope. The results show that the usage of exfoliated CF tows resulted in a rapid and effective milling of CFs and SiC powder. The results further show an excellent dispersion of CFs in SiC powder for all CFs loading without any dispersing agent.

Accurate electronic structures for Ce doped SiAlON using a semilocal exchange-correlation potential

  • 유동수;정용재
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2011년도 제40회 동계학술대회 초록집
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    • pp.438-438
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    • 2011
  • White light-emitting diodes (LEDs), the so-called next-generation solid-state lighting, offer benefits in terms of reliability, energy-saving, maintenance, safety, lead-free, and eco-friendly. Recently, rare-earth-doped oxynitride or nitride compounds have attracted a great deal of interest as a photoluminescent material because of their unique luminescent property, especially for white LEDs applications. Ce doped ${\beta}$-SiAlON has been studied as a wavelength conversion phosphor in white LEDs thanks to its high absorption rates, high quantum efficiency, and excellent thermal stability. Previously researches were not enough to understand the detail mechanism and characteristics of ${\beta}$-SiALON. The bandgap structures and electronic structures were not exact due to limitation of calculation methods. In this study, to elucidate the Ce doping effect on the SiAlON system, accurate band structures and electronic structure of the Ce doped ${\beta}$-SiAlON was intensively investigated using density functional theory calculations. In order to get a better description of the band gaps, MBJLDA method were used. We have found a single Ce atom site in ${\beta}$-SiAlON super cell. Furthermore, the density of state, band structure and lattice constant were intensively investigated.

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Reproductive fecundity of Iraqi Awassi ewes immunized against synthetic inhibin-α subunit or steroid-free bovine follicular fluid

  • Al-Sa'aidi, Jabbar Abbas Ahmed;Khudair, Khalisa Khadim;Khafaji, Sura Safi
    • Asian-Australasian Journal of Animal Sciences
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    • 제31권8호
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    • pp.1169-1175
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    • 2018
  • Objective: The present study was conducted to investigate the impacts of active and passive immunization against synthetic inhibin and steroid-free bovine follicular fluid, respectively, on reproductive fecundity out of breeding season in Iraqi Awassi ewes. Methods: Follicular fluid was aspired from mature bovine follicles, treated with activated charcoal, and used for immunization of male rabbits for obtaining steroid free bovine follicular fluid (SFBFF) antiserum. Forty non-pregnant Awassi ewes were allocated into 4 groups (n = 10 each). At day 38 of experiment, ewes were treated with intra-vaginal MPA sponge (60 mg for 12 days). At days 0, 28, and 50, ewes were treated with 4, 2, and 2 mL of normal saline (control; C-ve), 400, 200, and $200{\mu}g$ of ovalbumin (C+ve), 400, 200 and $200{\mu}g$ of inhibin (SI group), respectively, and 4 mL of normal saline at day 0, and 4 and 2 mL of SFBFF antiserum at days 28 and 50, respectively, (AI group). After mating with Awassi rams, pregnancy and embryo number were diagnosed, at day 38 of pregnancy, using ultrasonography. Blood samples were collected at days 30, 60, 90, and 120 of pregnancy, for assessment of estradiol-$17{\beta}$ (E2) and progesterone (P4) levels. After parturition, numbers of delivered lambs were recorded. Results: The results revealed significant increase of P4 and significant decrease of E2 levels in SI and AI pregnant ewes than controls at days 30, 60, 90, and 120. Newborn number increased significantly in SI and AI treated than control ewes. Conclusion: Active or passive immunization against endogenous inhibin could augment reproductive fecundity out of breeding season in Iraqi Awassi ewes.

수렴성빔 전자회절법을 이용한 $SiO_2/Si$ 계면 부위의 격자 변형량 측정 (Measurements of Lattice Strain in $SiO_2/Si$ Interface Using Convergent Beam Electron Diffraction)

  • 김긍호;우현정;최두진
    • Applied Microscopy
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    • 제25권2호
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    • pp.73-79
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    • 1995
  • The oxidation of silicon wafers is an essential step in the fabrication of semiconductor devices. It is known to induce degradation of electrical properties and lattice strain of Si substrate from thermal oxidation process due to charged interface and thermal expansion mismatch from thermally grown SiO, film. In this study, convergent beam electron diffraction technique is employed to directly measure the lattice strains in Si(100) and $4^{\circ}$ - off Si(100) substrates with thermally grown oxide layer at $1200^{\circ}C$ for three hours. The ratios of {773}-{973}/{773}-{953} Higher Order Laue Zone lines were used at [012] zone axis orientation. Lattice parameters of the Si substrate as a function of distance from the interface were determined from the computer simulation of diffraction patterns. Correction value for the accelerating voltage was 0.2kV for the kinematic simulation of the [012]. HOLZ patterns. The change in the lattice strain profile before and after removal of oxide films revealed the magnitudes of intrinsic strain and thermal strain components. It was shown that $4^{\circ}$ -off Si(100) had much lower intrinsic strain as surface steps provide effective sinks for the free Si atoms produced during thermal oxidation. Thermal strain in the Si substrate was in compression very close to the interface and high concentration of Si interstitials appeared to modify the thermal expansion coefficient of Si.

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High-Temperature Fracture Strength of a CVD-SiC Coating Layer for TRISO Nuclear Fuel Particles by a Micro-Tensile Test

  • Lee, Hyun Min;Park, Kwi-Il;Park, Ji-Yeon;Kim, Weon-Ju;Kim, Do Kyung
    • 한국세라믹학회지
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    • 제52권6호
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    • pp.441-448
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    • 2015
  • Silicon carbide (SiC) coatings for tri-isotropic (TRISO) nuclear fuel particles were fabricated using a chemical vapor deposition (CVD) process onto graphite. A micro-tensile-testing system was developed for the mechanical characterization of SiC coatings at high temperatures. The fracture strength of the SiC coatings was characterized by the developed micro-tensile test in the range of $25^{\circ}C$ to $1000^{\circ}C$. Two types of CVD-SiC films were prepared for the micro-tensile test. SiC-A exhibited a large grain size (0.4 ~ 0.6 m) and the [111] preferred orientation, while SiC-B had a small grain size (0.2 ~ 0.3 mm) and the [220] preferred orientation. Free silicon (Si) was co-deposited onto SiC-B, and stacking faults also existed in the SiC-B structure. The fracture strengths of the CVD-SiC coatings, as measured by the high-temperature micro-tensile test, decreased with the testing temperature. The high-temperature fracture strengths of CVD-SiC coatings were related to the microstructure and defects of the CVD-SiC coatings.