• Title/Summary/Keyword: Fracture Analysis

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Preparation of PMN-PT-BT/Ag Composite and its Mechanical and Dielectric Properties (PMN-PT-BT/Ag 복합체 제조 및 기계적, 유전적 특성)

  • Lim, Kyoung-Ran;Jeong, Soon-Yong;Kim, Chang-Sam;Nahm, Sahn
    • Journal of the Korean Ceramic Society
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    • v.39 no.9
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    • pp.846-850
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    • 2002
  • A PMN-PT-BT/Ag composite was prepared by surface modification with MgO sol with hoping to suppress silver's migration during sintering. The mixture of PbO, $N_2O_5,\;TiO_2\;with\;Mg(NO_3)_2$ instead of MgO was ball milled, the solvent was removed and then the dried powders were calcined at 950$^{\circ}C$/1h. The calcined powder were treated with 3.0 mol% $Ag_2O$ and 1.0 wt% MgO sol and calcined at 550$^{\circ}C$/1h. The dielectrics sintered at 1000$^{\circ}C$/4h under a flowing oxygen showed the density of 7.84g/$cm^3$, the room temperature dielectric constant of 18400, the dielectric loss of 2.4%, the specific resistivity of $0.24{\times}10^{12}{\Omega}{\cdot}cm$. It also showed the bending strength of $120.7{\pm}11.26$ MPa and the fracture toughness of $0.87{\pm}0.002\;MPam^{1/2}$ which were comparable to commercial PZT. The microstructure sonsisted of grains of ∼4${\mu}m$. SEM and SIMS analysis showed that Ag grew as ∼1${\mu}m$ and excess MgO as ∼0.5${\mu}m$.

AN EXPERIMENTAL STUDY OF THE EFFECT OF ALUMINA AND ZIRCONIA ON MECHANICAL PROPERTIES OF DENTAL CORE PORCELAIN (Alumina와 zirconia가 치과용 코아 도재의 물리적 성질에 미치는 영향에 관한 실험적 연구)

  • Shin Hyeon-Soo;Lee Sang-Jin;Lee Keun-Woo
    • The Journal of Korean Academy of Prosthodontics
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    • v.31 no.3
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    • pp.317-349
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    • 1993
  • This study investigated the effect of filler particle size and weight% on mechanical properties of dental core porcelain. In alumina, variation in particle size and weight% and in zirconia, variation in weight%, all specimens were tested three-point bending strength, transmittance, thermal expansion coefficient, porosity and shrinkage and observed with SEM and analysed with X-ray diffractometer. In order to develop shrink-free porcelain, after firing alumina only, glass wasinfiltrated. And aluminum was added to alumina with the expanding character of aluminum oxidize into alumina, and was followed by second firing of glass infiltration procedure. Then mechanical properties were observed. The results of this study were obtained as follows. 1. The bending strength of zirconia was higher than that of alumina, and $5{\mu}m$ alumina had highest strength in variation of particle size of alumina. Except for $5{\mu}m$ alumina, increased with weight%, bending strength increased up to 80% and decreased at 90%. In case of glass infiltration, bending strength was slight higher than 80% and 90% of $5{\mu}m$ alumina. 2. Transmittance increased with increase of shrinkage, decrease of porosity, and with increase of filler size and had no direct correlation with weight%. 3. Thermal expansion coefficient of alumina group was $7.42\sim8.64\times10^{-6}/^{\circ}C$ and that of zirconia group was $9.83\sim12.11\times10^{-6}/^{\circ}C$ and the latter was higher than the former. 4. In x-ray diffraction analysis, alumina group and zirconia group increased $Al_2O_3$ peak and $t-ZrO_2$ peak with increase of weight%. The second phase(cristobalite peak) was observed in zirconia 40% group. 5. Porosity of zirconia was lower than that of alumina and $5{\mu}m$ alumina group had many pores with SEM. In case of low filler content, fracture occurred in glass and high filler content, in glass and filler. In case of aluminum addition to alumina, small oxidised aluminum was observed. 6. Zirconia group had high shrinkage than alumina group, and mixed group of alumina group had high shrinkage. In case of glass infiltration, shrinkage decreased and aluminum addition to alumina group was almost shrink-free.

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Breakage and Liberation Characteristics of Iron Ore from Shinyemi Mine by Ball Mill (신예미 광산 철광석의 볼밀 분쇄 및 단체분리 특성 연구)

  • Lee, Donwoo;Kwon, Jihoe;Kim, Kwanho;Cho, Heechan
    • Resources Recycling
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    • v.29 no.3
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    • pp.11-23
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    • 2020
  • This study aims to investigate breakage and liberation characteristics of iron ore from Shinyemi mine, Jeongseon by ball mill. Parameters of breakage functions for three grade samples of iron ore were obtained using single-sized-feed breakage test and back-calculation based on nonlinear programming. The results showed that with the increase in the grade of iron ore, the breakage rate factor decrease whereas the particle size sensitivity decreases. This results from retardation of microcrack-propagation by magnetite grain in the ore. Breakage distribution analysis showed that the breakage mechanism appear to be impact fracture dominant with the increase of grade owing to the stress distribution effect by magnetite grain. Degree of liberation (DOL) increased with the increase in grade and decrease in particle size, respectively. Using the breakage function and size-DOL relationship, a model that can predict time-dependent-DOL is established. When scale-up factors from operating condition are available, the model is expected to be capable of predicting size and DOL with time in actual mining process.

Algorithm Development and Experimental Verification of Acoustic Emission First-arrival-time Determination for the Source Location (정확한 미소파괴음의 발생위치 분석을 위한 신호 도달시간 결정 알고리즘 연구 및 실험적 검증)

  • Jang, Hyun-Sic;Choi, Jun-Young;Jang, Bo-An
    • The Journal of Engineering Geology
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    • v.25 no.4
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    • pp.587-598
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    • 2015
  • We examined various existing threshold methods for the determination of the first arrival time of acoustic emission (AE), and developed a new variable threshold method that could determine the first arrival time of AE more accurately and more quickly than existing methods. The new method, a modification of an existing threshold method, does not fix the threshold, but applies variable thresholds for the AE signals according to noise analysis. Two- and three-dimensional models were established to test the effectiveness of the new method. It could determine source locations of AE in a two-dimensional model 38.3% more accurately than the pre-existing threshold methods. Its accuracy improvement over the existing methods in a three-dimensional model was about 15.2%. A practical test involved measuring the source locations of AE during three-point bending tests of granite cores. The new method placed the sources closer to the fracture plane than did the pre-existing methods, indicating its superior (and quicker) ability to determine the source locations of AE.

Characteristics of Large-Scale Fault Zone and Quaternary Fault Movement in Maegok-dong, Ulsan (울산 매곡동 일대의 대규모 단층대 특성과 제4기 단층운동)

  • Cho, Jin-Hyuck;Kim, Young-Seog;Gwon, Sehyeon;Edwards, Paul;Rezaei, Sowreh;Kim, Taehyung;Lim, Soon-Bok
    • The Journal of Engineering Geology
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    • v.25 no.4
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    • pp.485-498
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    • 2015
  • Structural analysis for a large-scale fault in Maegok-dong, Ulsan, was carried out based on filed-works to investigate the geometric and kinematic characteristics of the fault as well as its Quaternary slip. As results, a series of repeated stratigraphy, minor faults, fracture zones, and deformation band clusters are observed over a distance of about 100 m in the first studied site consisting of sedimentary rocks, which may indicate the damage zone of a large-scale fault in this site. In the second site, mainly composed of granitic clastic rocks, a large-scale thrust fault is expected based on low-angle dipping faults showing branched and/or merged patterns. Age of the last slip on this fault was restrained as after 33,275 ± 355 yr BP based on radiocarbon dating for organic material included in the gouge zone. Dimension of fault damage zone, dominant sense of slip, and age of the slip event associated with the fault suggest that these structures have a close relationship with the Ulsan Fault and/or Yeonil Tectonic Line, which are well-known large-scale neotectonic structural features around the study area. Therefore, it is necessary to study the characteristics of the faults in detail based on structural geology and paleoseismology in order to ensure seismic and geologic stability of the buildings under construction, and to prevent geologic hazards in this area.

The Analysis of Geothermal Gradient at Icheon Hot Spa Area (이천 온천원보호지구의 지온경사 해석)

  • Lee, Chol-Woo;Moon, Sang-Ho
    • The Journal of Engineering Geology
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    • v.18 no.2
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    • pp.185-190
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    • 2008
  • Nine wells have been developed for uses of thermal waters at the Icheon hot spa area. Drilling depths of those hot spring wells range from 166 to 294 m and their piezometric heads are located at about 50 m below the surface. Using the differences between the surface and bottom temperatures within all boreholes, we can simply estimate geothermal gradient in this area. Thus, we obtained the highest, lowest and average gradient values as $64^{\circ}C/km$ from SB-2 well, $45^{\circ}C/km$ from SB-1 well and approximately $54.28^{\circ}C/km$, respectively. However, observing the MRD-2 well additionally drilled into the depth of 996 m, we found out that this study area has widely experienced the temperature disturbance due to thermal groundwater penetration through the fracture systems within the depth of 720 m. Unlikely this phenomenon, we can conclude that the groundwater flow below the depth of 720 m does not exist. Therefore, using only those temperature data below the 720 m depth, we can estimate reasonable geo-thermal gradient values as $33^{\circ}C/km$ in this study area. Pumping test shows that outflowing temperature is $36^{\circ}C$ corresponding to the temperature logging data at 720 m depth.

Analysis of Predicting Factors for Cardiovascular Injuries in Sternal Fractures (흉골 골절 환자에서 심혈관계 동반 손상의 예측 인자의 분석)

  • 김찬웅;조대윤;손동섭;양기민
    • Journal of Chest Surgery
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    • v.34 no.12
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    • pp.937-943
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    • 2001
  • Background: The aims of this study are to determine the predicting factors related with cardiovascular injuries in sternal fractures and to suggest the indication of emergency echocardiography. Material and Method: A retrospective review of the Ewha Womans University Mok-Dong Hospital trauma registry revealed 40 patients, that visited the hospital with a sternal fracture a over 5-year period. We analyzed 4 factors as predicting factors; 1) presence of restraint, 2) presence of associated injuries, 3) presence of a past medical history involving cardiovascular system, and 4) Revised Trauma Score(RTS). We, also, assessed the utility of conventional study methods involving cardiovascular injuries, such as ECG, chest X-ray, and enzyme level. Based on the methods, we inferred an indication for emergency echocardiography in sternal fractures. Result: Statistically significant predicting factors were the presence of a past medical history involving cardiovascular system and abnormal RTS on admission. Usage of emergency echocardiography depended upon the predicting factors and the results from conventional evaluations. We can now suggest the indications of emergency echocardiography in sternal fractures as 1) if more than two studies reveal abnormality without any significant predicting factors, and 2) if more than one study reveals abnormality with any significant predicting factors. Conclusion: The past medical history involving cardiovascular system and initial vital signs imply the presence of cardiovascular injuries in sternal fractures. And if needed, emergency echocardiography should be performed.

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Injury Analysis of a 25-passenger Bus Left-quarter Turn Rollover Accident (25인승 버스 전복사고의 탑승자 손상 분석)

  • Park, Sang Min;Kim, Sang Chul;Lee, Kang Hyun;Lee, Jae Wan;Jeon, Hyuk Jin;Kim, Ho Jung;Kim, Jin Yong;Kwak, Young Soo;Lee, Woo Sung
    • Journal of Trauma and Injury
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    • v.27 no.3
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    • pp.50-56
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    • 2014
  • Purpose: Rollover motor vehicle crashes have a higher injury severity and fatality than other motor vehicle crash types. From a left-quarter turn rollover accident of 25-passenger bus, we intend to assess the injury of the occupant and the injury severities according to the occupants' position. Methods: We carried out the 3 steps investigation of occupants' interview, visiting the repair shop and using the police report. We analyzed injuries sustained by occupants, and compared injury severities considering column, row in occupant's position and passenger interaction Results: The rollover involved 14 passengers in the bus who were all old women except a man driver. The most common injury was in the upper extremity, with six occurrences being a left clavicle fracture. Major injuries including hemothorax and pneumothorax were diagnosed at left side of the occupant. In the comparison of injury severity among driver's column (left side), mid column and passengercolumn, ISS of passenger column was the highest ($9.9{\pm}7.4$, $8.8{\pm}5.5$, and $10.3{\pm}4.0$, respectively, p>0.05). The injury severity of multiple occupants by row was higher than that of single occupant (10.8 vs. 3, p<0.05). Conclusion: An occupant must fasten their seat belt to prevent an injury by passenger interaction in the left-quarter turn rollover accident of a bus.

Dependences of Ultrasonic Parameters for Osteoporosis Diagnosis on Bone Mineral Density (골다공증 진단을 위한 초음파 변수의 골밀도에 대한 의존성)

  • Hwang, Kyo Seung;Kim, Yoon Mi;Park, Jong Chan;Choi, Min Joo;Lee, Kang Il
    • Journal of the Korean Society for Nondestructive Testing
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    • v.32 no.5
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    • pp.502-508
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    • 2012
  • Quantitative ultrasound technologies for osteoporosis diagnosis measure ultrasonic parameters such as speed of sound(SOS) and normalized broadband ultrasound attenuation(nBUA) in the calcaneus (heel bone). In the present study, the dependences of SOS and nBUA on bone mineral density in the proximal femur with high risk of fracture were investigated by using 20 trabecular bone samples extracted from bovine femurs. SOS and nBUA in the femoral trabecular bone samples were measured by using a transverse transmission method with one matched pair of ultrasonic transducers with a center frequency of 1.0 MHz. SOS and nBUA measured in the 20 trabecular bone samples exhibited high Pearson's correlation coefficients (r) of r = 0.83 and 0.72 with apparent bone density, respectively. The multiple regression analysis with SOS and nBUA as independent variables and apparent bone density as a dependent variable showed that the correlation coefficient r = 0.85 of the multiple linear regression model was higher than those of the simple linear regression model with either parameter SOS or nBUA as an independent variable. These high linear correlations between the ultrasonic parameters and the bone density suggest that the ultrasonic parameters measured in the femur can be useful for predicting the femoral bone mineral density.

A STUDY ON THE BOND OF AESTHETIC RESTORATIVE MATERIALS TO FLUORIDE TREATED ROOT DENTIN (불소처리된 치근상아질에 대한 심미수복재의 결합에 관한 연구)

  • Tak, Heung-Soo;Park, Sang-Jin;Min, Byung-Soon;Choi, Ho-Young;Choi, Ki-Woon
    • Restorative Dentistry and Endodontics
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    • v.23 no.1
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    • pp.197-212
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    • 1998
  • The purpose of this study was to evaluate the effects of fluoride application on the aspect of shear bond strength of three aesthetic restorative materials to dentin. One light-cured composite resin(Palfique Esterite) and two light-cured glass ionomer cements(Fuji II LC and Compoglass)were used in this study. 120 permanent molars were used for this study. The teeth were extracted due to the origin of periodontal disease. The crowns of all teeth were removed, and the remaining roots were embedded in epoxy resin. The mesial or distal surfaces of roots were ground flat to expose dentin and polished on wet 320-, 400-, and 600 grit SIC papers for a total of 120 prepared flat root dentin surfaces. The prepared samples were divided into six groups. Group 1, 3, and 5 were control groups and group 2, 4, and 6 were experimental groups. Sixty samples for experimental groups were treated with 2% NaF solution for 5 minutes. Group 1 and 2 were bonded with Plafique Esterite, group 3 and 4 were bonded with Fuji II LC, and group 5 and 6 were bonded with Compoglass. After 24 hours water storage at $37{\pm}1^{\circ}C$, all samples were subjected to a shear to fracture with Instron universal testing machine(No.4467) at 1.0 mm/min displacement rate. Dentin surfaces treated with each conditioners before bonding and interfacial layers between dentin and aesthetic restorative materials were observed under Scanning Electron Microscope(Hitachi S-2300) at 20Kvp. The data were evaluated statistically at the 95% confidence level with ANOVA test. The result were as follows; 1. Among the control groups, group 1 showed strongest bond strength and group 3 showed weakest. 2. Among the experimental groups, group 2 showed strongest bond strength and group 6 showed weakest. 3. Statistical analysis of the data showed that pretreatment of dentin with 2% NaF solution significantly decreased the bond strength of three aesthetic restorative materials to dentin(P<0.05). 4. SEM findings of fluoride treated dentin surfaces (2, 4, 6 group) demonstrated dentin surfaces covered with fluoridated reaction products. 5. Except group 4 and 6, resin tags were formed in all groups.

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