• Computers and Concrete
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• v.1 no.4
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• pp.389-400
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• 2004

The examinations carried out have confirmed a relationship existing between the character of fracture surfaces and the composition and structure of (basalt and gravel) concretes. For both concretes investigated, a very good correlation was obtained between the profile line development factor, $R_L$, and the fracture surface development factor, $R_S$. With the increase in the $R_L$ parameter, the fracture surface development factor $R_S$ also increased. Agreement between the proposed relationship of $R_S=f(R_L)$ and the proposal given by Coster and Chermant (1983) was obtained. Stereological examinations carried out along with fractographic examinations made it possible to obtain a statistical model for the determination of $R_L$ (or $R_S$) based on the volume of air voids in concrete, $V_{air}$, the specific surface of air pores, $S_V_{air}$ the specific surface of coarse aggregate, $S_{Vagg.}$, and the volume of mortar, $V_m$. An effect of coarse aggregate type on the obtained values of the profile line development factor, $R_L$, as well as on the relationship $R_S=f(R_L)$ was observed. The increment in the fracture surface development factor $R_S$ with increasing $R_L$ parameter was larger in basalt concretes than in gravel concretes, which was a consequence of the level of complexity of fractures formed, resulting chiefly from the shape of coarse aggregate grains.

• Composites Research
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• v.18 no.4
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• pp.14-20
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• 2005

To determine the effect of chemical structure of aromatic amino curing agents on thermal and mechanical properties, standard epoxy resin DGEBF (diglycidylether of bisphenol F) was cured with diaminodiphenyl methane (DDM) and diaminodiphenyl sulphone (DDS) in a stoichiometrically equivalent ratio. From this work the effect of aromatic amino curing agents on the thermal and mechanical properties is significantly influenced by the chemical structure of curing agents. In contrast, the results show that the DGEBF/DDS system having the sulfone structure between the benzene rings had higher values in the thermal stability, density, shrinkage ($\%$), thermal expansion coefficient, tensile modulus and strength, flexural modulus and strength than the DGEBF/DDM system having methylene structure between the benzene rings, whereas the DGEBF/DDS system presented low values in maximum exothermic temperature, conversion of epoxide, and grass transition temperature. These results are caused by the relative effects of sulfone group having strong electronegativity and methylene group having (+) repulsive property. The result of fractography shows that the grain distribution of DGEBF/DDS system is more irregular than that of the DGEBF/DDM system.

• Journal of the Korean Society of Safety
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• v.9 no.1
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• pp.9-18
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• 1994

In this study, we conducted experimental tests to evaluate fracture behaviors of fresh-butt welded metal by Acoustic Emission technique. We selected similar welding and dissimilar welding process, the one welded for SM45C, SS41 and SUS304 of each material, the other for SM45C and SS41, SM45C and SUS304 and SS41 and SUS304. The fracturing processes of weld metal were estimatied through the fracture toughness test with compact tension specimens and fractography analysis. In ASTM test method E-399, type I curves for materials of this study were obtained by load-cod diagram of fracture toughness test. and 5% offset load( $P_{5}$) was estimated as the estimated crack initial load( $P_{Q}$), The estimated crack initial load( $P_{Q}$) of similar welding materials generally lower than base matal, and then SM45C appeared greatly in decreasing rate of PB, SS41 and SUS304 appeared in order. $P_{Q}$ of dissimilar welding materials were lower than the similar welding materials. $P_{Q}$ of welding of SM45C and SS41 appeared in small, SUS304 and SS41 appeared greatly in dissimilar welding materials. In fracture toughness test, AE counts increased before the inflection point of the slope, decreased after that. It was found that increasing of AE counts were due to the microcrack formation at the crack tip near the $P_{5}$ point through AE data. For welding materials in this study, both low and high AE amplitude appeared simulataneously. It was confirmed that the low AE amplotude was due to formation of micro void, micro crack or micro dimple, the high AE amplitude was caused by microvoid coalescence and quasi-cleavage fracture through analyses of fractograpy.apy.apy.apy.

• Korean Journal of Materials Research
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• v.2 no.3
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• pp.172-179
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• 1992

$Al_2O_3/ZrO_2$ composites were fabricated by pressureless sintering from commercial powders and/or nano composite powder of $Al_2O_3/ZrO_2$. The Properties of the composites such as density, strength, hardness and fracture toughness were evaluated. Microstructures and fracture surfaces ware also examined. The flexural strength remains unchanged(~640 MPa) as long as the content of commercial powders is not extreamly high, and depends on microstructures of the composites. Fracture toughness(4.3-5.3 $Mpa{\cdot}m^{1/2}$) increases with increasing content of commercial powders. Fractography shows that failure-initiating sources are 1)surface flaws resulting from machining damage, 2)crack-shaped voids formed due to $ZrO_2$ agglomeration, and 3)surface separation caused by inhomogeneous blending and by sinterability difference between nato composite powder and commercial powders of $Al_2O_3/ZrO_2$. Failure mode of the composites was mainly transgranular.

• Transactions of Materials Processing
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• v.18 no.4
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• pp.296-303
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• 2009

The effect of porosity on the high-cycle fatigue properties of Al-Si-Mg casting aluminum alloys was investigated in this study. Microstructure examination, tensile and high-cycle fatigue test were conducted on both Al-Si-Mg casted (F) and heat-treated (T6) conditions. Porosity characteristics on the fracture surfaces of fatigue-tested samples were examined using SEM and image analysis. The microstructure observation results showed that eutectic Si particles were homogeneously dispersed in the matrix of the Al-Si-Mg casting alloys, but there were porosities formed as cast defects. The high-cycle fatigue results indicated that the fatigue strength of the 356-T6 alloy was higher than that of the 356-F alloys because of the significant reduction in volume fraction of pores by heat treatment. The SEM fractography results showed that porosity affected detrimental effect on the fatigue life: 80% of all tested samples fractured as a result of porosity which acted as the main crack initiation site. It was found that fatigue life decreased as the size of the surface pore increased. A comparison was made between surface pore and inner pore for its effect on the fatigue behavior. The results showed that the fatigue strength with the inner pores was higher than that of the surface pore.

• Journal of the Korean Society of Propulsion Engineers
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• v.20 no.2
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• pp.11-17
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• 2016

Powder metallurgy nickel based superalloy has been used in a high temperature part of turbine engine for airplane. The fatigue crack growth behavior was investigated using CT specimens for the materials at room temperature(R.T.), $600^{\circ}C$ and $700^{\circ}C$. The direct current potential drop(DCPD) method suggested by ASTM E647 was used to measure the crack length during fatigue crack growth at various stress ratios. The fatigue crack growth rate at R=0.5 was faster than that at R=0.1 for all temperature conditions and increased with the increase of stress ratio and temperature. Fractography was conducted for analysis of fracture mechanism.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.05a
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• pp.350-352
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• 2009

The effect of porosity on the high-cycle fatigue properties of Al-Si-Mg casting aluminum alloys was investigated in this study. Microstructure examination, tensile and high-cycle fatigue test were conducted on both Al-Si-Mg casted (F) and heat-treated (T6) conditions. Porosity characteristics on the fracture surfaces of fatigue-tested samples were examined using SEM and image analysis. The microstructure observation results showed that eutectic Si particles were homogeneously dispersed in the matrix of the Al-Si-Mg casting alloys, but there were porosities formed as cast defects. The high-cycle fatigue results indicated that the fatigue strength of the 356-T6 alloy was higher than that of the 356-F alloys because of the significant reduction in volume fraction of pores by heat treatment. The SEM fractography results showed that porosity affected detrimental effect on the fatigue life: 80% of all tested samples fractured as a result of porosity which acted as the main crack initiation site. It was found that fatigue life decreased as the size of the surface pore increased. A comparison was made between surface pore and inner pore fur its effect on the fatigue behavior. The results showed that the fatigue strength with the inner pores was higher than that of the surface pore.

• Journal of Welding and Joining
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• v.32 no.1
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• pp.93-101
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• 2014

This study aims to investigate the effect of heat input of outside SAW weld on low temperature toughness($-20^{\circ}C$) of inside SAW weld for API 5L X70 with sour gas resistance. As increasing heat input of the outside weld, low temperature toughness of the inside weld was decreased. Especially, in spite of the same heat input, the value of low temperature toughness was fluctuated. On the basis of fracture and microstructure analysis, the low temperature toughness is correlated with the fracture area ratio of shear lips and four kinds of fracture sections. These sections were divided with size and shape of dimple correlated with grain boundary ferrite and cleavage correlated acicular and polygonal ferrite in grain. Therefore, it was seen that these sections were two of final solidification area in the inside weld and the outside weld, no reheated zone and reheated zone in the inside weld. In conclusion, it is thought that the difference of low temperature toughness at the same heat input is due to the fact that each of impact test specimens could have the different microstructure, even though the notch was machined under the error tolerance of 1mm. It is because the final solidification area of the inside weld is very narrow.

• Journal of the Korean Society of Safety
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• v.7 no.1
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• pp.65-72
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• 1992

Objective of this research is to evaluate fracture behaviors of fresh-butt welded metal by the acoustic emission technique. The specimens used are medium carbon steel(SM45C), mild steel (SS41) and stainless steel(SUS304), which have different weldability. The similar welding and dissimilar welding processes are considered, in the former SM45C, SS41 and SUS304 are used, in the later the following metals are used SM45C and SS41, SM45C and SUS304 and SS41 and SUS304. The characteristics of fracture in weld metal are eshmated by the tension test with nominal speciemns, the fracture toughness test with compact tension specimens and fractography analysis. The results of tension test show for base metals and similar welding materials that the yield strength and ultimate strength of similar welding materials are increased, the elongation of those are decreased. The weldability of SUS304 is better than that of SM45C and SS41 In similar welding materials. Mechanical properties of dissimilar welding mateiiths we lower than those of similar welding materials. In dissimilar welding materials, the weldability of SM45C and SUS304 is better than that of SM45C and SS41, and also weidability of SS41 and SUS304 is better than SS41 and SM45C. Comparing mechanical properties with AE counts, it is found that AE conuts appeared on a small before the limit load of elasticity(P$_{e}$), and apper greatly near yield strength region in tension test. These results could contribute to the safety analyses and the evaluation of strength for welding structure.e.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.39 no.11
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• pp.1091-1097
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• 2015

Graphite material has been widely used for making the rocket nozzle throat because of its excellent thermal properties. However, when compared with typical structural materials, graphite is relatively weak with respect to both strength and toughness, owing to its quasi-brittle behavior, and gets oxidized at $450^{\circ}C$. Therefore, it is important to evaluate the thermal and mechanical properties of this material for using it in structural applications. This study presents an experimental method to investigate the fracture behavior of ATJ graphite at elevated temperatures. In particular, the effects of major parameters such as temperature, loading, and oxidation conditions on strength and fracture characteristics were investigated. Uniaxial compression and tension tests were conducted in accordance with the ASTM standard at room temperature, $500^{\circ}C$, and $1,000^{\circ}C$. Fractography analysis of the fractured specimens was carried out using an SEM.