• Journal of the Korean Society for Heat Treatment
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• v.26 no.1
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• pp.14-20
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• 2013

Duplex stainless steel, which is a kind of stainless steel with a mixed microstructure of about equal proportions of austenite and ferrite, is generally known as a unique material with excellent corrosion resistance and high strength. However, toughness, strength, and corrosion resistance of the steel could be reduced due to precipitation of topologically closed packed phases such as sigma phase during cooling. In case of large forged products, they have strong possibility that ${\sigma}$-phase precipitates due to difference of cooling rate between surface and inner of the products. Investigation on sigma phase precipitation behavior of duplex stainless steel with change of cooling rate was carried out in this study. Forged SAF 2205 duplex stainless steel was used as specimens to examine the cooling rate effect. Dissolution behavior of sigma phase was also discussed through resolution test of duplex stainless steel containing lots of sigma phase. Experimental results revealed that impact energy was very sensitive to precipitation of small amount sigma phase. However, sigma phase could be removed by short term resolution treatment and impact resistance of the duplex stainless steel was restored.

• Transactions of Materials Processing
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• v.16 no.4 s.94
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• pp.293-298
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• 2007

Recently, there is a need to produce a large forged part for the flight, shipping, some energies, and military industries, etc. Therefore, an open die forging technique of cast ingots is required to obtain higher quality of large size forged parts. Cogging process is one of the primary stages in many open die forging processes. In the cogging process prior to some open die forging processes, internal cavities have to be eliminated for defect-free. The present work is concerned with the elimination of the internal cavities in large ingots so as to obtain sound products. In this study, hot compression tests were carried out to obtain the flow stress of cast microstructure at different temperature and strain rates. The FEM analysis is performed to investigate the overlap defect of cast ingots during cogging stage. The measured flow stress data were used to simulate the cogging process of cast ingot using the practical material properties. Also the analysis of cavity closure is performed by using the $DEFORM^{TM}-3D$. The calculated results of cavity closure behavior are compared with the measured results before and after cogging, which are scanned by the X-ray scanner. From this result, the criteria for deformation amounts effect on the cavity closure can be investigated by the comparison between practical experiment and numerical analysis.

• 보존과학연구
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• s.27
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• pp.165-180
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• 2006

The research was conducted to understand type of iron used by those who lived at dwelling site of Yangsoo-ri in between the first century B.C. and the first century A.D. to make steel products and their technique such as steel making process and heat treatment, based on micro structure information obtained through microscopic metallographic structure analysis with SEM-EDS of six steel productsexhumed at the site. Key findings are summarized as below. In the sense that Si-Ca-Al style and less than 0.5% of Ti were found in the non-metallic inclusion, the material used for forged iron ware was magnetite resolved in that. It is, however, unclear whether magnetite was resolved at high temperature or at low temperature. Microscopic structure analysis revealed that forged steel products were made through repeated hot working, the technique of molding by hitting after heating in the process of resolving and molding iron. As a result, the iron used here for the products was not the iron ore which was produced through resolution from discarded cast iron axe, ingot iron. It is probable that to make those steel products, disposed-of cast iron was reused after being molded by decarburizing. Although a few of relics were analyzed for the research, they were of critical importance in defining the process of ironware production from the first century B.C. and the first century A.D. at the Yangsoo-ri region. Judging from the iron from A-19 dwellingsite, it is possible to conclude that the iron was manufactured from cast iron decarburized and yet more research has to be done into relics yetto be exhumed in order to ascertain the finding. All of these findings are believed to play a critical role in further studies to define the steel-manufacturing technique used on the central Korean peninsular in the ancient times.

• 한국문화재보존과학회:학술대회논문집
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• 2004.10a
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• pp.33-42
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• 2004

The forged iron axe found in the No. 2 wood-framed tomb (the middle 3rd century) of Hwangseongdong, Gyeongju is rectangular on the plane level. It shows an obtuse angle in the edge part, while the joint part has the both sides folded up and shows the traces of wood. Under the reflected light, the Iron axe shines in metal luster, which is bright light gray or light creamy colors. The result of x-ray diffraction analysis shows that the axe consists of magnetite and geothite, which can explain why the composition and structure of the original ore has been kept intact. The microtexture of the axe has the irregular network of ferrite and pearlite, and tile cementite of tiny amount in the ferrite background. The overall treatment of the texture seems to be thermal with a high ratio of carbon. There are fine-grained magnetite, wolframite, quartz, calcite, mica, hornblende and pyroxene inside the axe. Those must be the impurities that they failed to remove in the refining process. The normal ferrite is composed of pure iron whose $Fe_2O_3$ proportion is from 99.16 to $99.84\;wt.\%$. Other than them, the ferrite parts usually contain $Al_2O_3\;and\;SiO_2$. The irregular network of pearlite also contains Impurities including $Al_2O_3\;and\;SiO_2$ and shows highly diverse patterns of carbon content. It's because the axe was carburized after the material was made to resemble pure iron. The decarbonization work didn't go well along the process marks. It's estimated that the original ore was bloom produced in low-temperature reduction and formed around in $727^{\circ}C$, which is eutetic temperature.

• Plant Journal
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• v.10 no.2
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• pp.48-59
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• 2014

Coupons which have same figure as weld joint of the forged steel valves and 1 inch nominal weld thickness were manufactured using ASTM A182 F92 material. After welding with GTAW method, the welded specimens have been post-weld heat treated at $705^{\circ}C$, $735^{\circ}C$, $750^{\circ}C$, $765^{\circ}C$, $795^{\circ}C$ and $825^{\circ}C$ for 1 hour per 1 inch nominal weld thickness each (Group 1) to evaluate characteristics of welds based on various holding temperature. Indeed, 3 welded specimens were post-weld heat treated for 30 minutes, 1 hour and 2 hour (Group 2) at $735^{\circ}C$ to evaluate characteristics of welds based on various holding time. Hardness values were measured at the weld metal, heat affected zone and base metal to observe hardness change depending on the condition. As a result of the evaluation, appropriate holding temperature for PWHT is proved as $750^{\circ}C$ and $765^{\circ}C$ for 1hour per 1 inch nominal weld thickness. Indeed, holding for 1 hour per 1 inch nominal weld thickness was insufficient for PWHT effect when the holding temperature was at $735^{\circ}C$. The microstructure of post-weld heat treated weld metal was determined as tempered-martensite structure.

• Journal of the Mineralogical Society of Korea
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• v.20 no.4
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• pp.231-245
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• 2007

The forged iron axe of the middle 3rd Century found in the No. 2 wood-framed tomb from the Hwangseongdong site, Gyeongju is rectangular on the plane level. The iron axe shines in met-allic luster, which is light grey with pale creamy tint. The result of X-ray diffraction analysis shows that the axe consists of magnetite and geothite, which can explain why the composition and texture of the original ore has been kept intact. There are fine-grained quartz, calcite, mica, magnetite, amphibole, unknown tungsten minerals, pyroxene and olivine inside the axe. Those must be the impurities that they failed to remove in the thermal treatment process. Generally, the iron axe consists mainly of pearlite texture coexisting ferrite and cementite, and show high carbon contents with homogeneous distribution. It can be interpreted the axe was carburized after the material was made to resemble pure iron. The decarbonization work didn't go well along the process marks. Crude ores of the iron axe are possible utilized by magnetite from the Ulsan mine on the basis of the occurrences and inclusions. It's estimated that the original ore was bloom produced in low-temperature reduction and formed around in $727^{\circ}C$, which is eutetic temperature.

• Journal of Ocean Engineering and Technology
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• v.30 no.4
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• pp.334-340
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• 2016

The combustion chamber of a diesel engine is often exposed to a more serious wear and corrosion environment than other parts of the engine because its temperature increases as a result of using heavy oil of low quality. Therefore, repair and built-up welding methods must be performed on worn or corroded parts of the piston crown, exhaust valve, etc. from an economical point of view. In this study, Inconel 718 filler metal was used in repair welding on the groove of a forged steel specimen for a piston crown, along with built-up welding on the surface of another forged steel specimen. Then, the corrosion characteristics of the weld metal zone for the repair welding and the deposited metal zone for the built-up welding were investigated using electrochemical methods in a 35% H₂SO₄ solution. The deposited metal zone indicated better corrosion resistance than the weld metal zone, showing a nobler corrosion potential, higher impedance, and smaller corrosion current density. It is considered that metal elements with good corrosion resistance were generally included in the filler metal, and these elements were also greatly involved in the deposited meta by built-up welding, whereas the weld metal consisted of metal elements mixed with both the filler metal and base metal elements because of the molten pool produced by the repair welding. Finally, it is considered that the hardness of the weld metal was increased by the repair welding, whereas the built-up welding improved the corrosion resistance of the deposited metal.

• Proceedings of the KSME Conference
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• 2001.06c
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• pp.111-115
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• 2001

The die design for hot forging was investigated for manufacturing precisely of scroll rotor made with Al-Si alloy. A scroll rotor is a non-symmetric 3-D shape part, having involute wraps. Disk-shaped billet of Al-Si alloy was extruded to wraps and boss simultaneously. Because the involute wraps is not axi-symmetric, the flow velocity and the stress of die is very much different at each portion. Moreover, the die in wraps portion is a cantilever beam and fractured. In this paper, the analysis of forming and die stress is investigated using the FEM tool, DEFORM-3D. The tensile strength of tool material is $250kg/mm^{2}$. From the analysis results, we can find the maximum principal stress of die is over the fracture strength and redesign the die. The prototype forged part is superior in net shaping and microstructure.

• Bulletin of the Korean Mathematical Society
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• v.20 no.2
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• pp.99-103
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• 1983

Internal heat generation is one of the insidious conditions affecting the quality of an industrial product after it is cast, coated, molded, forged or laminated. Frequently, the product is pressed into service before the exothermic chemical reactions in the generic material has been completed. The heat liberated from this continuing chemical reaction or the residual deformation from the rheological activities in the materials must be adequately removed or prevented, or the product may be discolored, warped, weakened or even "ignited" spontaneously. Numerous instances of premature structural failures, product-recalls, and/or system-malfunctions have been recorded in recent history. The Coulee Dam was poured with pre-chilled concrete just to negate this freakish encore. It is well-known that concrete (a non-isotropic conducting medium), for instance, takes 28 days to develop its full strength. During this period of curing it is conceivable that the processes of internal heat generation, heat conduction and heat dissipation take place simultaneously inside the medium.he medium.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.23 no.7 s.166
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• pp.1215-1222
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• 1999

It is advantageous to use an NDE method to assess the mechanical properties of materials since the conventional method is time-consuming and sometimes requires cutting of sample from the material/component. This paper shows that the ultrasonic and the Barkhausen noise(BHN) methods can be used to accurately characterize forged reactor vessels. The attenuation coefficient of the ultrasonic wave was changed with heat treatment temperature and condition[as-quenched, tempered, PWHT]. The RMS[root mean square] voltage of Barkhausen noise depended on heat treatment temperature and conditions. The fracture appearance transition temperature(FATT) can be predicted using nondestructive evaluation methods.