• Resources Recycling
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• v.8 no.1
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• pp.23-28
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• 1999

Firing characteristics, transverse rupture strength, and heat capacity were studied of the heat-reservoir refractory materials made of red-firing clay, mill scale, and water glass. The firing shrinkage increased with increase of the clay proportion in samples. The volume of fired bodies showed shrinkage by drying up to $300^{\circ}C$, steady expansion in the 300-$700^{\circ}C$ range due to phase transition of iron oxides. and drastic expansion above $1200^{\circ}C$. Flexural strength decreased from 5.6 Mpa to 2.35 Mpa with the decrease of the ratio of clay to mill scale from 1:1 to 1:3 Heat capacities changed from 1.1 Joul/g$^{\circ}$C to 1.35 Joul/g$^{\circ}$C with the ratio of millscale to clay ratio from 1:1 to 1:3. Mill scale in the specimen appears to exist as liquid phase during firing. Firing the specimens in air leads to the eruption of the molten mill scale to the sample surfaces. Contrarily, firing samples in a refractory sagger with a cover suppressed the eruption of the molten mill scale to the surfaces. The addition of mill scale gave rise to porous sintered bodies which would delay cooling rates of heat-reservoir brick.

• Journal of the Korean Ceramic Society
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• v.12 no.4
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• pp.29-36
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• 1975

Korean clinochlore, kaolin, pyrophillite and a technical grade of alumina have been used to investigate the effects of Al2O3 on the formation and properties of cordierite bodies. The body compositions were formulated from the proper proportions of the above raw materials to cover the range of composition from the point corresponding to the stoichiometric formula of cordierite, bythe consecutive increasment of 0.2mol. Al2O3, toward the apex of Al2O3 on the MgO-Al2O3-SiO2 triaxial diagram. Each of bodies was fired with the elevated temperatures from 110$0^{\circ}C$ to 140$0^{\circ}C$ by 5$0^{\circ}C$ interval. Linear shrinkage and water absorption were taken as measures for the firing range of the bodies. The formation of cordierite was estimated from the comparative study of X-ray diffraction and dilatometry of the fired bodies. The formation of a large amount of cordierite was initiated about 120$0^{\circ}C$. The content of Al2O3 exceeded up to 0.8 mol. comparing to the stoichiometric formula of cordierite broadens the firing range of the body.

• Journal of the Computational Structural Engineering Institute of Korea
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• v.22 no.3
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• pp.251-258
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• 2009

At the stage conceptual design, combat vehicle is classified into three general categories of fire power, mobility and physical properties of system. The present research is restricted to fire power and its optimization. At the stage of conceptual designing of system, it is appropriate to consider major variables affecting fire power - including the weight of bullet, which exerts a direct influence on destroying effect, maximum range which takes long range firing in consideration. To estimate the maximum firing range, a simple interior ballistic and an exterior ballistic model were built by using the lumped parameter method, Le Duc method and point mass trajectory model. Design of experiment and regression analysis was used to derive simulations of fire power. Finally, response surface models were built and design variables were analyzed.

• Journal of Soil and Groundwater Environment
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• v.21 no.3
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• pp.58-63
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• 2016

The study examined the level of heavy metal contamination by dividing military rifle shooting ranges into the three areas, i.e firing, trajectory, and target. The target area was found to be contaminated at a level higher (Cu 845 mg/kg, Pb 30,487 mg/kg) than the Worrisome Level of Soil Contamination (hereinafter referred to as the “Worrisome Level”) The trajectory area was predicted to be free from contamination, but it did indicate contamination although it was pretty much lower (Cu 23 mg/kg, Pb 99 mg/kg) than Worrisome Level. This is attributed to the contamination spread when rearranging the soil of the target area during the maintenance of the shooting range. The firing area was also predicted to be free from heavy metal contamination, but the results analyzed indicated a contamination higher (Cu 201 mg/kg, Pb 2,286 mg/kg) than Worrisome Level. This is attributed to the fragments of the broken bullet scattering due to the pressure generated as the bullet leaves the muzzle. An examination of heavy metal contamination in the discharge area as well as gutters to prevent the intrusion of rain water from perimeter revealed a high level of contamination (Cu 298 mg/kg, Pb 6,497 mg/kg), which makes it necessary to take measures.

• Journal of Bio-Environment Control
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• v.15 no.1
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• pp.107-113
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• 2006

These studies were carried out to investigate the quality of green tea processed by different pan-firing hand rolling and to select the best conditions during the procedure of green tea processing the results were as follows. At harvestion tea plant leaf, tea plants had 4 leaves. each leaf size was 7.5 cm'$\square$2.6 cm, and weight of 100 buds 46.6 g. The increase of pan-fired time decreased in the moisture content and yield of green tea. After processing green tea, 5 times pan-fired one had much more contents of total nitrogen (T-N:5.31%), caffeine (2.00%) and total amino acid (T.A.A. : 3,046 mg%) and less content of tannin (13.41%) than the other treatments. but 3 times pan-fired one had the highest contents of vitamin C (204.3 mg%) and chlorophyll (365.0 mg%) among three kinds pan-firing method. Sixteen kinds of free amino acid including theanine as a good taste component of pan-fired green tea were isolated and measured by HPLC. Free amino acid (FAA) contents were in the range of $2,683{\sim}2,925$ mg% and among various pan-firing methods, 5 tims pan-fired one had the highest content of F.A.A. Among these free amino acids, theanine occupied as much as $56.4{\sim}61.3%$ of F.A.A. Lightness, yellowness and redness of 5 times pan-fired green tea were middle value among three different treatments. Besides, it gained the highest score of sensory evaluation among them. These above results suggested that 5 times pan-fired green tea was considered to be the best level as pan-firing times of green tea processing.

• Journal of the Korea Institute of Military Science and Technology
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• v.22 no.6
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• pp.745-753
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• 2019

Recently, with the development of long-range / high-altitude guided weapon system for defense against ballistic missile, test range and firing altitude for guided weapons are increasing. Due to the increase in the test range and the intercepting altitude, it is expected to increase the range of safety area required for the firing test. Comparing to the foreign countries which have many desert or non-residence, in the domestic circumstances where the population is concentrated and distributed, it is more important to predict the falling area and to set the safety area for safely carry out the long-range / high-altitude intercept test. In this paper, we consider the following three points. The first is the booster fall trajectory modeling, the second is the shroud fall trajectory modeling, and finally, the debris dispersion modeling for the missile intercept. Especially, the AUTODYN model was used to predict debris falling area which produced in the high-speed guided missile intercepting test.

• Journal of Magnetics
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• v.5 no.2
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• pp.40-43
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• 2000

Acicular $\alpha-FeOOH\; and\; Ba(OH)_2\cdot8H_2O$ are starting materials in this study. This paper presents the characteristics of the contents of citric acid and heating condition for preparing acicular barium ferrite powder. They control particle shape, crystalline phase, magnetic properties of acicular barium ferrite powder So the effects of the contents of citric acid and heating condition are studied. The experimental condition for starting materials were 800~1000$\circ C$ in firing and 0~40 wt% citric acid, respectively, Ba-ferrite particles fired at the range of 800 $\circ C$to 900 $\circ C$ were maintained as acicular particle shape, but there were mixed particles of acicular and round shape after fired at 950 $\circ C$. Ba-ferrite powder of the single phase was obtained in firing at 900~1000$\circ C$ and with 20 wt.% citric acid. There were unreacted phase of $\alpha-Fe_2O_3 \;and \; BaFe_2O_4$ phases as a second phase in case of sintering at below 850 $\circ C$. Acicular barium ferrite powder of single phase was also produced in firing at 900 $\circ C$ with 20 wt.% citric acid. The saturation magnetization of single phase of acicular $BaFe_12O_19$powder was about 51 emu/g and coercivity was about 4200 Oe.

• Journal of the Korean Ceramic Society
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• v.21 no.1
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• pp.19-26
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• 1984

This study has exemined on the effect for the fitting in porcelain body of $MgO-SiO_2$ system. The mixture was made of corresponding in the theoretical composition of enstatite with Kyul Sung talc and sea water magnesia cake. Hyup Jin kaolin as clay minerals to give the mixtue plasticity was added 10% by weight of the mixture. Also feldspar was added 5% by weight of the above mixture. We added limestone in various kinds of 1%-20% by weight of mixture included kaoil and feldspar in order last of all. The mixture was fire at the various temperatures from 12$25^{\circ}C$ to 13$25^{\circ}C$. After we examined closely physcial properties and microstructures we achieved the following results. 1) 5% addition amount of limestone was good for the property of the strength at the full firing temperatures. But 10% and 15% additions were remarkably excellant below 1275$^{\circ}C$ 2)When we considered the apparent bulk density 5% addition was good for the full firing temperature. 3) 5% addition amount of limestone was proved to be the most excellant propeties between 130$0^{\circ}C$ and 13$25^{\circ}C$ when we considered the apparent bulk density and the range of the firing temperature.

• Journal of the Korean Ceramic Society
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• v.17 no.2
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• pp.96-100
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• 1980

The castable refractory, CaO.$2Al_2O_3$ is a useful alumina cement for iron, steel and cement for iron, steel and cement industries, however it is difficult to produce CaO.$2Al_2O_3$because of its high melting point(180$0^{\circ}C$) and narrow firing range. In this study, the coprecipitation method was used to produce CaO.$2Al_2O_3$ for lower temperature firing . This method involved the titration of mixed solution of calicum and aluminate which extracted from domestic kaolin with $NH4_OH$ solution under blowing $CO_2$ gas into the solution. The coprecipitate and its clacined products were analyzed by X-ray diffraction and DTA. The calcined products fired between 400 and 90$0^{\circ}C$ were amorphous, but at 100$0^{\circ}C$ the coprecipitate was converted into one compound, CaO$2Al_2O_3$. From those experimental results, it was found that we could synthesizze CaO.$2Al_2O_3$ at about 100$0^{\circ}C$ which is lower than conventional firing temperature by around 80$0^{\circ}C$. The refractoriness of this alumina cement was SK 34 and the compressive strength ( 1 day) was about 250kg/$\textrm{cm}^2$.

• Journal of the Korean Ceramic Society
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• v.18 no.4
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• pp.229-236
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• 1981

This study deals with the high temperature (600-135$0^{\circ}C$) properties of Kaolin-Phosphate-Water systems. Phosphoric acid, mono aluminum phosphate, mono ammonium phosphate, the mixture of phosphoric acid and mono aluminum phosphate, and the mixture of phosphoric acid and mono ammonium phosphate were used to characterize the M.O.R of the systems with to quantity of phosphates and firing temperature. Firing shrinkage, creeptest, DTA, TGA, and X-ray diffraction patterns were also measured in order to investigate the factors of strengthening. The resules of the experiments are as follows: 1. Linear shrinkage of kaolin-phosphate systems become larger as the firing temperature rise, and generally in the firing temperature of $600^{\circ}C$ and 100$0^{\circ}C$ the test pieces with phosphate binder show larger then Kaolin-Water system in linear shrinkage and reversed trends were found at 120$0^{\circ}C$ and 135$0^{\circ}C$. 2. Cold M.O.R. of kaolin-phosphate systems show higher trends in strength as the firing temperature rise. Comparing M.O.R. of test pieces after firing at 135$0^{\circ}C$, the mixture of phosphoric acid-mono aluminum phosphate, and phosphoric acid mono ammonium phosphate systems show higher strength than kaolin-mono aluminum phosphate system which widely used, and it shows highest strength when the mole ratio of phosphoric acid and mono ammonium phosphate is 1:1 among the test pieces of kaolin-phosphate systems. 3. The refractoriness of kaolin-phosphate systems are more deteriorated than Kaolin-Water system, and generally, the more addition of phosphate, the lower the refractoriness, however in the range of 4-8% phosphate addition, the difference of the fusion temperature is about 7$0^{\circ}C$. 4. The test pieces of T1 and T2 in creep test were same or even higher than kaolin-water system when 6% of phosphoric acid-mono ammonium phosphate was added to kaolin. 5. In case where the phosphoric acid-mono ammonium phosphate was added to kaolin in mole ratio 1:1 the cold M.O.R., after firing at 135$0^{\circ}C$, refractoriness and $T_2$ in creep test show better results than kaolin-mono-aluminum phosphate system which is widely used. 6. Phosphoric acid and mono ammonium phosphate react with kaolin in temperature over 100$0^{\circ}C$, and it forms aluminum phosphate.