• Title/Summary/Keyword: Firing range

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Optical and Electrical Properties of MgO-CaO thin films as a Protective Layer for AC PDPS (교류형 PDP 보호막용 MgO-CaO 박막의 광학적 특성과 전기적 특성)

  • Jo, Jin-Hui;Kim, Rak-Hwan;Park, Jong-Wan
    • Korean Journal of Materials Research
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    • v.9 no.6
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    • pp.547-550
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    • 1999
  • Optical and electrical properties of MgO-CaO films as a protective layer for AC plasma display panel were studied. When the [(CaO/(MgO+CaO)] ratio of evaporation starting materials was optimum composition, 0.1, firing voltage and memory margin of the film were 176V and 0.5, respectively. When [CaO/(CaO+MgO)] was 0, 0.1 and 0.2, memory margin was 0.39, 0.5 and 0.41, respectively, and surface roughness of films was $27.7\AA$, $21.1\AA$ and $40.3\AA$, respectively. It was thought that memory margin had a reverse-relation with surface roughness. The density of film was calculated by measuring the refractive index of film. The density of MgO film was 3.21g/㎤ and the density of film, when [CaO/(CaO+MgO)] was 0.1, was 3.632g/㎤. The mixture of MgO-CaO films showed a good transmittance property in the visual range.

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Effect of oxygen containing compounds in uranium tetrafluoride on its non-adiabatic calciothermic reduction characteristics

  • Gupta, Sonal;Kumar, Raj;Satpati, Santosh K.;Sahu, Manharan L.
    • Nuclear Engineering and Technology
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    • v.53 no.6
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    • pp.1931-1938
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    • 2021
  • Uranium ingot is produced by metallothermic reduction of uranium tetrafluoride using magnesium or calcium as reductant. Presence of oxygen containing compounds viz. uranyl fluoride and uranium oxide in the starting uranium fluoride has a significant effect on the firing time, final temperature of the charge, slag-metal separation and hence the metal recovery. As reported in the literature, the maximum tolerable limit for uranyl fluoride in the UF4 is 2.5 wt% and limit for uranium oxide content is in the range 2-3 wt%. No theoretical or experimental basis is available till date for these limits. Analyses have been carried out in this study to understand the effect of UO2F2 concentration in the starting fluoride on the final temperature of the products and thus the reduction characteristics. UF4 having uranyl fluoride concentration, less than as well as more than 2.5 wt%, have been investigated. Thermodynamic calculations have been carried out to arrive at a general expression for the final temperature attained by the products during calciothermic reduction of UF4. Finally, an upper limit for the oxygen containing impurities has been estimated using the CaO-CaF2 phase diagram.

Fabrication of $In_2O_3$-based oxide semiconductor thick film ozene gas sensor ($In_2O_3$ 계 산화물 반도체형 후막 오존 가스센서의 제조)

  • 이규정
    • Journal of the Korean Institute of Telematics and Electronics T
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    • v.36T no.1
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    • pp.19-24
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    • 1999
  • $In_2O_3$-based thick films for the ozone detection of ppb range have been investigated. The $In_2O_3$ sensing layer is quite sensitive to ozone, but the saturated stable sensitivity cannot be obtained at the ozone exposure of 100 ppb for 5 min. The addition of $Fe_2O_3$ into $In_2O_3$ indicates some improvement in response time and sensitivity, but it seems the improvement is not good enough for real applications. Firing of $In_2O_3$:$Fe_2O_3$ powder induces remarkable improvement in response and recovery, although the sensitivity decrease. The sensing layer fired at $1300^{\circ}C$ and operated $550^{\circ}C$ shows excellent properties of fast response time, saturated stable sensitivity and rapid recovery characteristics to 100 ppb ozone exposure for 5 min. Especially, it shows the reproducibility of the sensor signal for repeated measurements and the linearity between the ozone concentration and the sensor resistance. The preliminary results clearly demonstrated that the sensor can be successfully applied for the ozone detection of ppb range.

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Tunable Properties of Ferroelectric Thick Films With MgO Added on (BaSr)TiO3

  • Kim, In-Sung;Song, Jae-Sung;Jeong, Soon-Jong;Jeon, So-Hyun;Chung, Jun-Ki;Kim, Won-Jeong
    • Journal of Electrical Engineering and Technology
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    • v.2 no.3
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    • pp.391-395
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    • 2007
  • MgO enhanced $(Ba_{0.6}Sr_{0.4})$ $TiO_3$ thick films have been fabricated by a tape casting and firing method for tunable devices on the microwave frequency band. In order to improve ferroelectric properties, the composite thick films enhanced with MgO on BST have been asymmetrically annealed by a focused halogen beam method. Dielectric constants of composite thick films are changed from 1050 to 1300 at 100 kHz after 60 s and 150 s annealing by the focused halogen beam. Even though no prominent changes were previously observed from the thick films before and after annealing in terms of chemical composition and surface morphology, it is clear that the average particle size of the thick films calculated by Scherrer's formula were increased by annealing. Furthermore, a strong correlation between particle size and dielectric constant of the composite thick films has been observed; dielectric constant increases with increased particle size. This has been attributed to the increased volume of ferroelectric domain due to increased particle sizes. As a result, the tuning range was improved by halogen beam annealing.

Combustion Test Results of Regenerative Cooling Combustor for 30 tonf-class Liquid Rocket Engine (30톤급 액체로켓엔진 연소기 재생냉각 연소시험 결과)

  • Han, Yeoung-Min;Kim, Jong-Gyu;Lee, Kwang-Jin;Lim, Byoung-Jik;Ahn, Kyu-Bok;Kim, Mun-Ki;Seo, Seong-Hyeon;Choi, Hwan-Seok
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2008.05a
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    • pp.133-137
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    • 2008
  • Results of combustion tests performed for a regenerative cooling combustor of a 30 tonf-class liquid rocket engine were described. The combustion chamber has chamber pressure of 60 bar, propellant mass flow rate of 89 kg/s, and nozzle expansion of 12. The combustion chamber is composed of mixing head, baffle injector, and regenerative cooling chamber. The hot firing tests were performed at design and off-design points. The test results show that the combustion characteristic velocity is in the range of 1738${\sim}$1751 m/sec and the specific impulse of the combustion chamber is in the range of 253${\sim}$270 sec. The peak of combustion characteristic velocity and specific impulse for this combustor is shown at mixture ratio of 2.35 and 2.5, respectively.

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Characterization of ITO Films Prepared by Metal Organic Decomposition (유기금속분해 법에 의한 ITO 박막의 제조 및 특성)

  • Go, Seong-Min;Lee, Byeong-Su
    • Korean Journal of Materials Research
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    • v.5 no.8
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    • pp.1045-1049
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    • 1995
  • Thin films of Indium tin oxie (ITO) were prepared by the process of metal organic decomposition. Light transmittance and electrical transport properties of the films were studied with varying the firing temperature and SnO$_2$content. XRD study showed that tin substituted indium in the In$_2$O$_3$lattice. The resistivity had the minimum value of 2.5 ${\times}$ 10$\^$-3/$\Omega$-cm when the content of SnO$_2$was 9wt.%. This value was higher by a factor of 10 than the previously reported results. This difference was attributed to the low mobilities presumably caused by the fine grain size. The transmittance of ITO films in the visible range was over 90%, and the optical energy gap calculated from the absorption edge was in the range of 4.51 and 4.96eV.

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Reduction of 2,4,6-Trinitrotoluene Mobility in Operational Range Soil by Sorption Enhancement and Desorption Decrease Using Monopotassium Phosphate and Montmorillonite (제일인산칼륨과 몬트모릴로나이트 점토를 이용한 사격장 토양 내 2,4,6-trinitrotoluene의 흡착증진 및 탈착감소에 의한 이동성 저감 연구)

  • Jung, Jae-Woong;Yu, Gihyeon;Nam, Kyoungphile
    • Journal of Soil and Groundwater Environment
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    • v.23 no.6
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    • pp.46-53
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    • 2018
  • Mobility reduction of 2,4,6-trinitrotoluene (TNT) was tested by amending monopotassium phosphate (MKP) and montmorillonite to a firing range soil contaminated with TNT. While addition of MKP enhanced sorption of TNT on soil matrix, and combined use of MKP with montmorillonite significantly decreased desorption of TNT as well as remarkably increased the TNT sorption. Montmorillonite amendment by 5% of soil mass resulted in TNT desorption of 0.12 mg/kg from soil loaded with 9.93 mg/kg-TNT. The decrease of TNT desorption was proportional to the amount of montmorillonite amended. At 10 and 15% amendment, only 0.79 and 1.23 mg/kg-TNT was desorbed from 29.33 and 48.80 mg/kg-TNT. In addition, the leaching of TNT with synthetic precipitation leaching procedure (SPLP) and hydroxypropyl-${\beta}$-cyclodextrin (HPCD) decreased, indicating that TNT in MKP/montmorillonite-treated soil became more stable and less leachable. The results demonstrate that addition of MKP and montmorillonite to TNT-contaminated soil reduces the mobility of TNT from soil not only by increasing TNT sorption, but also decreasing TNT desorption. It was found that MKP and montmorillonite amendments by 5 and 10% of soil mass, respectively, were optimal for reducing the mobility of soil TNT.

The Effects of Burning on Composition and Productivity of Grasslands (초지의 구조 및 생산성에 미치는 산불의 영향)

  • 강상준
    • Journal of Plant Biology
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    • v.14 no.3
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    • pp.36-42
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    • 1971
  • The effects of irregular burning of vegetation by man were studied in relation to composition and productivity in a non-agricultural montane grassland in the Chongsun area, Kangwon-Do, Korea. The floristic composition in all study area includes 38 species. Three of the stations are dominated by Arundinella hirta and one is dominated by Miscanthus sinensis. The standing crop of the first station, which was fired in early spring, 1970, was 358.7g/$m^2$ to 497.5g/$m^2$; that of the second station, fired in late 1969 was 351. 5g/$m^2$; the third station, fired sometime in 1968, had a standing crop of 314.5g/$m^2$ to 397.1/$m^2$; the fourth station, having had no recent fires, had a standing crop of 370.0g/$m^2$ to 448.0g/$m^2$. The daily productivity shows a maximum of 6.03g/$m^2$ in the first station, and a minimum of 0.85g/$m^2$ in the fourth station. The productivity of grassland in the study area is at a maximum during July and August because of much precipitation, and decreases rapidly in the months to follow. The productive structure of the first and fourth stations is shown in Fig. 2 and 3. At the first station the maximum height attained by the plants was 180cm. In the height range of 50cm to 100cm there was a maximum of assimilative organs (5.6g/0.25$m^2$$\times$10cm), while in the height range below 50cm there was a maximum of non-assimilative organs (13.0g/0.25$m^2$$\times$10cm). At the fourth station, which has not been fired recently, the maximum height reached by the plants was commonly below 100cm. The assimilative organs showed a maximum abundance in the height range of 40cm to 50cm (4.5g/0.25$m^2$$\times$10cm). while the non-assimilative organs showed their greated abundance in the height range below 10cm (6.0g/0.25$m^2$$\times$10cm). There was a direct relationship between daily productivity and organic matter, available phosphorous, exchangeable calcium and potassium. It appears that the nutrients provided by the ash created in the firing of the study can be an important factor in the productivity of these grasslands.

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Sintering and Microstructure of PZT Ceramics Prepared from Nanoparticles by Sol-Gel Process (나노 입자를 이용한 PZT 압전 세라믹스의 소결 및 미세구조)

  • Park Yong-Kap
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.6 no.6
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    • pp.457-460
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    • 2005
  • Nano-sized titanium oxide and zirconium oxide powders were synthesized by hydrolysis of titanium isopropoxide $[Ti(OC_3H7)_4]$ and zirconium tetrachloride ($ZrC1_4$) via a sol-gel technique. Lead titanate powders were prepared by mixing $TiO_2$ precursors with PbO slurry made with dilute $NH_4OH$. Lead zirconate titanate powders were, then, synthesized by mixing $PbTiO_3$ with $ZrO_2$ powders. The goal of this research was to obtain the $PbZrTiO_3(PZT)$ powders and sintering these powders at low temperature. The $PbTiO_3$ and PZT powders after firing were analyzed by X-ray diffraction(XRD) and transmission electron microscopy(TEM) was utilized to observe the shape and size of the synthesized nano-particles. In the XRD pattern, the well-crystallized PZT phase could be obtained in consequence of firing at $900^{\circ}C$. SEM micrographs also showed that grains of PZT were relatively well grown with the size of the range of $2{\~}4{\mu}m$. The densified perovskite structure of $PbZrTiO_3$ could be obtained by sintering at temperature as low as $900^{\circ}C$. Characterization of the samples showed improved piezoelectric properties.

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Inhibitory action of adenosine on sinus rate in isolated rabbit SA node (토끼 동방결절 박동수에 대한 아데노신의 작용)

  • Chae, Hurn;Suh, Kyung-Phlill;Kim, Ki-Whan
    • Journal of Chest Surgery
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    • v.16 no.2
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    • pp.199-212
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    • 1983
  • The inhibition/influences of adenine compounds on the heart have been described repeatedly by many investigators, since the first report by Druny and Szent-Gyorgyi [1929]. These studies have shown that adenosine and adenine nucleotides have an over-all effect similar to that of acetylcholine [ACh] by slowing and weakening the heartbeat. The basic cellular and membrane events underlying the inhibitory action of adenosine on sinus rate, however, are not well understood. Furthermore, the physiological role of adenosine in regulation of the heartbeat remains still to be elucidated. Therefore, this study was undertaken in order to examine the response of rabbit SA node to adenosine and to compare the response to that of ACh. Isolated SA node preparation, whole atrial pair, or left atrlal strip was used in each experiment. Action potentials of SA node were recorded through the intracellular glass microelectrodes, which were filled with 3M KCI and had resistance of 30-50 M. All experiments were performed in a bicarbonate-buffered Tyrode solution which was aerated with 3% $CO_2-97%$ $O_2$ gas mixture and kept at $35^{\circ}C$. Spontaneous firing rate of SA node at 35C [Mean + SEM, n=16] was 154 + 3.3 beats/min. The parameters of action potentials were: maximum astolic potential [MDP], -731.7mV: overshoot [OS], 9 + 1.4mV; slope of pacemaker potential [SPP], 94 3.0mV/sec.Adenosine suppressed the firing rate of SA node in a dose dependent manner. This inhibitory effect appeared at the concentration of $10^{-6}M$ and was potentiated in parallel with the increase in adenosine concentration. Changes in action potential by adenosine were dose-dependent increase of MDP and decrease of SPP until $10^{-4}$. Above this concentration, however, the amplitude of action potential decreased markedly due to the simultaneous decrease of both MDP and OS. All these effects of adenosine were not affected by pretreatment of atropine [2mg/l] and propranolol [$5{\times}10^{-6}M$]. ACh [$10^{-6}M$] responses on action potential were similar to those of adenosine by increasing MDP and decreasing SPP. These effects of ACh disappeared by pretreatment of atropine [2mg/1]. Inhibition/effects of adenosine and ACh on sinus rate were enhanced synergistically with the simultaneous administration of adenosine and ACh. Marked decrease of overshoot potential was the most prominent feature on action potential. Dipyridamole [DPM], which is known to block the adenosine transport across cell membrane, definitely potentiated the action of adenosine . Adenosine suppressed the sinus rate and atrial contractility in the same dosage range, even in the reserpinized preparation. Above` results suggest that adenosine suppresses pacemaker activity, like ACh, by acting directly on the membrane of SA node, increasing MDP and decreasing SPP.

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