• Transactions of the Korean Society of Mechanical Engineers A
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• v.38 no.5
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• pp.483-487
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• 2014

In this study, joining methods with SiC powder as the joining adhesives were studied in order to avoid the residual stresses coming from CTE (Coefficient of Thermal Expansion) mismatch between substrate and joining layer. The shear strength and microstructure of joined material between SiC substrates are investigated. The commercial Hexoloy-SA (Saint-Gobain Ceramics, USA) used in this work as substrate material. The fine ${\beta}$-SiC nano-powder which the average particle size is below 30 nm, $Al_2O_3$, $Y_2O_3$, and $SiO_2$ were used as joining adhesives. The specimens were joined with 20MPa and $1400-1900^{\circ}C$ by hot pressing in argon atmosphere. The shear test was performed to investigate the bonding strength. The cross-section of the joint was characterized by using an optical microscope and scanning electron microscopy (SEM).

• Journal of the Korean Society for Nondestructive Testing
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• v.20 no.5
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• pp.438-444
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• 2000

The prediction of mechanical properties for WC-Co alloys by evaluation of coercive force and magnetic saturation were studied in relation to their microstructure. The WC-8%Co alloys were prepared using different WC particle size, carbon content and various sintering temperature by PM process. The magnetic properties such as coercive force and magnetic saturation of sintered WC-Co alloys were critically dependent upon their final composition and microstructure. Slight changes of carbon contents and small variation of WC grain size result in marked changes of magnetic properties, hardness and transverse rupture strength of sintered WC-Co alloys. It was found that the coercive force and hardness were increased by fine WC grain size of sinterd alloys, and the coercive force was proportional to hardness. With decreasing total carbon content below the stoichiometric value in WC-8%Co alloys the volume fraction of $\eta$ phase increased steadily, while the magnetic saturation and transverse rupture strength decreased. The magnetic saturation was inversely proportional to the coercive force of WC-Co alloys.

• Applied Chemistry for Engineering
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• v.25 no.2
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• pp.222-226
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• 2014

In this study, the purposes are investigating and analyzing car emission factors for estimating road emissions and the legal framework for the control of particulate matters. At the result, when input emission data are not realistic, the modeling output concentration distributions can lead to a serious distortion of the results. So, the spatial analysis of the dust emission vehicles have to be based on the actual traffic volumes. Because dust emission factors used in the car by National Institute of Environmental Research Method (2010) are mainly targeted for 2003-2007 cars these could not reflect the effect of DPF and the dust emission of gasoline passenger car. So, the real dust emission factors of diesel and gasoline cars need to be developed.

• Geomechanics and Engineering
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• v.23 no.1
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• pp.85-92
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• 2020

This study adopted soil test and laboratory physical model experiments to simulate the tailings impoundment accumulation process according to the principle of similarity. Relying on the practical engineering, it analyzed the tailings deposition characteristics on dry beach surface during the damming process, as well as the variation rules of dam saturation line. Results suggested that, the tailings particles gradually became finer along the dry beach surface to inside the impoundment. The particle size suddenly changed at the junction between the deposited beach and the water surface, which displayed an obvious coarsening phenomenon. Besides, the deposited beach exhibited the vertical feature of coarse upward and fine downward on the whole. Additionally, in the physical model, the saturation line elevated with the increase in dam height, and its amplitude was relatively obvious within the range of 1.0-4.5 m away from the initial dam. Under flood condition, the saturation line height was higher than that under normal condition on the whole, with the maximum height difference of 4 cm. This study could provide an important theoretical basis for further studies on dam failure experiments and the evolution rules of leaked tailings flow.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2005.11a
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• pp.17-20
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• 2005

This study investigates mock-up test of the concrete containing crushed sands with improved quality and following could be draws as conclusions. The slump satisfies the target value. The air content reaches the goal, however, it decreases by the occurrence of loss with elagse of age. In normal strength region, the setting time of CS24 member is shorter than that of SS24 member. In high strength region, the setting time of SS50 member is make only slower than that of CS5O because of the use of retarding AE agent. The compressive strength of the concrete using crushed sands is little higher than the concrete using washed sea sands, and the compressive strength of core sample increases at lower part. Drying shrinkage of the concrete using crushed sands is larger than that using washed sea sands. At water caring condition, both the concrete using crushed sands and using washed sands expand at first, exhibit to be swelled and with elagse of age, they remain relatirely constant. Also, the drying shrinkage occurred greatly when the width and thickness of a member are small because it is easy to evaporate the inner part vapor in the small width and thickness of a member. there can be little different according to the location of a contact gauge, however it is similar to the change of specimen's length change. The concrete using crushed sands, of which grading, grain shape and fine particle is improved, are comparable to the quality of the concrete using washed sea sand.

• Geomechanics and Engineering
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• v.14 no.4
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• pp.307-314
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• 2018

Strength of loess that experienced cyclic freeze and thaw is of great significance for evaluating stability of slopes and foundations in loess regions. This paper takes the frequently encountered loess in the Northwestern China as the study object and carried out three kinds of laboratory tests including freeze-thaw test, direct shear test and SEM test to investigate the strength behaviors of loess after cyclic freeze and thaw, and the correlation with meso-level changes in soil structure. Results show that for loess specimens at four dry densities, the cohesion decreases with freeze-thaw cycles until a residual value is reached and thus an exponential equation is proposed. Besides, little change in the angle of internal friction was observed as freeze-thaw proceeds. This may depend on the varying of soil structure, based on which a clue can be found from the surface morphology and mesoscopic scanning of loess specimens. Clearly we observed significant changes in surface morphology of loess and it tends to aggravate at higher water contents or more cycles of freeze and thaw. Moreover, freeze-thaw cycling leads to obvious changes in the meso-structure of loess including lowering the particle aggregates and increasing both the proportion of fine particles and porosity area ratio. A damage variable dependent on the ratio of porosity area is introduced based on the continuum damage mechanics and its correlation with cohesion is discussed.

• Journal of Korean Society for Atmospheric Environment
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• v.10 no.2
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• pp.90-97
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• 1994

PIXE( Proton Induced X- ray Emission ) analysis has been applied to the analysis of aerosol for the Purpose of pollution monitoring. Coarse and fine Particle fractions were sampled selectively, using Nuclepore filter in stacked filter units, once a month from February to September in 1993 at urban and rural sites. Concentration of 9 elements, Si, S, K, Ca, Mn, Fe, Cu, Zn and Pb was determined without Pretreatment of Samples. Comparison of data between urban and rural site revealed higher elemental concentration level in urban aerosol. From April to May aerosol sampling was carried out daily to observe the effect of Yellow Sand on the composition of aerosol in the Korean Peninsula. During the Yellow Sand period, Si, Ca, Fe content level in aerosol became more than 5 times higher than normal. The elemental concentration of the aerosol samples of Daejeon City was compared with that of two foreign cities. S and Pb( which are fuel- derived elements) levels in Daejeon City aerosol appeared to be lower than those of foreign cities. And it may be due to the leaded-fuel restriction policy of Korean government since 1987.

• Journal of the Korean institute of surface engineering
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• v.26 no.2
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• pp.87-107
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• 1993

The grain size of the final products of WC-Co and WC-Ni composite powders is dependent on the size of the starting material and the conditions employed for the reduction and carburization. APT-Co and -Ni com-plex salts were prepared by the substitution reaction between ammonium ions in APT and the metal ions in Co(NO3)2 and Ni(NO3)2 solutions of different concentrations(0.1 to 0.7M) at $50^{\circ}C$ and the grain sizes of the com-plex salts was $0.54~0.76\mu\textrm{m}$. The complex which calcined the complex salts at $700^{\circ}$~80$0^{\circ}C$ for 60min. were 0.2~0.5$\mu\textrm{m}$. W-Co($5.92^{\circ}C$) and -Ni(6.95%) powders which reduced the complex oxides with H2d atmo-sphere(flow rate;600cc/min.) at $700^{\circ}$~$800^{\circ}C$ for 60min. were $0.5~0.6\mu\textrm{m}$. The mean grain sizes of WC-Co and WC-Ni composite powders which carburized both complex metals of W-Co and W-Ni at $800^{\circ}C$ for 60min. were $0.5~0.6\mu\textrm{m}$, and take place the coarsening of the grain above $800^{\circ}C$ and the optmium ratio of C3H8 and H2 was 0.2 for the control of the free carbon. The effect of Co contents on the particle sizes decreased from 0.4 to $0.25\mu\textrm{m}$ with increasing the content from 2.0 to 7.6w%. The activation energies on the reductions of oxides and the formations of carbides were as follows ; W-Co : Q = 8.7 kcal/mole, W-Ni : Q = 8.1 kcal/mole, WC-Co pow-der : Q = 17.8 kcal/mole, WC-Ni powder : Q = 16.6 kcal/mole.

• YAKHAK HOEJI
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• v.42 no.2
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• pp.153-158
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• 1998

Calcium hydrogen phosphate was synthesized by reacting calcium chloride and sodium hydrogen phosphate solution in this study. It is well known that the particle size and yield o f calcium hydrogen phosphate produced is greatly affected by the synthetic conditions such as the reactant concentration, reaction temperature, reacting fine, mole ratio and drying temperature, etc. The purpose of this study is to investigate the optimum synthesis condition from the viewpoint of yield and sedimentation volume of the prepared calcium hydrogen phosphate powder according to a randomized complete block design proposed by G.E.P. Box and K.B. Wilson. It was found that the optimum synthetic conditions of calcium hydrogen phosphate were as follows: It was found that optirnum temperature range of reactant solutions was $28-38^{\circ}C$ and $32-42^{\circ}C$ respectively, on the viewpoint of yield and sedimentation volume. The optimum concentration range of reactant solutions was 5.5-10.0% and 6.9-7.4% respectively, on the viewpoint of yield and sedimentation volume. The optimum mole ratio of $CaCl_2$ to $Na_2HPO_4$ was in the range of 1.2-2.0 and the optimum reacting time range was 8.5-11.0 minutes. The optimum drying temperature range was $39-41^{\circ}C$ from the viewpoint of yield, but it was $39-43^{\circ}C$ on the basis of sedimentation volume. Crystallographic analysis to X-ray diffraction patterns of commercially available ecalcium hydrogen phosphate and calcium hydrogen phosphate samples prepared in this study suggested that all samples tested belonged to monoclinic crystal system characteristic of $CaHP0_4{\cdot}2H_20$ crystals.

• Proceedings of the Korea Concrete Institute Conference
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• 2008.04a
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• pp.733-736
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• 2008

This study, with the purpose for early quality improvement of concrete which used large quantity of fly ash, changed various admixture material type and reviewed the basic characteristics. First off, the flow overall was highest when polycarb onic Acid high early strength AE water reducing agent was displaced, while air amount satisfied target level only in the case of plain, and setting time was shown best by getting 30 more minutes than plain and about 3 more hours than conventional when KOH is displaced. Compressive strength was shown best at age 1 day and 3 days when KOH was displaced, and at age 28 days when fine particle cement was displaced. By and large, this study concludes that concrete quality improvement admixture material that used large amount of fly ash showed worse effects than plain, therefore it is determined that there need be more study for development of concrete early quality improvement admixture material that used large amount of fly ash.