• 한국재료학회지
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• 제1권2호
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• pp.93-98
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• 1991

The as-grown $YBa_2Cu_3O_{7-x}$ superconducting thin films on MgO(100) substrate have been prepared by a reactive coevaporation method. The superconducting transition temperature, surface morphology and crystalline quality were examined as a function of the substrate temperature ranging from $450^{\circ}C$ to $590^{\circ}C$. From the reflection high energy electron diffraction (RHEED) analysis, it was found the film consisted of almost amorphous phase with a halo pattern deposited at the substrate temperature of $450^{\circ}C$. The film deposited at the substrate temperature of $510^{\circ}C$ consisted of polycrystalline phase, showing a broad ring pattern. On the other hand, for the film deposited at $590^{\circ}C$, RHEED showed spotty pattern indicating that this film consisted of single crystal phase. It has rough film surface due to the surface outgrowth. The surface outgrowth increased as the substrate temperature increased from $510^{\circ}C$ to $590^{\circ}C$. the surface outgrowth may be due to the anisotropic growth rate. The highest transition temperature obtained in this study was $Tc_{zero}$ of 83K with $Tc_{onset}$ of 88K for the film deposited at $590^{\circ}C$ using activated RF oxygen plasma.

• 한국세라믹학회지
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• 제43권9호
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• pp.515-518
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• 2006

The microstructure of $ZrO_2$ toughened $Al_2O_3$ ceramics was carefully controlled so as to obtain dense and fine-grained ceramics, thereby improving the properties and reliability of the ceramics for capillary applications in semiconductor bonding technology. $Al_2O_3-ZrO_2(Y_2O_3)$ composite was produced via Ceramic Injection Molding (CIM) technology, followed by Sinter-HIP process. Room temperature strength, hardness, Young's modulus, thermal expansion coefficient and toughness were determined, as well as surface strengthening induced by the fine grained homogenous microstructure and the thermal treatment. The changes in alumina/zirconia grain size, sintering condition and HIP treatment were found to be correlated.

• 한국세라믹학회지
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• 제43권12호
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• pp.829-832
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• 2006

In this study, the influence of the magnetic field on ferrite slurry's injection time during the slurry forming process was investigated. The evaluation system of the slurry's injection time under the strong magnetic field was designed with FEM and manufactured. Studied parameters were the applied magnetic field, the input pressure of the slurry, and the supplying tube materials. As the results, the injection time was increased with the external magnetic field strength and rapidly decreased with increasing the input pressure of the slurry. Also the injection time was decreased when the supplying tube was manufactured with the magnetic material having the higher magnetic permeability than the ferrite.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 1998년도 제27회 춘계학술대회
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• pp.139-145
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• 1998

This paper addresses the R-curve properties, wear resistance, and erosion resistance of the two silicon carbide ceramics with different microstructures, i.e. , fine grained SiC and in situ-toughened SiC(IST SIC). Fine grained SiC exhibits a relatively flat R-curve behavior whereas the IST SiC exhibits a increasing R-curve behavior. The increasing R-curve behavior in IST SiC is attributed to relatively weak grain boundaries. The rate of material removal during wear tests and erosion tests was higher for IST SiC than that for fine grained SiC. This is attributed to the weaker grain boundaries in IST SiC than that in fine grained SiC. It is implied that fracture toughness in short crack regime should be taken into consideration in the interpretation of the microscopical material removal process. We show that the higher the strength of grain boundaries is, the higher wear and erosion resistances are.

• 한국세라믹학회지
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• 제42권11호
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• pp.753-757
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• 2005

In this study, we attempted to recycle the fly ash as a mullite whisker with addition of $Al_{2}O_{3}$ to obtain the high yield of mullite whisker. During the reaction process, mullite whisker was formed with the reaction of amorphous $\alpha$-Cristobalite and Anorthite above $1350^{\circ}C$. With increasing the heat treatment temperature and time, the mean length and aspect ratio of mullite whiskers was gradually increased.

• 한국세라믹학회지
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• 제30권12호
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• pp.987-992
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• 1993

In order to synthesize the heat resistance ceramics of LAS system, we studied on preparing the fine powder with homogeneity by sol-gel method using metal alkoxide. Various results were obtained depending on the composition and process. When the amount of H2O added at initial stage is higher than 10mol/$\ell$, and when the amount of catalyst is 0.1mol/$\ell$, the particle size of synthesized hydrate becomes finer. On condition that partial prehydrolysis time of TEOS is more than 50 hours, the monosized fine powder is obtained(below 1${\mu}{\textrm}{m}$).

• 한국초전도학회:학술대회논문집
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• 한국초전도학회 2001년도 High Temperature Superconductivity Vol.XI
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• pp.67-67
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• 2001

• 한국세라믹학회:학술대회논문집
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• 한국세라믹학회 1986년도 Priceedings Of The Third Korea-Japan Seminar On New Ceramics
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• pp.23-49
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• 1986

• 한국세라믹학회:학술대회논문집
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• 한국세라믹학회 1986년도 Priceedings Of The Third Korea-Japan Seminar On New Ceramics
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• pp.55-65
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• 1986

• 대한화학회지
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• 제38권6호
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• pp.411-417
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• 1994

난용성 신소재 중의 하나인 파인 세라믹의 분석을 위하여, 알칼리 용융법과 고압 산분해법 등의 시료 전처리법을 유도결합원자발광분석기(ICP-AES)를 이용하여 연구하였다. Al2O3 분말을 분석하여 본 결과, 고압 산분해법이 알칼리 용융법보다 재현성 있는 측정치를 얻을 수 있었다. SiC분말의 경우에서는 고압산분해법으로 처리한 후 Si매트릭스를 Si-F형태로 증발시켜서 분석하여 본 결과 분말 중의 ppm 농도 범위의 불순물들이 매트릭스에 의한 간섭없이 분석되었다. 일본 인증기준물인 JCRM022, JCRM023 초미립 분말을 고압 산분해법으로 분석하여 본 결과, 좋은 재현성과 높은 정확성을 나타내었다.