• Journal of Powder Materials
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• v.8 no.3
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• pp.210-213
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• 2001

$Si_3N_4$/TiN nano/nano-type composites were successfully fabricated by the combination of a mechano-chemical grinding (MCG) method and a short time sintering process, and their wear resistance was evaluated. Powder mixtures of $\alpha-Si_3N_4$and Ti were prepared using mechano-chemical grinding process and the resulting nanocomposite powder mixtures were consolidated using pulsed electric current sintering (PECS). TEM observation showed that the nano/nano-type composites consisted of homogeneous and very fine matrix grains with the size less than 100 nm. The obtained $Si_3N_4$-based nano/nano-type showed high wear resistance and electric discharge machinability.

• Journal of Powder Materials
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• v.9 no.2
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• pp.124-132
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• 2002

Nano Cu powders, synthesized by Pulsed Wire Evaporation (PWE) method, have been compacted by Magnetic Pulsed Cojpaction(MPC) method. The microstructure and mechanical properties were analyzed. The optimal condition for proper mechanical properties with nanostructure was found. Both pure nano Cu powders and passivated nano Cu powders were compacted, and the effect of passivated layer on the mechanical properties was investigated. The compacts by MPC, which had ultra-fine and uniform nanostructure, showed higher density of 95% of theoretical density than that of static compaction. The pur and passivated Cu compacted at $300^{\circ}C$ exhibited maximum hardnesses of 248 and 260 Hv, respectively. The wear resistance of those compacts corresponded to the hardness.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2006.05a
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• pp.57-61
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• 2006

Waste foundry sand of industrial waste which is happening by vast quantity according to fast development of industry has much the occurrence amount and processing method is depended on reclamation, and is using by fine aggregate for construction by recycling method among others. In this research Waste foundry sand powder into cement replace fare use possibility availability judge wish to Slump and air content decreased the replacement ratio increases by concrete special quality that do not harden according to experiment result, and unit capacity mass and bleeding increased the replacement ratio increases. Hardening concrete intensity special quality displayed strength improvement to replacement ratio 20%, and tendency that watertightness increases most in replacement ratio loft in watertight property appear. Considering the strength and watertight properties, the adequate usage of waste foundry sand powder is the 10% of replacement ratio.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.1292-1293
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• 2006

A non-equilibrium powder metallurgy processing such as an MA/SPS (Mechanical Alloying / Spark Plasma Sintering) process is examined in a Ti-48moll%Al. TiAl intermetallic compound is a potential light-weight/high-temperature structural material. One of the major problems, however, limiting the practical use of the material is its poor workability. From this point, the powder metallurgy (PM) processing route has been attractive alternative of the conventional processing for such material The MA/SPS process is able to apply to a LIGA process. Optimization of the pseudo-superplasticity enables to fabricate micro-parts made of fine grained ceramics composites of TiAl by the LIGA process.

• Journal of Powder Materials
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• v.10 no.3
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• pp.157-160
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• 2003

Phase contents and elemental composition of ultradispersed powders obtained by the electrical explosion of tin-leadalloy powders are investigated. It is demonstrated that during the explosion and subsequent cooling, surface layers of powder particles are enriched in lead compared to the initial alloy. The thermal stability of powders oxidizing in air is also investigated.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.720-721
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• 2006

The new alloy$^{1)}$ is made from rapidly solidified Al-Ni-Zr-Ce aluminum alloy powder, and has the following unique mechanical characteristics:(1) The stress-strain curve shows a yield point; (2) The alloy shows high heat resistance; (3) Although the alloy is submicron particle diameter, it shows excellent creep resistance. We observed the micro structures of this new alloy, and it is thought that is based on the following reasons:(1) The dislocation strongly adheres to the alloy's many crystal boundaries;(2) The added alloying elements have a small diffusion coefficient in aluminum;(3) The tiny intermetallic compound particles crystallizing at the grain boundary.

• Journal of the Korean Ceramic Society
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• v.23 no.4
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• pp.11-16
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• 1986

$BaTiO_3$ ceramics powder was prepared by coprecipitation method either in oxalic acid solution or in potassium hydroxide solution. Thermal decomposition of coprecipitated $BaTiO(C_2O_4)_2$.$4H_2O$ powder in oxalic acid solution was investigated by means of Themogravimetry Differential Thermal Analysis and X-ray Diffraction Analysis. Low temperature decomposition of coprecipitated $BaTiO(C_2O_4)_2$.$4H_2O$ caused narrow particle size distribution whereas high temperature decomposition caused fairly wide particle size distribution by partial sintering. As the reaction time increased the average particle size of coprecipitated $BaTiO_3$ powder in KOH solution was increased. The most narrow paticle size distribution was obtained when the coprecipi-tates were ripened for 4hrs.

• Journal of the Korean Ceramic Society
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• v.26 no.2
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• pp.201-209
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• 1989

Fine Si-Al-OH coprecipitate powders were prepared from Si- and Al-alkoxides by the hydrolysis method. $\beta$-Sialon powder was obtained from prepared Si-Al-OH coprecipitate by the simultaneous reduction and nitridation method. The syntehsized Sialon powder was pressureless sintered at 175$0^{\circ}C$ for 90 min in N2 atmosphere. The characterization of the Sialon powder was performed with XRD, BET, SEM, TEM and particle size analysis. The sinterability and mechanical properties of sintered bodies were investigated in terms of relative density, M.O.R., fracture toughness, hardness and the morphology of microstructure. The highest values of their mechanical properties were obtained for the $\beta$-Sialon ceramics at Z=1 and those values are as follows : M.O.R., KIC and HV of $\beta$-Sialon ceramics(Z=1) are 499.1 MPa, 5.9MN/m3/2 and 18.7GPa, respectively.

• Journal of the Korean Ceramic Society
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• v.25 no.6
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• pp.585-592
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• 1988

Aluminum sec-butoxide was synthesized from aluminum foil and alcohol. The characteristics of the alumina powder prepared from the synthesized alkoxide by the Yoldas method were studied. As a result of measuring the synthesized aluminum sec-butoxide by GC, the purity of the synthesized alkoxide was 98.7% on the basis of commercial alkoxide and the yield was 78.5%. A127-MASNMR analysis shows that powders dried at 9$0^{\circ}C$ and $\alpha$-Al2O3 have 6-cordinated structure and ${\gamma}$-Al2O3 has 4-coordinated structure. The characteristics of alumina powder prepared from the synthisized alkoxide showed the same characteristics with the alumina powder prepared from the commercial alkoxide.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2019.05a
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• pp.207-208
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• 2019

In this study, compressive strength was measured to evaluate the initial strength of cement mortar substituted with coal gasification slag containing desulfurized gypsum, and the reactivity of desulfurized gypsum was confirmed. In order to improve the reactivity, 2% gypsum mixed type and gypsum unfedged type specimens were fabricated and the influence of desulfurization gypsum on compressive strength of coal gasification slag and blast furnace slag fine powder replacement cement mortar was compared and confirmed. As a result of the experiment, it was confirmed that the initial compressive strength of the specimen containing the desulfurized gypsum was improved at the initial stage.