• Title/Summary/Keyword: Fine material

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Production of Fine ZnO Powders by Carbothermal Reduction

  • Choi, Heon-Jin;Lee, June-Gunn;Jung, Kwang-Taik;Kim, Ki-Hwan
    • The Korean Journal of Ceramics
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    • v.4 no.4
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    • pp.304-310
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    • 1998
  • Carbothermal reduction has been one of the important processes for the production of ceramic raw materials such as silicon carbide, silicon nitride, boron carbide, etc. The process has also been one of several trials for the recovery of ZnO from ZnO-containing waste. It usually involves two consecutive steps: the evolution of Zn vapor and its oxidation with air. In this study a ZnO-containing raw material is reduced by carbon at $1250^{\circ}C$ and the evolved Zn vapor is oxidized with air, resulting in fine powders of ZnO. computer programs, THERMO and PYROSIM developed by MINTEK, are used to simulate the process thermodynamically and the results are compared with the experimental results. It is shown that the ZnO-containing raw material can be reduced and can form fine ZnO with the yield as high as 98.7% under a proper condition. Based on these results, a process is engineered for the production of ZnO in a rotary kiln at a rate of 3 tons/day. The produced ZnO powders show properties suitable to the usual applications in ceramic industries with a purity of > 95wt% and an average particle size of ∼3${\mu}m$.

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Adaptive fluid-structure interaction simulation of large-scale complex liquid containment with two-phase flow

  • Park, Sung-Woo;Cho, Jin-Rae
    • Structural Engineering and Mechanics
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    • v.41 no.4
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    • pp.559-573
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    • 2012
  • An adaptive modeling and simulation technique is introduced for the effective and reliable fluid-structure interaction analysis using MSC/Dytran for large-scale complex pressurized liquid containment. The proposed method is composed of a series of the global rigid sloshing analysis and the locally detailed fluid-structure analysis. The critical time at which the system exhibits the severe liquid sloshing response is sought through the former analysis, while the fluid-structure interaction in the local region of interest at the critical time is analyzed by the latter analysis. Differing from the global coarse model, the local fine model considers not only the complex geometry and flexibility of structure but the effect of internal pressure. The locally detailed FSI problem is solved in terms of multi-material volume fractions and the flow and pressure fields obtained by the global analysis at the critical time are specified as the initial conditions. An in-house program for mapping the global analysis results onto the fine-scale local FSI model is developed. The validity and effectiveness of the proposed method are verified through an illustrative numerical experiment.

Growth of High Uniform Polycrystalline Grain on the Highly Ordered Porous Anodic Alumina (다공질 양극산화 피막을 이용한 고균일 다결정 살리콘의 성장)

  • Kim, Jong-Yeon;Han, Jin-Woo;Kim, Young-Hwan;Kim, Byoung-Yong;Seo, Dae-Shik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.375-375
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    • 2007
  • In the conventional crystallization method, thepoly-Si TFTs show poor device-to-device uniformity because of the random location of the grain boundaries. However, our new crystallization method introduced in this paper employed substrate-embedded seeds on the highly ordered anodic alumina template to control both the location of seeds and the number of grain boundaries intentionally. In the process of excimer laser crystallization (ELC), a-Si film deposited on the anodic alumina by low pressure chemical vapor deposition (LPCVD) is transformed into fine poly-Si grains by explosive crystallization (XC) prior to primary melting. At the higher energy density, the film is nearly completely melted and laterally grown by super lateral growth (SLG) from remained small part of the fine poly-Si grains as seeds at the Si/anodic alumina interface. Resultant grain boundaries have almost linear functions of the number of seeds in concavities of anodic alumina which have a constant spacing. It reveals the uniformity of. device can be enhanced prominently by controlling location and size of pores which contains fine poly~Si seeds under artificial anodizing condition.

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The effects of applied voltage on copper powder manufactured by electric explosion (전기폭발방식을 이용한 동(Cu) 미분 제조 및 인가전압의 영향)

  • Lee, Hoo-In;Kim, Won-Baek;Suh, Chang-Youl;Sohn, Jeong-Soo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.11a
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    • pp.474-475
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    • 2007
  • Wire electrical explosion(WEE) has been used for the production of fine metal particles. In WEE, electrical powder was stored and compressed into capacitor and released to produce fine particles through evaporation and condensation. In this study, the effect of applied voltage on the size of copper powders was investigated. High tension was added up to the explosion device by dividing 4 steps. At voltages lower than 5.2 kV, the fraction of powders finer than $44{\mu}m$ was almost negligible. The effectiveness of explosion increased sharply with increased voltage over 5.8 kV. At the highest voltage of 6.4 kV, more than 80% of explosion products were finer than $44{\mu}m$.

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Fabrication and Characterizations of Nickel Metal Mask with fine Pitch by Additive Process (Additive 공정을 이용한 미세 피치용 니켈 메탈마스크의 제조 및 특성평가)

  • Park, Eui-Cheol;Lim, Jun-Hyung;Kim, Kyu-Tae;Park, Si-Hong;Hwang, Soo-Min;Shim, Jong-Hyun;Jung, Seung-Boo;Kim, Bong-Soo;Joo, Jin-Ho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.20 no.11
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    • pp.925-931
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    • 2007
  • We successively fabricated the Ni metal mask by additive method and evaluated the effects of wetting agents addition on the microstructure, hardness, and friction coefficient. In the process, the additive patterns with fine hole and pitch were made by photolithography technique and subsequently Ni plate was electroformed on the patterns. We found that the microstructure and mechanical properties were significantly varied when the different combinations of the wetting agents were used. When the wetting agents of both SF-1 and SF-2 were added, the microstructure consisted of crystal and amorphous phases, the grain size reduced to 5-40 nm, the RMS value decreased to 11.4 nm and the wear resistance improved. In addition, the hardness was as high as 638 Hv which is higher than that of commercial stainless steel mask and this improvement is probably due to the presence of amorphous Phase and fine grain size. The improvement of the wear resistance can provide a higher reliability and a longer service life.

An Experimental Study on the Properties of Concrete Substituting the Rapid Chilled Steel Slag for Fine Aggregate (잔골재를 급냉제강(急冷製鋼)슬래그로 대체(代替)한 콘크리트의 특성(特性)에 관(關)한 실험적(實驗的) 연구(硏究))

  • Kim, Nam-Wook;Park, Min-Wook;Bae, Ju-Seong
    • Resources Recycling
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    • v.17 no.1
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    • pp.73-79
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    • 2008
  • Along with the increased social infrastructures and reconstruction, the demand for aggregate, which is used in concrete, has rapidly increased. However, there are problems due to the exhaustion of natural aggregate resources, and strict restrictions. In this study, the possibility of using rapid chilled steel slag as a substitutive material of fine aggregate is determined from the property test and mechanical test for the concrete that is made with rapid chilled steel slag, which highly decreases the free CaO, the main problem of the steel slag.

Effect of Co-Substitution on the Crystallization and Magnetic Properties of a Mechanically Milled Nd15(Fe1-xCox)77B8 (x=0-0.6) Alloy

  • Kwon, H.W.;Yang, C.J.
    • Journal of Magnetics
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    • v.7 no.4
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    • pp.143-146
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    • 2002
  • Mechanical milling technique is considered to be a useful way of processing the fine Nd-Fe-B-type powder with high coercivity. In the present study, phase evolution of the $Nd_{15}(Fe_{1-x}Co_{x})_{77}B_{8}$ (x=0-0.6) alloys during the high energy mechanical milling and annealing was investigated. The effect of Co-substitution on the crystallization of the mechanically milled $Nd_{15}(Fe_{1-x}Co_{x})_{77}B_{8}$ amorphous material was examined. The Nd-Fe-B-type alloys can be amorphized completely by a high-energy mechanical milling. On annealing of the amorphous material, fine $\alpha$-Fe crystallites form first from the amorphous. These fine $\alpha$-Fe crystallites reacts with the remaining amorphous afterwards, leading to crystallization to $Nd_2Fe_{14}$B phase. The Co-substitution for Fe in $Nd_{15}(Fe_{1-x}Co_{x})_{77}B_{8}$ ($\mu$x=0∼0.6) alloys lower significantly the crystallization temperature of the amorphous phase to the $Nd_2Fe_{14}$B phase. The mechanically milled and annealed $Nd_{15}Fe_{77}B_8$ alloy without Co-substitution exhibits consistently better magnetic properties with respect to the alloys with Co-substitution.

Influence of plastic viscosity of mix on Self-Compacting Concrete with river and crushed sand

  • Rama, J.S. Kalyana;Sivakumar, M.V.N.;Kubair, K. Sai;Vasan, A.
    • Computers and Concrete
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    • v.23 no.1
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    • pp.37-47
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    • 2019
  • In view of the increasing utility of concrete as a construction material, the major challenge is to improve the quality of construction. Nowadays the common problem faced by many of the concrete plants is the shortage of river sand as fine aggregate material. This led to the utilization of locally available materials from quarries as fine aggregate. With the percentage of fines present in Crushed Rock Fines (CRF)or crushed sand is more compared to river sand, it shows a better performance in terms of fresh properties. The present study deals with the formulation of SCC mix design based on the chosen plastic viscosity of the mix and the measured plastic viscosity of cement pastes incorporating supplementary cementitious materials with CRF and river sand as a fine aggregate. Four different combinations including two binary and one ternary mix are adopted for the current study. Influence of plastic viscosity of the mix on the fresh and hardened properties are investigated for SCC mixes with varying water to cement ratios. It is observed that for an increasing plastic viscosity of the mix, slump flow, T500 and J-ring spread increased but V-funnel and L-box decreased. Compressive, split tensile and flexural strengths decreased with the increase in plastic viscosity.

Properties of Cement Matrix Using Vegetable Activated Carbon (식물성 활성탄을 활용한 시멘트 경화체의 특성)

  • Lee, Jae-Hoon;Park, Chae-Wool;Lee, Sang-Soo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2020.06a
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    • pp.138-139
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    • 2020
  • With the rapid progress of industrialization, indoor air quality is a very important factor for modern people who spend most of their day indoors. The recent issue of fine dust and radon on the portal site's popularity search shows that interest in indoor air quality has increased. Fine dust causes respiratory diseases, and radon causes severe lung cancer. The new material was tested using plant activated carbon, palm activated carbon and bamboo activated carbon. Both palm activated carbon and bamboo activated carbon are porous materials and generate smooth physical adsorption. As a result of the experiment, both the activated carbon tends to gradually decrease in strength and fluidity as the replacement ratio increases. The reason for this is that both activated carbons have the property of absorbing moisture, so it is judged that the strength is lowered by absorbing moisture necessary for curing. In the case of fluidity, it is judged that the fluidity is reduced by absorbing the moisture required for the flow. In the future, if the problem of the color of the finished cured body is compensated, it will be possible to manufacture a functional finishing board to replace the existing interior finishing material.

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Effects of Dolomite Fine Aggregate and Cement-Based Materials on Viscosity Characteristics, Flow and Flow Time of High-Strength Grout (돌로마이트 잔골재와 시멘트계 재료의 용적 구성비가 고강도 그라우트의 점도 특성, 플로우 및 유하시간에 미치는 영향)

  • Jeong, Min-Gu;Lee, Han-Seung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2023.05a
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    • pp.197-198
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    • 2023
  • This study was conducted as part of research and development of high-strength grout. Accordingly, dolomite aggregate was used as a filler incorporated into the high-strength grout. Dolomite aggregate has a disadvantage of increasing the viscosity of the grout due to higher generation of fine powder than other aggregates. Accordingly, in this experiment, it was confirmed that the viscosity, flow time, and flow of high-strength grout change according to the volume composition ratio of dolomite aggregate and cement-based material. All experiments were conducted based on the Korean Industrial Standard KS F 4044, and the mixing factor was applied according to the composition ratio of the binder and the filler. In the experiment, the amount of fine powder contained in the dolomite aggregate rather than the silica sand used in the past is grasped, and after mixing with the grout accordingly, the mixture is proceeded to measure the viscosity in an unhardened state. In addition, the flow and flow time of the grout are evaluated according to the viscosity. As a result of the experiment, it was confirmed that the viscosity and flow time decreased and the flow increased as the volume composition ratio of the dolomite aggregate to the cement-based material increased.

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