• Title/Summary/Keyword: Fine Tube

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Microstructure Control of Porous Ceramics by Freeze-Drying of Aqueous Slurry (동결건조공정을 이용한 다공성 세라믹스의 미세구조 제어)

  • 황해진;문지웅
    • Journal of the Korean Ceramic Society
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    • v.41 no.3
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    • pp.229-234
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    • 2004
  • In this study, we proposed new forming process for a porous ceramic body with unique pore structure. h tubular-type porous NiO-YSZ body with radially aligned pore channels was prepared by freeze-drying of aqueous slurry. A NiO-YSZ slurry was poured into the mold, which was designed to control the crystallization direction of the ice, followed by freezing. Thereafter the ice was sublimated at a reduced pressure. SEM observations revealed that the NiO-YSZ porous body showed aligned large pore channels parallel to the ice growth direction, and fine pores are formed around the outer surface of the tube. It was considered that the difference in the ice growth rate during the freezing process resulted in such a characteristic microstructure. Bilayer consisting of dense thin electrolyte film of YSZ onto the tubular type porous body has been successfully fabricated using a slurry-coating process followed by co-firing. It was regarded that the obtained bilayer structure is suitable for constructing electrode-support type electrochemical devices such as solid oxide fuel cells.

The Effect of HEMM on Microstructure and Mechanical Properties of Ti-Nb Alloy for Implant Biomedical Materials (생체의학 임플란트재료로서 Ti-Nb계 합금의 조직과 기계적 성질에 미치는 HEMM의 영향)

  • Woo, Kee-Do;Choi, Gab-Song;Lee, Hyun-Bum;Kim, In-Yong;Zhang, Deliang
    • Korean Journal of Materials Research
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    • v.17 no.11
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    • pp.587-592
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    • 2007
  • Al-42wt%Nb powder was prepared by high-energy mechanical milling(HEMM). The particle size, phase transformation and microstructure of the as-milled powder were investigated by particle size distribution (PSD) analyzer, scanning electron microscopy (SEM), X-ray diffractometery (XRD), transmission electron microscopy (TEM)and differential thermal analysis (DTA). The milled powders were heated to a sintering temperature at 1000C with under vaccum with vaccum tube furnace. Microstructural examination of sintered Ti-42wt%Nb alloy using 4h-milled powder showed Ti-rich phases (${\alpha}$-Ti) which are fine and homogeneously distributed in the matrix (Nb-rich phase: ${\beta}$-Ti). The sintered Ti-42wt%Nb alloy with milled powder showed higher hardness. The microstructure of the as quenched specimens fabricated by sintering using mixed and milled powder almost are same, but the hardness of as quenched specimen fabricated by using mixed powder increased due to solution hardening of Nb in Ti matrix. The aging effect of these specimens on microstructural change and hardening is not prominent.

Development of Evaluation Technique of High Temperature Creep Characteristics by Small Punch-Creep Test Method (ll) - Boiler Header - (Sp-Creep 시험에 의한 고온 크리프 특성 평가 기술 개발(ll) - 보일러 헤더 -)

  • Baek, Seung-Se;Lee, Dong-Hwan;Ha, Jeong-Su;Yu, Hyo-Seon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.1
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    • pp.55-60
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    • 2002
  • For the development of a new creep test technique, the availability of SP-Creep test is discussed for 1Cr-0.5Mo boiler header material. And some results are also compared with those of 2.25Cr- 1Mo steel which widely uses as boiler superheater tube. The results can be summarized as follows. The load exponents(n) obtained by SP-Creep test for 1Cr-0.5Mo steel are decreased with increasing creep temperature and the values are 15.67, 13.89, and 17.13 at 550$^{circ}C$ ,575$^{circ}C$ and 600$^{circ}C$, respectively. The temperature dependence of the load exponent is given by n = 107.19 - 0.1108T. This reason that load exponents show the extensive range of 10∼16 is attributed to the fine carbide such as M$_{23}$C$_{6}$ in lath tempered martensitic structures. At the same creep condition, the secondary creep rate of 1Cr-0.5Mo steel is lower than the 2.25Cr-1Mo steel1 due to the strengthening microstructure composed by normalizing and tempering treatments. Through a SEM observation, it can be summarized that the primary, secondary, and tertiary creep regions of SP-Creep specimen are corresponding to plastic bending, plastic membrane stretching, and plastic instability regions among the deformation behavior of four steps in SP test, respectively.y.

Grain Refining and Age Hardening of Mg-Zn Alloys by Addition of Cu and Si (Cu 및 Si첨가에 의한 Mg-Zn합금계의 입자미세화 및 시효경화)

  • Hwang, Jin-Hwan;Nam, Tae-Hyeon;An, In-Seop;Kim, Yu-Gyeong;Heo, Gyeong-Cheol;Heo, Bo-Yeong
    • Korean Journal of Materials Research
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    • v.5 no.6
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    • pp.682-689
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    • 1995
  • In order to refine the grain size of Mg-Zn alloy 0.5 to 6wt.%Cu or Si elements were added. Alloy ingot was made under vacuum atmosphere of 4 ${\times}$ 10$\^$-4/ Torr in the quartz tube coated by BN. Grain size and hardness were measured after solution treatment for 8 hours at 435$^{\circ}C$. Optimal condition for grain size refining effect was obtained at the minimum composition of 2wt.%Cu or 1.5wt.%Si addition to Mg-6wt%Zn alloy. Age hardening behavior was experimented at the optimal compositions of the Mg-6wt.%Zn, Mg-6wt.% Zn-2wt.%Cu and Mg-6wt.% Zn-1.5wt.%Si. The hardness increment due to fine grain size was higher at the Mg-Zn-Cu alloy system, but that due to age hardening was higher at the Mg-Zn-Si alloy system.

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Efficacy of Fluoroscopy-Guided Cutting Needle Lung Biopsy in Patients with Diffuse Infiltrative Lung Disease (미만성 침윤성 폐질환을 보이는 환자에서 방사선투시유도 절단침 폐생검의 유효성)

  • Choi, Soo-Jeon;Shin, Eun-Ah;Kim, Joung-Sook
    • Tuberculosis and Respiratory Diseases
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    • v.70 no.1
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    • pp.43-50
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    • 2011
  • Background: Open lung biopsy is used for diagnosis of diffuse infiltrative lung diseases (DILD), but it is invasive and relatively expensive procedure. Fluoroscopy-guided cutting needle lung biopsy (FCNLB) has merits of avoidance of admission and rapid diagnosis. But diagnostic accuracy and safety were not well known in the diagnosis of DILD. Methods: We included 52 patients (37 men, 15 women) having DILD on HRCT with dyspnea, except the patients who could be confidently diagnosed with clinical and HRCT findings. FCNLB was performed using 16G Ace cut needle (length 1.5 cm, diameter 2 mm) at the area of most active lesion on HRCT. Final diagnoses were made by the consensus. Results: The mean interval between the HRCT and FCNLB was 4.5 days. Most cases were performed one biopsy during 5~10 minutes. Specific diagnosis was obtained in 43 of 52 biopsies (83%). The most common diagnosis was nonspecific interstitial pneumonia (11 cases) and followed by cryptogenic organizing pneumonia (7 cases), diffuse alveolar hemorrhage and usual interstitial pneumonia (5 cases in each), hypersensitivity pneumonitis (3 cases), tuberculosis and drug induced interstitial pneumonitis (2 cases in each), the others are in one respectively. Mild complication was developed in 9 patients (8 pneumothorax, 1 hemoptysis). Most of complications were regressed without treatment except one case with chest tube insertion for pneumothorax. Conclusion: Fluoroscopy-guided 16 G cutting needle lung biopsy was an useful method for the diagnosis of DILD.

A study of the fresh properties of Recycled ready-mixed soil materials (RRMSM)

  • Huang, Wen-Ling;Wang, Her-Yung;Chen, Jheng-Hung
    • Computers and Concrete
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    • v.17 no.6
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    • pp.787-799
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    • 2016
  • Climate anomalies in recent years, numerous natural disasters caused by landslides and a large amount of entrained sands and stones in Taiwan have created significant disasters and greater difficulties in subsequent reconstruction. How to respond to these problems efficaciously is an important issue. In this study, the sands and stones were doped with recycled materials (waste LCD glass sand, slag powder), and material was mixed for recycled ready-mixed soil. The study is based on security and economic principles, using flowability test to determine the water-binder ratio (W/B=2.4, 2.6, and 2.8), a fixed soil: sand ratio of 6:4 and a soil: sand: glass ratio of 6:2:2 as fine aggregate. Slag (at concentrations of 0%, 20%, and 40%) replaced the cement. The following tests were conducted: flowability, initial setting time, unit weight, drop-weight and compressive strength. The results show that the slump values are 220 -290 mm, the slump flow values are 460 -1030 mm, and the tube flow values are 240-590 mm, all conforming to the objectives of the design. The initial setting times are 945-1695 min. The unit weight deviations are 0.1-0.6%. The three groups of mixtures conform to the specification, being below 7.6 cm in the drop-weight test. In the compressive strength test, the water-binder ratios for 2.4 are optimal ($13.78-17.84kgf/cm^2$). The results show that Recycled ready-mixed soil materials (RRMSM) possesses excellent flowability. The other properties, applied to backfill engineering, can effectively save costs and are conducive to environmental protection.

Bukpo's History and Transition of the Hemp Fabric Production Technique (북포(北布)의 내력과 제섬(製纖) 기술의 변천)

  • Kong, Sang-Hui
    • Korean Journal of Heritage: History & Science
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    • v.50 no.3
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    • pp.44-63
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    • 2017
  • 'Bukpo' is called 'Tongpo' or 'Balnaepo,' which respectively mean hemp fabric that goes into a small bamboo tube and women's table utensil 'bari' in Chosen. It is fine hemp fabric produced in Yukjin, Hamgyeong province. Korea has been divided into North and South since the Korean War in 1950. As it is hard to get information about Northern life style or their traditional technology, their hemp fabric production is also left unknown. This study demonstrates characteristics of the production of 'Bukpo' through "Ojuyeonmunjangjeonsango", the only document that marked about 'Bukpo' making process of the late Chosen dynasty. It aims to analyze the transition of the technique and the meaning by comparing the characteristics of the production of 'Bukpo' with the modern era's documents. In this process, I discovered that the hemp fabric production technique at 19th century shares some sort of similarities with that of Europe or Chinese Miao(hmong). But the hemp fabric production technique changed before the 20th century. The evolution of Northern hemp fabric production technique can be a good example to examine the context of the traditional craft technique.

The Effect of Hot and Cold Water for The Hand Dexterity on Patients with Hemiplegia (냉·온수적용이 편마비환자의 손기민성에 미치는 영향)

  • Hwang, Seong-Soo;Cho, Eun-Sook;Ko, Ji-Young;Jang, Eun-Jung;Joo, Jae-Uk;Son, Jung-Il;Sim, Hee-Jung;Lee, Jong-Hyeon
    • PNF and Movement
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    • v.9 no.1
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    • pp.65-73
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    • 2011
  • Background : This study was to investigate effect of hot and cold water for the hand dexterity. Methods : A total of 37 subjects having hemiplegia(men=6, women=11) and normal(men=10, women=10) were participated in this study. After both hands was soaked in the small tube for 1 minute, we measured 'making dots in circles(BOTMP)', 'lifting small objects(JHFT)', 'disk turning(MMDT)' test. Results : In the case of normal's dominant hand, there were statistically significant differences in all tests after soaked in the hot water but there were statistically significant differences in 'disk turning' test after soaked in the cold water. In the case of hemiplegia's unaffected hand, there were statistically significant differences in 'disk turning' test after soaked in the hot water but there were statistically significant differences in 'making dots in circles', 'disk turning' test after soaked in the cold water. In the case of hemiplegia's affected hand, there were statistically significant differences in 'lifting small objects', 'disk turning' test after soaked in the hot water but there were statistically significant differences in 'making dots in circles', 'disk turning' test after soaked in the cold water. Conclusion : The hot and cold water were affected in the hand dexterity. Especially, in the case of both normal and hemiplegia, there were statistically significant differences in 'disk turning' test after soaked in the cold and hot water. Therefore, We were founded that affected in gross movement than fine movement.

Mechanical and Electrical Properties of Low-Cement Mortar Using a Large Amount of Industrial By-Products (산업부산물을 다량활용한 저시멘트 모르타르의 역학적·전기적 특성)

  • Kim, Young-Min;Im, Geon-Woo;Lim, Chang-Min;Lee, Gun-Cheol
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2023.05a
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    • pp.43-44
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    • 2023
  • This study evaluated the mechanical and electrical properties of low-cement mortar using a large amount of industrial by-products to reduce carbon emissions from the cement industry. As types of industrial by-products, blast furnace slag and fly ash, which are representative materials, were used, and ultra-high fly ash was mixed and evaluated to solve the problem of initial strength loss. In addition, in order to evaluate the electrical properties, 1% of MWCNT was incorporated relative to the powder mass. As experimental items, the compressive strength was measured on the 1st, 3rd, 7th and 28th days of age, and the rate of change in electrical resistance was measured on the 28th day of age. As a result of the experiment, the initial strength of the test specimen mixed with blast furnace slag and fly ash was significantly lower than that of 100% cement, and the specimen mixed with blast furnace slag showed strength equal to that of cement at 28 days of age. As an electrical characteristic, the electrical resistance was reduced when the load was loaded, and this reason is judged to be the effect of improving the conductivity as the connection between CNTs is narrowed by the compressive load.

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Exact Solutions of Plasma Diffusion in a Fine Tube Positive Column Discharge (세관 양광주 방전에서 플라즈마 확산의 완전 해)

  • Jin, D.J.;Jeong, J.M.;Kim, J.H.;Hwang, H.C.;Chung, J.Y.;Cho, Y.H.;Lim, H.K.;Koo, J.H.;Choi, E.H.;Cho, G.S.
    • Journal of the Korean Vacuum Society
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    • v.19 no.1
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    • pp.36-44
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    • 2010
  • The ambipolar diffusion equation has been solved in a fine-tube lamp of a few mm in diameter. In the diffusion of radial direction, the plasma diffuses and vanishes away at the glass wall by recombination with the characteristic time of plasma loss is given by $\tau_r\;=\;(r_0/2.4)^2/D_a$. With the radius $r_0{\sim}1\;mm$ and the ambipolar diffusion coefficient $D_a{\sim}0.01\;m^2/s$, the vanishing time is calculated $\tau_r{\sim}10\;{\mu}s$ which corresponds to the least value of frequency 30 kHz for the sustaining the plasma in the operation of high voltage AC-power. In the diffusion of longitudinal z-direction, a high density plasma generated at the area of a high voltage electrode, diffuses into the positive column with the characteristic time $\tau_z{\sim}0.1\;s$. The plasma diffusion velocity at the boundary of high density plasma is $u_D{\sim}10^2\;m/s$ at the time $t{\sim}10^{-6}$ s and the diffusion velocity becomes slow as $u_D{\sim}1\;m/s$ at $t{\sim}10^{-3}\;s$. Therefore, for the long lamp of 1 m, it takes about several seconds for the high density plasma at the area of electrode to diffuse through the whole positive column space.