• 제목/요약/키워드: Fibrous materials

검색결과 315건 처리시간 0.029초

상압소결 질화알루미늄의 소결 첨가제 변화에 따른 열적 및 기계적 특성 (Effects of Sintering Additives on the Thermal and Mechanical Properties of AlN by Pressureless Sintering)

  • 황진욱;문소윤;남상용;도환수
    • 한국분말재료학회지
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    • 제26권5호
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    • pp.395-404
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    • 2019
  • Aluminum nitride (AlN) has excellent electrical insulation property, high thermal conductivity, and a low thermal expansion coefficient; therefore, it is widely used as a heat sink, heat-conductive filler, and heat dissipation substrate. However, it is well known that the AlN-based materials have disadvantages such as low sinterability and poor mechanical properties. In this study, the effects of addition of various amounts (1-6 wt.%) of sintering additives $Y_2O_3$ and $Sm_2O_3$ on the thermal and mechanical properties of AlN samples pressureless sintered at $1850^{\circ}C$ in an $N_2$ atmosphere for a holding time of 2 h are examined. All AlN samples exhibit relative densities of more than 97%. It showed that the higher thermal conductivity as the $Y_2O_3$ content increased than the $Sm_2O_3$ additive, whereas all AlN samples exhibited higher mechanical properties as $Sm_2O_3$ content increased. The formation of secondary phases by reaction of $Y_2O_3$, $Sm_2O_3$ with oxygen from AlN lattice influenced the thermal and mechanical properties of AlN samples due to the reaction of the oxygen contents in AlN lattice.

Organic Solvent Absorption Characteristics of Split-type Microfiber Fabrics

  • Lee Kwang Ju;Kim Seong Hun;Oh Kyung Wha
    • Fibers and Polymers
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    • 제5권4호
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    • pp.280-288
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    • 2004
  • Split-type nylon/polyester microfiber and polyester microfiber fabrics possess drapeability, softness, bulkiness, and smoothness, so that they can be applied in various industrial fields. In particular, these fabrics are able to absorb various organic solvents, and can be used as clean room materials. To investigate the chemical affinity between solvents and the compositional materials of these fabrics, the contact angle of thermally pressed film fabrics was measured with different solvents. The thermally pressed nylon/polyester fabric films showed a chemical attraction to formamide. The sorption properties of the microfiber fabrics were investigated using a real time testing device, and these tests showed that the sorption behavior was more influenced by the structure of the fibrous assembly than by any chemical attraction. The effect of the fabric density, specific weight, and sample structure on the sorption capacity and rate was examined for various organic solvents. The sorption capacity was influenced by the density and the specific weight of the fibrous assembly, and knitted fabric showed a higher sorption capacity than woven fabric. However, the sorption rate was less affected in lower viscosity solvents. On applying Poiseuille's Law, the lower viscosity solvents showed higher initial sorption rates, and more easily penetrated into the fibrous assembly.

악골 낭종 적출술시 내시경의 이용 (THE USE OF ENDOSCOPY IN ENUCLEATION OF JAW CYSTS)

  • 김영균
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • 제27권1호
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    • pp.61-64
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    • 2001
  • This study evaluated the use of endoscopy to examine jaw cysts during the operation. Fifteen jaw cysts were explored with a endoscope immediately before and after enucleation. Endoscopic findings were evaluated and recorded with video tape. Before enucleation, there were many white fibrous floating materials within the cystic cavity. Cystic lining showed smooth and regular appearance with capillary network. However, there were some fibrous scar tissues and irregular architecture in preoperative infection. After enucleation, there were white shiny bony surfaces with fresh vascular network. In some cases, floating fibrous tissues remained after removal.

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자전연소합성법에 의한 여러 가지 섬유상 및 입상 탄화물의 제조 (Fabrication of Various Carbides with Fibrous and Particulate Shapes by Self-Propagating High Temperature Synthesis Method)

  • 방환철;윤존도
    • 한국재료학회지
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    • 제10권5호
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    • pp.343-349
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    • 2000
  • 자전연소합성(SHS)법을 이용하여 탄소섬유와 티타늄, 지르코늄, 니오븀, 규소, 붕소, 중석, 몰리브덴의 분말로부터 여러 가지 섬유상 탄화물의 합성을 시도하였다. 티타늄과 지르코늄은 예열없이, 그 이외의 경우는 전기로 또는 화학로를 사용하여 예열하여 반응을일으킨 결과, TiC, ZrC, NbC, SiC, $B_4$C, WC,$ Mo_2$C 의 순수한 탄화물의 형성되었다. TiC, ZrC, NbC 및 $B_4$C 탄화물의 형상은 속의 빈 섬유상이었고, SiC는 보다 작은 입자와 미세 휘스커로 이루어진 섬유상을 하고 있었고 WC와 $Mo_2$C 는 비섬유상을 하고 있었다. 여러 가지 형상의 원인에 대하여 합리적 설명을 시도하였으며 정성적 메카니즘을 제안하였다.

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무기 필러가 첨가된 현무암섬유 강화 에폭시 복합재료의 난연 특성 (Flame Retardant Properties of Basalt Fiber Reinforced Epoxy Composite with Inorganic Fillers)

  • 문소윤;이수연;임형미
    • Composites Research
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    • 제32권6호
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    • pp.368-374
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    • 2019
  • 무기필러가 첨가된 현무암섬유 강화 에폭시 복합재료를 제조하여 그 특성을 평가하였다. 첨가된 무기필러는 각각 수산화마그네슘, 수산화알루미늄, 알루미나, 베마이트이며 이를 첨가제로한 에폭시 수지를 현무암섬유에 핸드레이업으로 함침시킨 후 hot pressing하여 수지 함침량이 30 wt%인 섬유복합재료를 제조하였다. LOI 평가 결과 BFRP의 LOI (28.9)는 에폭시 수지 (21.4)에 비해 향상된 것을 확인하였으며 무기필러가 첨가될 경우 그보다 더욱 향상되는 것을 확인하였다. 또한 무기필러가 첨가된 복합재료는 무기필러가 첨가되지 않은 복합재료에 비해 콘칼로리미터 시험에서 PHRR, THR, TSR 등이 감소하여 무기필러 첨가에 따른 난연 특성 향상을 확인하였다.

폴리카보실란 전구체의 용매 처리에 따른 열적 및 유변학적 특성 분석 (Thermal and Rheological Characterizations of Polycarbosilane Precursor by Solvent Treatment)

  • 송예은;주영준;신동근;조광연;이두진
    • Composites Research
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    • 제35권1호
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    • pp.23-30
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    • 2022
  • 폴리카보실란은 탄화규소 섬유 방사와 세라믹 제조를 위해 필요한 중요한 전구체이며, 이 전구체는 제조방법 및 공정에 따라 고내열성 및 내산화성 및 연속적인 탄화규소 섬유 생산 능력이 달라진다. 탄화규소 섬유는 폴리카보실란의 합성, 정제 및 분자구조제어기술, 그리고 이를 이용한 용융방사 및 안정화, 열처리 공정을 통해 제조된다. 본 논문에서는 폴리카보실란 전구체를 다양한 용매처리를 통하여 전구체 내에 존재하는 미반응물 및 저분자량의 정제효과를 파악하였으며, 또한 다양한 온도에서의 열처리에 따른 폴리카보실란 전구체의 중합 및 네트워크 재배열에 의한 변화에 대해 열적 분석을 실시하였다. 특히, 폴리카보실란 전구체의 유변물성 특성을 통해 용매처리 및 열처리에 따른 복합점도 및 구조적 배열의 변화를 분석하였다.