• Title/Summary/Keyword: Fiber Composition

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Thermogravimetric Analysis of Rice Husk Flour for a New Raw Material of Lignocellulosic Fiber-Thermoplastic Polymer Composites

  • Kim, Hyun-Joong;Eom, Young-Guen
    • Journal of the Korean Wood Science and Technology
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    • v.29 no.3
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    • pp.59-67
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    • 2001
  • Rice husk flours were analyzed by chemical composition and thermogravimetric methods in nitrogen atmosphere to discuss its feasibility as a raw material for manufacturing agricultural lignocellulosic fiber-thermoplastic polymer composite. It was revealed in the chemical composition analysis that rice husk flour was composed of moisture, 5.0%; lignin, 21.6%; holocellulose, 60.8%; ash, 12.6%. In the thermogravimetric analysis (TGA), thermal decomposition behavior of rice husk flour from room temperature to $350^{\circ}C$ was similar to that of wood flour, but rice husk flour was more thermally stable from 350 to $800^{\circ}C$ than wood flour because of higher silica content in the rice husk flour and smaller particle size of rice husk flour. The activation energy of thermal decomposition was evaluated using Flynn & Wall expression. As the thermal decomposition proceeded in rice husk flour, the activation energy of thermal decomposition appeared almost constant up to ${\alpha}=0.25$, but thereafter increased. Activation energy of thermal decomposition in wood flour, however, decreased steeply up to ${\alpha}=0.3$, but thereafter remained almost constant. From the results, rice husk flour was thought be a substitute for wood flour in manufacturing agricultural lignocellulosic fiber-thermoplastic polymer composite in the aspect of thermal decomposition.

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Effect of Pulp Type and Fines Content in a Stock on the Polyelectrolyte Multilayering onto Pulp Fiber (펄프 종류와 지료 내 미세분 함량이 고분자전해질 multilayering에 미치는 영향)

  • Chin, Seong-Min;Ryu, Jae-Ho;Lee, Sung-Rin;Youn, Hye-Jung
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.40 no.3
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    • pp.15-22
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    • 2008
  • Properties of pulp fibers can be modified by LbL multilayering technology. We evaluated the effect of stock composition on the polyelectrolyte multilayering performance of pulp fibers in this study. Stock composition was varied with pulp type and fines content. Three types of pulp-Hw-BKP, BCTMP and KOCC-were treated with polyelectrolytes of poly-DADMAC and PSS. Fines content of stock were controlled at 0, 10, 20, 30, and 40%. Zeta potential of pulp fibers and charge demand of filtrate were evaluated. The highest adsorption ratio was obtained for BCTMP because of its shortest fiber length and highest specific surface area. Higher fines content in the stock increased the adsorption ratio of polyelectrolyte onto pulp fiber and it required a higher amount of polyelectrolyte for charge neutralization. For the pulp stock with higher fines content, a higher level of polyelectrolyte and the increased layer number were required to modify and stabilize the electrochemical properties of pulp fibers.

Comparative Anatomy of Diffuse-Porous Woods Grown in Korea(II) -Characteristics by Habit and Phenology- (한국산(韓國産) 산공재(散孔材)의 해부학적(解剖學的) 특성(特性)에 관한 비교연구(比較硏究)(II) -Habit과 Phenology에 따른 특성(特性)-)

  • Chung, Youn-Jib;Lee, Phil-Woo
    • Journal of the Korean Wood Science and Technology
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    • v.24 no.1
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    • pp.1-10
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    • 1996
  • The frequency distribution diagrams of Korean diffuse-porous woods, 36 families, 75 genera, 145 species, 215 specimens in relation to habit and phenology were analyzed. As the habit character changes from shrub to tree, such quantitative features as vessel frequency, percentage of solitary vessels, length/diameter(L/D) ratio of vessel element decreased but tangential vessel diameter, fiber length/vessel element length(F/V) ratio increased. Qualitative features such as helical vessel wall thickening, diffuse distribution of longitudinal parenchyma, heterogeneous ray composition decreased, while alternate intervessel pits, libriform wood fiber, simple perforations increase. As the phenology character changes from evergreen to deciduous species, such quantitative features as percentage of solitary vessels, vessel element length and L/D ratio decreased but tangential vessel diameter, F/V ratio increased. Diffuse distribution of longitudinal parenchyma, heterogeneous ray composition, and crystals in qualitative features decreased, while alternate intervessel pits, libriform wood fiber, simple perforation of vessel element, ray width and ray height increased.

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The Effect of Electron Beam Irradiation on Chemical and Morphological Properties of Hansan Ramie Fibers

  • Lee, Jung Soon
    • Fashion & Textile Research Journal
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    • v.15 no.3
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    • pp.430-436
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    • 2013
  • The purpose of this study investigates the effects of electron beam(EB) irradiation on the chemical and morphological properties of Hansan ramie fiber. Hansan ramie fibers were irradiated with electron beam doses of 0, 1, 3, 5 and 10kGy. The effect of electron beam irradiation on the chemical components of fibers as well as the surface chemical and morphological properties were investigated using chemical component analysis methods based on TAPPI standards, XPS, and SEM. The results indicate that the surface layers can be removed under suitable EB irradiation doses. Alcohol-benzene extraction and lignin content increases gradually with an increase in EB irradiation and reaching a maximum at an EB dose of 3kGy, and decreases at 10kGy. The surface chemical changes measured by XPS corresponded to the chemical composition analysis results. The C1 peak and the O/C ratio decreased with the removal of the multi-layer and primary layer by EB irradiation. The SEM images show the inter-fibrillar structure etched by EB irradiation up to 5kGy. At 10kGy, the surface structure of the ramie fiber shows highly aligned and distinctive striations in a longitudinal direction. The removal of these exterior layers of the fiber was confirmed by changes in surface morphology as observed in SEM images.

Wear of the Alumina Short Fiber Reinforced Tin-Bronze Matrix Composites at the Room Temperature and an Elevated Temperature (알루미나 단섬유 보강 청동기지 복합재의 상온 및 고온 마모)

  • 최준호;허무영
    • Tribology and Lubricants
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    • v.11 no.4
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    • pp.45-52
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    • 1995
  • The wear behavior of alumina short fiber reinforced tin-bronze matrix composites was studied at the room temperature and an elevated temperature. The effect of the composition of specimens and the variation of wear conditions on the wear properties was examined by a pin-on-disc type wear testing machine. The wear mechanism according to the compositon of specimens at various wear conditions was discussed by the observation of the microstructure and the analysis of the composition on the worn surfaces. A thicker oxide layer on worn surfaces led to a lower wear loss because of the lubricating effect of oxide layers between pin and disc. As the testing temperature was raised to 350$^{\circ}$C, the fiber reinforced composites exibited markedly increased wear resistance even at a higher applied load since the reinforcement of composites with alumina fibers was not affected to a large extent by raising temperature. The results obtained by AES and EDS analysis indicated that the oxide layer of the worn surfaces formed at 350$^{\circ}$C was proved as Fe-oxide. This was explained by the faster formation of Fe-oxide than Cu-oxide at 350$^{\circ}$C.

Cooling Speed Effects of Fluoride Glasses (불화 유리의 냉각 속도 효과)

  • 류선윤
    • Journal of the Korean Ceramic Society
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    • v.32 no.2
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    • pp.183-188
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    • 1995
  • The properties of the glasses are not dominantly dependent on the chemical composition, temperature, and pressure but also on the thermal history. For example, electrical, thermal, optical, and mechanical properties are all known to be strongly dependent on the thermal history. Fluoride glasses have received a great deal of attention as candidate materials for an infra-red transmitting medium. A series of fluoride glasses and fibers were prepared under a nitrogen atmosphere. Thermal history effects of the fluoride glass fibers associated with the fast cooling rate employed during the fiber drawing process were discussed in terms of the glass temperatures and the fictive temperatures on the basis of the results obtained from the Differential Scanning Calorimeter (DSC) measurements of the fiber and bulk forms of the same chemical composition.

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Edible Basis and Ingredient Analysis of Song-gi Used for Pyeon of Jong-ga Ancestral Ritual Food (종가 제례음식 편(䭏)에 사용하는 송기(松肌)의 식용 근거와 성분 분석)

  • Lee, Chang-Hyeon;Kim, Young;Kang, Min-Sook;Lee, Young-Eun
    • Journal of the Korean Society of Food Culture
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    • v.32 no.4
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    • pp.311-322
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    • 2017
  • This study examined the traditional edible basis and ingredients of Song-gi used for Pyeon of Jong-ga ancestral ritual food. Through an investigation of references, a case study, and ingredient analysis for traditional edible basis of Song-gi, the nutritional value and availability as food material were reviewed. Among the 4 kinds of pine trees from 4,705 types of edible materials usable as food listed in the ${\ll}$Korea Food Standards Codex${\gg}$, 'Pinus radiata D. Don', in which the husk is acknowledged as an edible food, was applied in this study. This study processed the Song-gi following the method of jong-ga and divided into pine inner bark (PIB) and pine inner bark powder (PIBP) to analyze the general composition and dietary fiber. The main composition of PIB was carbohydrate, in which the content was 88.7% per 100 g. The content of dietary fiber was 73.7% per 100 g and the insoluble dietary fiber reached 92.3% in total dietary fiber. In conclusion, the edibility of Song-gi, which has a considerable amount of insoluble dietary fiber caused constipation because it absorbed the moisture in the intestine due to the lack of nutrients but may be developed as a functional food that helps the digestive activation of the intestine and improve the health of the intestine if taken with balanced nutrition.

Analyses of Fatty Acids and Dietary Fiber in Soy Sprouts (콩나물의 지방산 및 식이섬유 함량 분석)

  • Kim, Sea-Young;Lee, Kyong-Ae;Yun, Hong-Tae;Kim, Jeong-Tae;Kim, Uk-Han;Kim, Yong-Ho
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.56 no.1
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    • pp.29-34
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    • 2011
  • Soy sprout is a traditional food in Korea. It has been a source of protein, lipid and vitamin etc. as cooked and fresh vegetable supplying throughout the year. Soy sprouts of five soybean cultivars were analyzed fatty acid composition and dietary fiber contents. The compositional analysis confirmed that soy sprout contained five major fatty acids(16:0 palmitic, 18:0 stearic, 18:1 oleic, 18:2 linoleic and 18:3 linolenic). Fatty acid levels in soy sprout were not significant statistically between fresh and boiled soy sprout, the result support a conclusion that boiling treatment could not affect the fatty acid composition in soy sprouts. Fatty acid levels in whole and cotyledon part of soy sprout were not changed during sprout production, whereas the content in hypocotyl increased by approximately 13.2% of total unsaturated fatty acid compared to whole soy sprout. In case of dietary fiber, boiled soy sprouts showed higher contents than in fresh soy sprouts. These changes were associated with an increase in the mean level of insoluble dietary fiber expecially. Fatty acid levels and dietary fiber contents varied with soybean cultivars suggesting chemical composition of soybean seed was important to soy sprout characters.

A Quality Comparison of Traditional Korean Papers: Mixtures of Bast-Fiber with Straw pulp(Rice straw paper) in Different Composition Ratio (고정(藁精) 혼합비율에 따른 한지의 물성 비교)

  • Jung, Sun-Young
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.39 no.1 s.119
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    • pp.48-55
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    • 2007
  • The aim of this article is to review the general property of the famous traditional Korean paper, "rice straw paper"(Bast-Fiber mixed with straw pulp), and to compare the paper qualities varying with the composition ratio of straw pulp, in order to revive the traditional paper in modem Korea. The experiment was carried out by making first the two different mixture papers, i. e., one is the paper of 50% bast fiber mixed with 50% straw pulp, and the other is the paper of 75% bast fiber with 25% oats straw pulp, and finally the 100% bast fiber paper was made for the purpose of comparison. The qualitative properties of these three kinds of paper with the different mixing ratio of the straw pulp were evaluated, and the findings of the experiment can be summarized as follow: 1. As to the quality aspects of the paper strength like tensile strength, breaking length, elongation, and tear strength, the test proved the 100% bast fiber paper as best, and the 50% mixed paper as the next good one. 2. In aspect of the printing adaptability such as density, opacity, brightness, whiteness, lab colors, air permeability, and roughness, the 50% mixed paper proved to be the best, due to the short cells in the straw pulp. 3. As to the air permeability, the larger ratio of straw pulp was found to be the lesser, and 75% bast fiber with 25% straw pulp mixture paper and the 100% bast fiber one were found 1/5 degree efficient. 4. In terms of the water absorption degree, 100% bast fiber paper was the fastest, but in case of mixture paper, 50% mixed one was a little faster up to the point of 1cm, while the two kinds of mixed ones appear to be almost similar to each other beyond the point. 5. The straw pulp mixed paper, especially the 50% mixed one was evaluated as the highest by the calligraphers who had experienced using the papers in terms of movement and feeling of the caligraphy and painting. In addition, although the 25% mixed paper is judged to be good for book printing because of the strength, the 50% mixed paper can be thought to be more desirable for painting and calligraphy. In conclusion, we will be able to make the quality paper with durability, by mixing the straw pulp with the bast fiber in proper ratio, following the tradition of Korean paper making.

Characterization of Reinforcing Efficiency in Hybrid Fiber Reinforced Cementitous pastes (하이브리드 섬유보강 시멘트 페이스트의 보강효율에 대한 특성화)

  • Park, Tae-Hyo;Noh, Myung-Hyun;Park, Choon-Keun
    • Proceedings of the Korea Concrete Institute Conference
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    • 2004.05a
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    • pp.644-647
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    • 2004
  • Modulus of rupture (MOR) and flexural toughness in hybrid fiber reinforced cement pastes mixed with micro-fiber (carbon fiber) and macro-fiber (steel fiber) and replaced with silica fume according to the fixed ratio were researched. Reinforcing efficiency in specimens were estimated by two factors, such as strengthening factor $(F_s)$ and toughening factor $(F_t)$, which were calculated from the analysis of variance (ANOVA) of the response values, such as MOR and absorbtion energy $(W_0)$. According to the experimental design by the fractional orthogonal array, nine hybrid fibrous reinforced paste series and one non-reinforced control paste were manufactured. Specimens of each series were tested by the INSTRON Inc. 8502(model) equipment in three-points bending and then measured the load-deflection response relationships. Considerable strengthening of cement pastes resulted in' the case of other factors without carbon fiber and toughening of cement pastes about all factors showed high. Based on the significance of factors related to response values from ANOVA, following assessments were available; $F_s$ or MOR: silica fume $\gg$ steel fiber $\gg$ carbon fiber; $F_t\;or\;W_0$: steel fiber > carbon fiber > silica fume. Optimized composition condition was estimated by steel fiber of $1.5\%$, carbon fiber of $0.5\%$ and silica fume $7.5\%$ in side of strengthening and steel fiber of $1.5\%$, carbon fiber of $0.75\%$ and silica fume $7.5\%$ in side of toughening.

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