• Journal of Korea Foundry Society
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• v.15 no.3
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• pp.242-251
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• 1995

Highly alloyed high speed tool steels(ASP steels) were rapidly solidified by melt spinning process, and the microstructures of melt spun tool steel ribbons were examined by optical microscopy and transmission electron microscopy with energy dispersive x-ray spectroscope. The microstructure of melt spun tool steel ribbon was found to be consisted of ${\delta}-ferrite$ cells surrounded by austenite and V-rich MC carbides. The size of ${\delta}-ferrite$ cells and intercellular MC carbides were about $0.4{\mu}m$ or less and 30nm or less, respectively. From the melt spun tool steel ribbons, only the MC type carbide phase was observed, instead of $M_2C$, $M_{23}C_6$ and $M_6C$ carbides which were generally observed in other rapidly solidified high speed steels. Such a change in type of carbide phase formed could be attributed to the increase in alloying content of vanadium and carbon. However, changes in microsturcture of melt spun tool steels with alloying content of cobalt, vanadium and carbon were not observed.

• Journal of Magnetics
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• v.22 no.2
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• pp.188-195
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• 2017

The ferromagnetic resonance and other magnetic properties dependence on $Ni^{2+}/Fe^{3+}$ ratio and crystallite size were investigated for nano nickel ferrite ($NiFe_2O_4$). The crystallite size was controlled by controlling the nickel content in the starting material solution. The XRD and TEM were utilized to measure the crystallite size through Scherrer formula and particle size respectively. The most frequent particle sizes were lower than crystallite size, which ranged from 16.5 to 44.65 nm. The general behavior of M-H loop shapes and parameters showed superparamagnetic one. The saturation magnetization had a maximum value at $Ni^{2+}/Fe^{3+}$ molar ratio equal to 0.186. The FMR signals showed, generally, broad linewidths, where the maximum width and minimum resonance field were for the sample of the lowest crystalline size. Furthermore, FMR resonance field shows linear dependence on crystalline size. The fitting relation was estimated to express this linear dependency on the base of behavior coincidence between particle size and the inverse of saturation magnetization. The given interpretations to understand the intercept and the slope meanings of the fitted relation were based on Larmor equation, and inhomogeneous in the anisotropy constant.

• Journal of Korea Foundry Society
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• v.13 no.2
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• pp.175-186
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• 1993

In this study, the effect of Mo addition on the microstructure and mechanical properties of ductile cast iron have been investigated. The amounts of Mo and the thickness of specimen have been varied from 0 to 4.79wt% and 13mm, 10mm and 6mm, respectively. As the casting thickness decreases, the average size of spheroidal graphite is decreased and the hardness increases. By increasing the Mo content, the tensile strength of ferrite and pearlite matrix increases and shows maximum which is about $30{\sim}40%$ higher than ordinary ductile cast iron. After the maximum, adding more Mo results in gradual transformation of ferrite and pearlite to bainite and thus tensile strength decreases again. The elongation decreases continueously with Mo content. The addition of Mo about $0.5{\sim}1.0wt%$ improves the wear resistance and tensile strength of thin ductile cast iron.

• Journal of the Korean Ceramic Society
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• v.16 no.1
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• pp.3-12
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• 1979

The effects of sintering temperature and sintering atmosphere on magnetic properties and microstructuresof Mn-Zn ferrites have been studied. Mixture of 52.8mole% $Fe_2O_3$, 26.4mole% MnO, 15.1mole0% ZnO and 5.7mole% NiO was prepared, and 0.1mole% CaO, 0.02mole% $SiO_2$ were added as minor additives. After calcining and ball milling the powder was granulated for compacting. The specimens were sintered at $1, 250^{\circ}$, $1, 300^{\circ}$and 1, 35$0^{\circ}C$ in the various atmosphere of $N_2$, $N^_2\DIV0.6% O_2$, $N_2＋2.7% O_2$, $N_2＋4.1% O_2$, $N^2＋8.2% O_2$ and air for 3 hours and cooled in $N_2$ atmosphere. The grian growth rate and densities increase as sintering temperature and oxygen content of atmosphere increase. At the sintering temperature of $1, 250^{\circ}C$ the initial permeabilities increase as oxygen content of atmosphere increase. At the sintering temperature of$ 1, 300^{\circ}$and $1, 350^{\circ}$ the initial permeabilities show maximum values at $N_2＋4.1% O_2$ atmosphere. The secondary peaks of initial permeabilities are observed between 100$^{\circ}$and 20$0^{\circ}C$, and the positions of secondary peaks move to higher temperature as oxygen content of atmosphere increases. Q-factors decrease as sintering temperature increases and oxygen content of atmosphere decreases.

• Journal of the Korean Magnetics Society
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• v.5 no.1
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• pp.15-20
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• 1995

We have prepared 20 kinds of Mn-Zn ferrites as content of CaO(0.1 mol%), NiO(0.0~0.60 mol%) and CoO(0.0~0.8 mol%) adding by the coprecipitation method and studied the magnetic properties as content of CaO, NiO and CoO adding. Initial permeability decrease as the content of NiO and CoO adding increases, while Curie tem~ perature increase as the content of NiO and CoO adding increases. $(H_{c})$, $(B_{s})$ and $(W_{h})$ increase as content of NiO adding increases.

• International Journal of Korean Welding Society
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• v.3 no.1
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• pp.23-28
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• 2003

The effect of the welding speeds on the weld bead shape, microstructure, and mechanical properties in type 304 austenitic stainless steels was investigated by microscopic test, Erichsen test and tensile test. In this study welds were produced using autogeneous Direct Current Straight Polarity (DCSP) and pulsed current GTA welding. This study shows the ferrite content, ductility, tensile strength and elongation of high speed welds are decreased with increasing welding speed. The high speed welds exhibits satisfactory tensile strength, though the ductility is not good as that of the base metal.

• Proceedings of the KIEE Conference
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• 1999.11a
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• pp.4-6
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• 1999

We have performed spin-spray ferrite plating of $Fe_{3-x}Zn_xO_4$($X=0.47{\sim}0.97$) films in the temperature region T=85[$^{\circ}C$]. A reaction solution and an oxidizing solution were supplied to a reaction chamber by supply pumps. The Zn composition X in the $Fe_{3-x}Zn_xO_4$ Film increases as the content of $ZnCl_2$ increase, from X=0.47 at O.05[g/l] to X=0.97 at 0.15[g/l]. All the films are polycrystalline with no preferential orientation, and the magnetization exhibits no definite anisotropy. Grain size in the films increases as X increases, reaching 0.98[${\mu}m$] at X=0.97.

• Journal of Welding and Joining
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• v.17 no.5
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• pp.89-96
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• 1999

The base metal and weld metal of alloy designed austenitic stainless steels were electrochemically tested in artificial sea water. Pitting resistance of 14 different stainless steels was evaluated by measuring pitting potential. The effect of alloy element to pitting potential was evaluated by changing chromium, nickel, sulfur content. The site of pitting initiation was observed by optical microscope. As a result of electrochemical test, pitting resistance of weld metal was higher than base metal, and rapidly cooled weld metal has higher pitting potential than slowly cooled weld metal. In case of primary δ-ferrite solidification, pitting potential was increased, but residual δ-ferrite was detrimental to pitting resistance. Chromium was more effective to pitting resistance than nickel, and sulfur was very detrimental element to pitting resistance.

• Nuclear Engineering and Technology
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• v.36 no.3
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• pp.237-247
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• 2004

To investigate the applicability of automated ball indentation (ABI) tests in the evaluation of the tensile properties of cast stainless steel (CSS), ABI tests were performed on four types of unaged CSS and on 316 stainless steel, all of which had a different microstructure and strength. The reliability of ABI test data was analyzed by evaluating the data scattering of the ABI test and by comparing tensile properties obtained from the ABI test and the tensile test. The results show that the degree of scattering of the ABI test data is reasonably acceptable in comparison with that of standard tensile data, when two points data that exhibit out-of-trend are excluded from five to seven points data tested on a specimen. In addition, the scattering decreases slightly as the content of ${\delta}-ferrite$ in CSS increases. Moreover, the ABI test can directly measure the flow parameters of CSS with error bounds of about ${\pm}10\%$ for the ultimate tensile stress and the strength coefficient, and about ${\pm}15\%$ for the yield stress and the strain hardening exponent. The accuracy of the ABI test data is independent of the amount of ${\delta}-ferrite$ in the CSS.

• Transactions of Materials Processing
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• v.12 no.4
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• pp.284-289
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• 2003

The effects of nitrogen on the deformation behavior of duplex stainless steel have been studied. The variation of strength was correlated with the characteristic microstructures pertaining to nitrogen. Analysis based on Hall-fetch relation confirmed that nitrogen enhances phase-boundary strengthening effect. The evolution of dislocation structure, slip traces and misorientation distribution during deformation were also characterized to elucidate the effect of nitrogen on inelastic deformation mechanism. It has been verified in this study that the higher nitrogen content provides a dual-phase microstructure with smaller strength difference between austenite and ferrite resulting into the earlier transfer of inelastic deformation from austenite to ferrite.