• 제목/요약/키워드: Fe-based

검색결과 2,890건 처리시간 0.028초

Al-Fe 레이저 오버레이층 경계면에서의 금속간화합물 거동 (Intermetallic Compounds Behavior at Laser Overlay Interface of Aluminum and Fe-based Powder)

  • 강남현;유연곤;이창우;김정한
    • Journal of Welding and Joining
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    • 제25권3호
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    • pp.51-56
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    • 2007
  • A $CO_2$ laser overlay was conducted by using a Fe-based powder on the AC2B aluminum substrate. Cracks and intermetallic compounds (IMC) were observed inconsistently along the interface between the overlay and post-molten layer. A scanning electron microscopy (SEM) with energy dispersive spectroscopy (EDS) detected some Fe-rich IMC ($Fe_3Al$, FeAl) as well as the brittle Al-rich IMC ($Fe_2Al_5,\;FeAl_3$). Micro vickers hardness proved the formation of Al-rich IMC ($FeAl_3$) along the interface by showing HV0.1 $800{\sim}900$. Furthermore, nano indentation was successfully applied to investigate the behavior of IMC more precisely than the micro vickers hardness.

A New Fe (III)-Selective Membrane Electrode Based on Fe (II) Phthalocyanine

  • Ozer, Tugba;Isildak, Ibrahim
    • Journal of Electrochemical Science and Technology
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    • 제10권3호
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    • pp.321-328
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    • 2019
  • A new miniaturized all solid-state contact Fe (III)-selective PVC membrane electrode based on Fe (II) phthalocyanine as a neutral carrier was described. The effects of the membrane composition and foreign ions on the electrode performance was investigated. The best performance was obtained with a membrane containing 32% poly (vinyl chloride), 64% dioctylsebacate, 3% Fe (II) phthalocyanine, and 1% potassium tetrakis (p-chlorophenyl) borate. The electrode showed near Nernstian response of $26.04{\pm}0.95mV/decade$ over the wide linear concentration range $1.0{\times}10^{-6}$ to $1.0{\times}10^{-1}M$, and a very low limit of detection $1.8{\pm}0.5{\times}10^{-7}M$. The potentiometric response of the developed electrode was independent at pH 3.5-5.7. The lifetime of the electrode was approximately 3 months and the response time was very short (< 7 s). It exhibited excellent selectivity towards Fe (III) over various cations. The miniaturized all solid-state contact Fe (III)-selective membrane electrode was successfully applied as an indicator electrode for the potentiometric titration of $1.0{\times}10^{-3}M$ Fe (III) ions with a $1.0{\times}10^{-2}M$ EDTA and the direct determination of Fe (III) ions in real water samples.

NiFe/FeMn/NiFe 스핀밸브 구조의 다층박막에서 상 하부 NiFe 두께에 따른 교환바이어스 조사 (Anomalous Exchange Bias of the Top and Bottom NiFe Layers in NiFe/FeMn/NiFe Based Spin Valve Multilayers)

  • S.M. Yoon;J.J. Lim;V.K. Sankar;Kim, C.G.;Kim, C.O.
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2003년도 추계학술발표강연 및 논문개요집
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    • pp.212-212
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    • 2003
  • Many of the spin valve multilayer structures with FeMn as antiferromagnetic layer consist of a NiFe/FeMn/NiFe trilayer where the bottom NiFe layer is the seed layer to facilitate the growth of (111) gama-FeMn antiferromagnetic phase and the top NiFe layer forms the pinned layer[1], In this study, exchange bias of bottom NiFe layer has been investigated as functions of thicknesses of top and bottom NiFe in NiFe/FeMn/NiFe, prepared by rf magnetron sputtering, MH-loop was measured by vibration sample magnetometer (VSM). Two hysteresis loops are corresponded to bottom and top layers, similar to reported loops in spin valve structure. Exchange bias of bottom NiFe could be induced by the interfacial coupling between bottom NiFe and FeMn. But those coupling are strongly dependent on the top and bottom NiFe thicknesses, revealing anomalous character ul exchange bias of bottom NiFe layer.

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Dynamic Magnetostriction Characteristics of an Fe-Based Nanocrystalline FeCuNbSiB Alloy

  • Chen, Lei;Li, Ping;Wen, Yumei
    • Journal of Magnetics
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    • 제16권3호
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    • pp.211-215
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    • 2011
  • The dynamic magnetostriction characteristics of an Fe-based nanocrystalline FeCuNbSiB alloy are investigated as a function of the dc bias magnetic field. The experimental results show that the piezomagnetic coefficient of FeCuNbSiB is about 2.1 times higher than that of Terfenol-D at the low dc magnetic bias $H_{dc}$ = 46 Oe. Moreover, FeCuNbSiB has a large resonant dynamic strain coefficient at quite low Hdc due to a high mechanical quality factor, which is 3-5 times greater than that of Terfenol-D at the same low $H_{dc}$. Based on such magnetostriction characteristics, we fabricate a new type of transducer with FeCuNbSiB/PZT-8/FeCuNbSiB. Its maximum resonant magnetoelectric voltage coefficient achieves ~10 V/Oe. The ME output power reaches 331.8 ${\mu}W$ at an optimum load resistance of 7 $k{\Omega}$ under 0.4 Oe ac magnetic field, which is 50 times higher than that of the previous ultrasonic-horn-substrate composite transducer and it decreases the size by nearly 86%. The performance indicate that the FeCuNbSiB/PZT-8/FeCuNbSiB transducer is promising for application in highly efficient magnetoelectric energy conversion.

유한요소해석(FEA)에서의 Error-estimation에 관한 연구

  • 박종권;김동권;성활경
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 1995년도 춘계학술대회 논문집
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    • pp.603-607
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    • 1995
  • Static and dynamic response of a mechanical system can be easily and readily obtained using an approximate method such as the Finite Element Method. However, FE solution cannot be totally trusted, since there are many numerical uncertainies inherent in an FE analysis. FE solution error can be estimated based on FE analysis result. Error estimator shows the quality of the FE solution, and helps FE users to enhance the accuracy of the FE solution.

Direct frequency domain analysis of concrete arch dams based on FE-(FE-HE)-BE technique

  • Lotfi, Vahid
    • Computers and Concrete
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    • 제1권3호
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    • pp.285-302
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    • 2004
  • A FE-(FE-HE)-BE procedure is presented for dynamic analysis of concrete arch dams. In this technique, dam body is discretized by solid finite elements, while the reservoir domain is considered by a combination of fluid finite elements and a three-dimensional fluid hyper-element. Furthermore, foundation rock domain is handled by three-dimensional boundary element formulation. Based on this method, a previously developed program is modified, and the response of Morrow Point arch dam is studied for various conditions. Moreover, the effects of canyon shape on response of dam, is also discussed.

플라즈마 아크 방전법에 의한 Zr계 나노분말 제조 (Synthesis of Zirconium-Based Nanopowder by the Plasma Arc Discharge Process)

  • 이길근;김경주;박제신
    • 한국분말재료학회지
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    • 제14권1호
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    • pp.63-69
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    • 2007
  • The present study was focused on the synthesis of a zirconium-based alloyed nanopowder by the plasma arc discharge process. The chemical composition, phase structure, particle size and hydrogen sorption property of the synthesized powders under various synthesis conditions were analyzed using XRF, XRD, SEM, XPS and the ASTM-F798 method. The chemical composition of the synthesized Zr-V-Fe-based powders approached that of the raw material with an increasing hydrogen fraction in the powder synthesis atmosphere. The synthesized $Zr_{55}V_{29}Fe_{16}$ powder consist of a mixed phase structure of the $Zr,\;ZrH_2,\;FeV\;and\;Zr(V_{1-x}Fe_{x})_2$ phases. This powder has an average particle size of about 20 nm. The synthesized $Zr_{55}V_{29}Fe_{16}$ nanopowder showed getter characteristics, even though it had a lower hydrogen sorption speed than the $Zr_{57}\;V{36}\;Fe_7$ getter powder. However, the synthesized Zr nanopowder with an average particle size of 20 nm showed higher hydrogen sorption speed than the $Zr_{57}\;V{36}\;Fe_7$ getter powder.

최적화 기법을 이용한 로터 축 유한요소모델 개선 (FE MODEL UPDATING OF ROTOR SHAFT USING OPTIMIZATION TECHNIQUES)

  • Kim, Yong-Han;Feng, Fu-Zhou;Yang, Bo-Suk
    • 한국소음진동공학회:학술대회논문집
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    • 한국소음진동공학회 2003년도 추계학술대회논문집
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    • pp.104-108
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    • 2003
  • Finite element (FE) model updating is a procedure to minimize the differences between analytical and experimental results, which can be usually posed as an optimization problem. This paper aims to introduce a hybrid optimization algorithm (GA-SA), which consists of a Genetic algorithm (GA) stage and an Adaptive Simulated Annealing (ASA) stage, to FE model updating for a shrunk shaft. A good agreement of the first four natural frequencies has been achieved obtained from GASA based updated model (FEgasa) and experiment. In order to prove the validity of GA-SA, comparisons of natural frequencies obtained from the initial FE model (FEinit), GA based updated model (FEga) and ASA based updated model (FEasa) are carried out. Simultaneously, the FRF comparisons obtained from different FE models and experiment are also shown. It is concluded that the GA, ASA, GA-SA are powerful optimization techniques which can be successfully applied to FE model updating, the natural frequencies and FRF obtained from all the updated models show much better agreement with experiment than that obtained from FEinit model. However, FEgasa is proved to be the most reasonable FE model, and also FEasa model is better than FEga model.

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FE model updating based on hybrid genetic algorithm and its verification on numerical bridge model

  • Jung, Dae-Sung;Kim, Chul-Young
    • Structural Engineering and Mechanics
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    • 제32권5호
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    • pp.667-683
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    • 2009
  • FE model-based dynamic analysis has been widely used to predict the dynamic characteristics of civil structures. In a physical point of view, an FE model is unavoidably different from the actual structure as being formulated based on extremely idealized engineering drawings and design data. The conventional model updating methods such as direct method and sensitivity-based parameter estimation are not flexible for model updating of complex and large structures. Thus, it is needed to develop a model updating method applicable to complex structures without restriction. The main objective of this paper is to present the model updating method based on the hybrid genetic algorithm (HGA) by combining the genetic algorithm as global optimization method and modified Nelder-Mead's Simplex method as local optimization method. This FE model updating method using HGA does not need the derivation of derivative function related to parameters and without application of complicated inverse analysis methods. In order to allow its application on diversified and complex structures, a commercial FEA tool is adopted to exploit previously developed element library and analysis algorithms. Moreover, an output-level objective function making use of measurement and analytical results is also presented to update simultaneously the stiffness and mass of the analysis model. The numerical examples demonstrated that the proposed method based on HGA is effective for the updating of the FE model of bridge structures.

$\alpha$-(Fe, Co)기 Nd-(Fe, Co)-B-Nb-Cu 초미세결정립합금의 자기특성에 미치는 Nd의 영향 (Influence of Nd Content on Magnetic Properties of Nanocrystalline $\alpha$-(Fe, Co)-Based Nd-(Fe, Co)-B-Nb-Cu Alloys)

  • 조덕호;조용수;김택기;송민석;김윤배
    • 한국자기학회지
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    • 제9권3호
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    • pp.154-158
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    • 1999
  • Nd 함유량을 2~6at.%로 변화시킨 $\alpha$-(Fe, Co)-B-Nb-Cu 초미세결정립합금의 미세조직 및 자기특성을 조사하였다. 급속응고된 Ndx(Fe0.9Co0.1)90-xB6Nb3Cu1(2$\leq$x$\leq$6, 1at.% 간격) 합금은 x=3 이상에서 비정질상으로 제조되었다. 제조된 비정질합금은 열처리에 의해 $\alpha$-(Fe, Co) 및 Nd2(Fe, Co)14B1상으로 구성된 초미세결정립합금으로 결정화 되었다. 최적열처리조건에서 잔류자화는 Nd의 증가에 따라 감소하며, x=3에서 1.55T로 최대 값을 나타내었다. 보자력은 Nd함유량 증가에 따라 직선적으로 증가하여 x=6에서 4.6kOe이었으며, 최대에너지적은 10.6MGOe였다.

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