• Analytical Science and Technology
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• v.14 no.2
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• pp.173-179
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• 2001

The study was carried out to analyze the pollutant Fe, Cu, Cr, Zn, Cd for sediments collected from lake in K river basin. Three analytical methods currently used in Korea, Japan, U.S.A, were compared. Pretreatment using microwave digestion showed higher analytical results for Fe, Cu, Cr, Zn, Cd than Korean Official Method(KOM) and American Toxicity Characteristic Leaching Procedure(TCLP) Method. Also, analytical results using microwave digestion, TCLP and KOM were as follows: 38.1-48.0 mgFe/kg, 10.2-15.9 mgFe/kg AND 3.5-12.6 mgFe/kg, 37.0-50.1 mgCu/kg, 0.06-0.24 mgCu/kg and 0.01-0.03 mgCu/kg, 137.0-152.0 mgZn/kg, 0.67-0.82 mgZn/kg and 0.3-0.5 mgZn/kg, respectively. From this result, a new analytical method for the determination of heavy metal in sediment should be developed for the accurate estimation of pollution degree in sediment.

• Journal of Electrical Engineering and Technology
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• v.2 no.2
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• pp.216-220
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• 2007

This paper deals with the characteristic analysis of the single phase switched reluctance motor based on the converter coupled FE analysis. The converter comprises a rectifier, LC filter and switching power device. A computational technique for the converter coupled FE analysis is introduced and its validity is proven by the experiment.

• Journal of Magnetics
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• v.16 no.3
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• pp.308-311
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• 2011

In order to obtain mono-dispersed Fe NPs with high saturation magnetization, quantitative analysis method to investigate the growth dynamics of the Fe NPs synthesized by a conventional thermal decomposition method has been developed. As a result, fast nucleation process promotes formation of ~4 nm of initial nucleus with a non-equilibrium phase, resulting in low saturation magnetization. And slow particle growth with atomic-scaled surface precipitation mode (< 100 atoms/($min{\cdot}nm^2$)) can form the growth layer on the surface of initial nucleus with high saturation magnetization (~190 emu/$g_{Fe}$) as an equilibrium a phase of Fe. Therefore, higher stabilization of small initial nucleus generated just after the injection of $Fe(CO)_5$ should be one of the key issues to achieve much higher $M_s$ of Fe NPs.

• Transactions of the Korean Society for Noise and Vibration Engineering
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• v.21 no.8
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• pp.761-767
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• 2011

Free and forced vibration analysis of the global ship structure using the 3-dimensional finite element(FE) method requires not only the specialized knowledge such as ship structure interacted with fluid, damping and various excitations due to propulsion system but also time-consuming manual tasks in FE modeling, analysis and response evaluation. As a result, the quality of the vibration analysis highly depends on engineer's expertise and experience. In this study, a framework system to improve the efficiency of global ship vibration analysis is introduced. The system promising the utilization of MSC/Patran and MSC/Nastran consists of various modules to support data management, FE modeling of ship structure and loading, input deck generation for free and forced vibration analysis, data extraction and evaluation of analysis results, and databases for FE models of marine diesel engines and vibration criteria. The system may be useful for pursuing standardization of uncertain analysis factors as well as reducing time, cost and human dependency in ship vibration analysis.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2011.04a
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• pp.779-784
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• 2011

Free and forced vibration analysis of the global ship structure using the 3-dimensional finite element(FE) method requires not only the specialized knowledge such as ship structure interacted with fluid, damping and various excitations due to propulsion system but also time-consuming manual tasks in FE modeling, analysis and response evaluation. As a result, the quality of the vibration analysis highly depends on engineer's expertise and experience. In this study, a framework system to improve the efficiency of global ship vibration analysis is introduced. The system promising the utilization of MSC/Patran and MSC/Nastran consists of various modules to support data management, FE modeling of ship structure and loading, input deck generation for free and forced vibration analysis, data extraction and evaluation of analysis results, and databases for FE models of marine diesel engines and vibration criteria. The system may be useful for pursuing standardization of uncertain analysis factors as well as reducing time, cost and human dependency in ship vibration analysis.

• Journal of the Korean Ceramic Society
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• v.48 no.5
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• pp.454-457
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• 2011

We report the preparation of nanocrystalline cobalt ferrite, $CoFe_2O_4$, particles using recycled $Co_3O_4$ and their surface coating with silica using micro emulsion method. Firstly, the $Co_3O_4$ powders were separated from waste cemented carbide with acid-base chemical treatment. The cobalt ferrite nanoparticles with the size 10 nm are prepared by thermal decomposition method using recycled $Co_3O_4$. $SiO_2$ was coated onto the $CoFe_2O_4$ particles by the micro-emulsion method. The $SiO_2$-coated $CoFe_2O_4$ particles were studied their physical properties and characterized by X-ray diffraction (XRD), high resolution-transmission electron microscopy (TEM) analysis and CIE Lab value.

• Resources Recycling
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• v.20 no.5
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• pp.58-63
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• 2011

pH control-precipitation method is used for recovery of EDTA from waste fluid of archeological waterlogged wood conservation treatment. EDTA has been used for eliminating of blacken effect in archeological waterlogged wood which was buried in the ground for long period of time. The black substance is generated by Fe$^{3+}$ in the soil reacted with tannin in the archeological waterlogged wood. In order to remove the black substance in archeological waterlogged wood, EDTA was used. The black substance is eliminated from wood as Fe-EDTA complex are formed, and EDTA is separated and precipitated from Fe-EDTA complexes at pH 2.68 or less. The result of analysis of the precipitated products and the commercial EDTA by FT-IR and FE-SEM showed that precipitated product by pH adjusted was not a type of Fe-EDTA complex, but pure EDTA. In this study, Fe$^{3+}$ from waste fluid of EDTA can be separated by HCl added. EDTA can be recycled by using the method of precipitation of EDTA in a strong acid.

• Resources Recycling
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• v.1 no.1
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• pp.44-50
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• 1992

The $\alpha$-FeOOH powders were prepared by allkaline and acidic method on the small scale plant from the waste pickling liquor of iron. $\alpha$-FeOOH, $\alpha-Fe_2O_3$, $Fe_3O_4$ and ${\gamma}-Fe_2O_3$ powders were examined by TEM, SEM, TG-DTA, X-ray diffraction, VSM and chemical analysis. The results obtained from the experiment could be summerized as follows : the reaction time for the preparation of $\alpha$-FeOOH was observed to be smaller in the case of alkaline method and the products was acicular with the size of about $0.5\mu\textrm{m}$. The color of $\alpha-FeOOH and $\alpha-Fe_2O_3$was lovely yellow and red, respectively. The magnetic properties of $Fe_3O_4$ obtained by the reduction of $\alpha-Fe_2O_3$in the $H_2$ atomosphere at $370^{\circ}C$ for 1 hour showed 367(Oe) and 82.7(emu/g).

• Transactions of Materials Processing
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• v.16 no.1 s.91
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• pp.25-30
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• 2007

The present study covers an integrated simulation method to evaluate optical performance of an aspheric plastic lens by connecting a finite element (FE) analysis of injection molding with a ray tracing simulation. Traditional ray tracing methods have based on the assumption that the optical properties of a lens are homogeneous throughout the entire volume. This assumption is to a certain extent unrealistic for injection-molded plastic lenses because material properties vary at every point due to the injection molding effects. To take into account the effects of the inhomogeneous optical properties of the molded lens, a new.ay tracing scheme is proposed in conjunction with a FE analysis of the injection molding. A numerical scheme is developed to calculate ray paths on every element layer with more realistic information of the refractive indices which can be obtained through the FE analysis. This information is then used to calculate the ray paths based on the FE mesh of which nodal points have unique index values. The proposed tracing scheme is implemented on the tracing of an aspheric lens, and its validity is ascertained through experimental verification.

• International Journal of High-Rise Buildings
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• v.3 no.4
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• pp.305-310
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• 2014

Wind-induced responses of a structure are often evaluated through dynamic analysis, where measured wind forces obtained from a wind-tunnel test and dynamic properties obtained from a FE (Finite Element) model are utilized. However, the FE model generally shows considerable discrepancies in the estimation of natural frequencies compared to field measurements due to some assumptions and simplifications. In this paper, a calibration method that can improve the estimation of natural frequencies in the FE model is proposed, and specific cases are studied for its validity with comparison to the field measurement results.