• Title/Summary/Keyword: F8WT

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Morphology Observation of Nanostructured Ti-25Ta-xZr Alloys

  • Kim, Hyun-ju;Ko, Yeong-Mu;Choe, Han-Cheol
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2012.05a
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    • pp.331-331
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    • 2012
  • In this study, we investigated morphology observation of nanostructured Ti-25Ta-xZr alloys. Ti-25Ta-(3wt%~15 wt%) Zr alloys were prepared by a vacuum arc-melting furnace. Formation of nanotubular structure was achieved by an electrochemical method in 1M $H_3PO_4$ electrolytes containing 0.8%wt.% NaF. Nanotube morphology depended on alloying elements.

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Effect of PbO on Microwave Dielectric Properties of (Pb, Ca) (Fe, Nb, Sn) O3 Ceramics

  • Yoon, Seok-Jin;Park, Ji-Won;Kang, Chong-Yun;Kim, Hyun-Jai;Jung, Hyung-Jin;Sergey Kucheiko;Cho, Bong-Hee
    • The Korean Journal of Ceramics
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    • v.4 no.3
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    • pp.249-253
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    • 1998
  • The influence of PbO additive on dielectric properties and sintering behavior of $(Pb_{0.46}Ca_{0.55})$ {$(Fe__1/2}Nb_{1/2}){0.9}Sn_{{0.1}$}$O_3$ ceramics has been investigated. The incorporation of a limited excess PbO ($\leq$2.0 wt. %) in the starting materials is quite beneficial for densification in the temperature range of 1150~$1175^{\circ}C$ in air. At a small doping level (0.8 wt. %) the ceramics prepared from powders calcined at $900^{\circ}C$ showed the best dielectric properties. The dielectric constants ($\varepsilon_r$) and Q.f were found to be 85.8~85.6 and 8530~8600 GHz, respectively. The temperature coefficient of resonant frequency ($\tau_f$) varied in the range of -2~4 $ppm/^{\circ}C$. Examination of the microstructure as well as analysis of the second phases in these materials revealed the presence of the pyrochlore-type phase which is detrimental to the dielectrics.

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Preparation of Formed Ceramic materials by Recycling of Aluminium Dross (알루미늄 드로스를 이용한 무기 발포재 제조)

  • 박제신;박형규;장대규
    • Resources Recycling
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    • v.10 no.4
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    • pp.42-47
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    • 2001
  • Recycling of aluminum dross is a significant issue in domestic aluminum industry. In this study, formed ceramic materials were prepared using aluminum dross mixed with feldspar powders to investigate its application as industrial materials and utilization of aluminum dross. In the prepared sample, feldspar was melted at the sintered temperature, and its phase was trans-formed into amorphous, and spinel ($MgA1_2$$O_4$) phase in the dross was remained clearly. Density of the test specimen Increased from 0.91 to 0.65 gr/㎤ and water absorbance decreased from 2.5 to 1.7f% with increasing of sintered time at the sintered temperature $1220^{\circ}C$ with composition of feldspar 55 wt%, dross 40wt% and bentonite 5 wt%. At the same experimental conditions, bending strength of the test specimen was 10.8 MPa, and heat conductivity was 0.34 W/m.K with sintered time 30 minutes.

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Catalytic Decomposition of SF6 from Semiconductor Manufacturing Process (촉매를 이용한 반도체 공정 SF6 처리에 관한 연구)

  • Hwang, Cheol-Won;Choi, Kum-Chan
    • Journal of Environmental Science International
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    • v.22 no.8
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    • pp.1019-1027
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    • 2013
  • Sulfur hexa-fluoride has been used as a etching gas in semiconductor industry. From the globally environmental issues, it is urgent to control the emissions of this significant greenhouse gas. The main objective of this experimental investigation was to find the effective catalyst for $SF_6$ decomposition. The precursor catalyst of hexa-aluminate was prepared to investigate the catalytic activity and stability. The precursor catalyst of hexa-aluminate was modified with Ni to enhance the catalytic activities and stability. The catalytic activity for $SF_6$ decomposition increased by the addition of Ni and maximized at 6wt% addition of Ni. The addition of 6wt% Ni in precursor catalyst of hexa-aluminate improved the resistant to the HF and reduced the crystallization and phase transition of catalyst.

Al-10wt%Ti-4wt%F Alloys as In-situ Composites through Rapid Solidification(II) (급냉응고법에 의한 In-Situ 복합재료로서의 Al-10wt%Ti-4wt%Fe 합금 (II))

  • Kim, Hye-Seong;Jeong, Jae-Pil;Gwon, Suk-In;Geum, Dong-Hwa
    • Korean Journal of Materials Research
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    • v.8 no.12
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    • pp.1127-1132
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    • 1998
  • The possibilities of producing Al-10%Ti-4%Fe composites through in-situ processing and thus achieving mechanical property improvements over binary Al-10%Ti to a level or higher exhibited by PM SiC/A12124 composites were explored in this study. The microstructure of in-situ processed Al-10%Ti-4%Fe composites was similar to that of Al matrix composites reinforced with discontinuous SiC particulates(SiC/A12124) and significant enhancements in elastic modulus, tensile strength and wear resistance were observed as compared to Al-10%Ti alloy. These results can be attributed to the in-situ formed Al. Fe by third element addition, leading to additional dispersion strengthening effect over $Al_3Ti$ phase reinforcement in Al-Ti system.

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Effect of Action Observation Training with Auditory Feedback for Gait Function of Stroke Patients with Hemiparesis

  • Kim, Hyeong Min;Son, Sung Min
    • The Journal of Korean Physical Therapy
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    • v.29 no.5
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    • pp.246-254
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    • 2017
  • Purpose: Previous studies have reported that action observation training has beneficial effects on enhancing the motor task, such as balance and gait functions. On the other hand, there have been few studies combined with action observation training and auditory feedback. The purpose of this study was to determine the effects of action observation training with auditory feedback on the gait function in stroke patients with hemiparesis Methods: A total of 24 inpatients with post-stroke hemiparesis were assigned randomly to either an experimental group 1 (EG 1, n=8), experiment group 2 (EG 2, n=8), control group (CG, n=8, EG 1). The EG 2 and CG watched video clip demonstrating three functional walking tasks with auditory feedback, without auditory feedback, and showing a landscape image, respectively. The exercise program consisted of 30 minutes, five times a week, for four weeks. The participants were measured to 10MWT (10 m walk test), 6MWT (6 minutes walking distance test), TUG (timed up and go test), DGI (dynamic gait index), time and steps of F8WT (figure-of-8 walk test). Results: In the intra-group comparison after the intervention, EG 1 and EG 2 showed a significantly different gait function (10MWT, 6MWT, DGI, TUG, F8WT) (p<0.05). In the inter-group comparison after intervention, EG 1 showed significant improvements in the entire gait parameters and EG 2 only showed significant improvement in DGI and TUG compared to CG (p<0.05). Conclusion: These findings show that action observation training with auditory feedback may be used beneficially for improving the gait function of stroke patients with hemiparesis.

Study of enhanced physical and pervaporation properties in composite membrane

  • RajiniKanth, Vanarch;Ravindra, Sakey;Madalageri, Priya M;Kajjari, Praveen B.;Mulaba-Bafubiandi, Antoine F
    • Membrane and Water Treatment
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    • v.8 no.5
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    • pp.483-498
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    • 2017
  • Novel mixed matrix membranes of Sodium Alginate (NaAlg) were developed by the incorporation ofunmodified, modified Phosphomolybdic acid (PMA) then cross-linked with glutaraldehyde externally. These membranes were prepared by the solution casting technique. Pervaporation (PV) experiments have been performed with pure NaAlg, unmodified NaAlg-PMA5, NaAlg-PMA10, modified NaAlg-mPMA5, and NaAlg-mPMA10 (wt. % of PMA 5 and 10) at 30, 40 and $50^{\circ}C$, to separate water-isopropanol feed mixtures containing 10-30 wt. % of water. Pervaporation results of NaAlg-mPMA10 produced a highest separation factor of 9028 with a flux of $0.269kg/m^2.h$ for 10 wt. % of water containing feed mixture. Both separation factor and flux for water increased significantly with increasing content of mPMA into NaAlg; a significant improvement in PV performance was observed for NaAlg-mPMA5 and NaAlg-mPMA10 membranes when compared to pure NaAlg& PMA-5, PMA-10 membrane.

Effect of Pb based flux on the Microwave Dielectric Properties of PCFN-PZW System (PCFN-PZW계의 마이크로파 유전 특성에 미치는 Pb계 Flux의 영향)

  • 강동헌;설충의;차훈주;김영호;길상근;조봉희
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.15 no.12
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    • pp.1027-1032
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    • 2002
  • (Pb$\_$0.4/Ca$\_$0.6/)(Fe$\_$1/2/Nb$\_$1/2/)O$_3$ system was modified by 10 mol% Pb(Zn$\_$1/2/W$\_$1/2/)O$_3$ addition and their sinterability and microwave properties were investigated as a function of the amount of flux (0.975PbO-0.025SnO$_2$). With increasing flux content, single perovskite phase was maintained up to 3 wt% flux addition and further addition led to the presence of Pb-rich second phase which was confirmed by EDS analysis. The apparent densities of PCFN-PZW specimen increased and showed maximum values at 2.5 wt% flux addition for the Ts=1000$^{\circ}C$ and 2.0wt% flux addition for the Ts=1050$^{\circ}C$, respectively. The dielectric constant and Q$.$f values strongly depended on the variation of density and microstructure, where the optimum values of $\varepsilon$$\_$r/ = 91.95, Q$.$f = 5938GHz, TCF = +8.15ppm/$^{\circ}C$ were obtained for the 2.5wt% flux added PCFN-PZW specimen sintered at 1000$^{\circ}C$ for 4h.

Solubility of TiO2 in NaF-CaF2-BaF2 Melts

  • Yoo, Jeong-Hyun;Cho, Sung-Wook
    • Metals and materials international
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    • v.24 no.6
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    • pp.1386-1393
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    • 2018
  • The solubility of $TiO_2$ in $NaF-CaF_2-BaF_2$ ternary eutectic melts was investigated at the temperature range of $1025-1150^{\circ}C$. The least-squares equation was obtained from the relationship between the reciprocal temperature and the natural logarithm of the titanium concentration in the melts saturated with $TiO_2$. The corresponding partial molar enthalpy of dissolution of $TiO_2$ was found to be 188 kJ/mol. The titanium saturation concentration was 3.73 wt% at $1100^{\circ}C$. From the titanium concentration change with the added amount of $TiO_2$ at different holding time after a final stirring, it was found that not only complete dissolution of $TiO_2$ but also enough sedimentation of excessive $TiO_2$ should be guaranteed to obtain more reliable solubility data. The holding time of 10 h was found to be enough for the excessive $TiO_2$ particles to settle down in our experimental conditions. It is noteworthy that in case of adding $TiO_2$ in excess of its solubility, the $Ba_{1.12}(Ti_8O_{16})$ phase was observed at the lower and bottom of the solidified salt ingots.

Effect of Calcination Temperature on the Sintering Behaviors and Microwave Dielectric Properties of (Zn0.8Mg0.2)TiO3 System (하소온도가 (Zn0.8Mg0.2)TiO3계의 소결거동과 마이크로파 유전특성에 미치는 영향)

  • 심우성;방재철
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.12S
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    • pp.1205-1209
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    • 2003
  • We investigated the effects of calcination temperatures on the sintering behaviors and microwave dielectric Properties of (Z $n_{0.8}$M $g_{0.2}$)Ti $O_3$ system. Highly densified samples were obtained at the sintering temperatures below 100$0^{\circ}C$ with additions of 0.45 wt.%B $i_2$ $O_3$ and 0.55 wt.% $V_2$ $O_{5}$. From the examination of the existing phases and microstructures before and after sintering of (Z $n_{0.8}$M $g_{0.2}$)Ti $O_3$ system which is calcined at the various temperatures ranging from 80$0^{\circ}C$ to 100$0^{\circ}C$, it was found that higher Q${\times}$ $f_{o}$ values were obtained when unreacted phases in calcined body were reduced. When calcined at 100$0^{\circ}C$ and sintered at 90$0^{\circ}C$, it consists of hexagonal as. a main phase with uniform microstructure and exhibits Q${\times}$ $f_{o}$ value of 42,000 GHz and dielectric constant of 22. 22. 22.