• 제목/요약/키워드: F0 Range

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$(Ba_{0.93}Sr_{0.07}O)-0.5Sm_2O_3-4.5TiO_2$계 세라믹스의 불순물 첨가에 따른 마이크로파 유전특성 (Effect of Impurity Addition on the Microwave Dielectric Properties of $(Ba_{0.93}Sr_{0.07}O)-0.5Sm_2O_3-4.5TiO_2$ Ceramics)

  • 김태중;장재훈;이희영
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2002년도 하계학술대회 논문집 Vol.3 No.2
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    • pp.1148-1151
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    • 2002
  • Dielectric ceramics with nominal composition of $(Ba_{0.93}Sr_{0.07}O)-0.5Sm_2O_3-4.5TiO_2$ was prepared using the conventional mixed oxide process-derived powder. Effect of $SiO_2$, $MnO_2$ and $Al_2O_3$ impurity addition on the microwave properties was examined in some detail. Measured relative permittivity $(\varepsilon_r)$ values were in the range of 53 to 59 and showed little dependence on impurity addition. In contrast, quality factor $(Q{\cdot}f)$ and temperature coefficient of resonant frequency $(\tau_f)$ values were greatly influenced by the type and the amount of impurities. It was found that 0.1~0.2wt% addition of $Al_2O_3$ was most effective for improving the properties, where ${\varepsilon}_r$, $Q{\cdot}f$ and $\tau_f$ values were 57.7, 10000, and +7ppm/$^{\circ}C$, respectively.

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지리산에 방사한 반달가슴곰의 행동권 크기 및 서식지 이용 특성 연구 (The Studies on Characteristics of Home Range Size and Habitat Use of the Asiatic Black Bear Released in Jirisan)

  • 양두하;김보현;정대호;정동혁;정우진;이배근
    • 한국환경생태학회지
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    • 제22권4호
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    • pp.427-434
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    • 2008
  • 2004년 10월부터 2006년 12월까지 지리산에 방사한 반달가슴곰 7개체를 무선추적하여 연간 행동권 크기를 분석한 결과, 95% MCP에서 반달가슴곰 암컷은 71.66$km^2$, 수컷은 90.20$km^2$로 분석되었다. 계절별 행동권 크기는 암컷곰이 봄 19.8$km^2$, 여름 30.48$km^2$, 가을 22.63$km^2$, 겨울 0.22$km^2$이었고, 수컷곰은 봄 33.47$km^2$, 여름 20.26$km^2$, 가을 23.23$km^2$, 겨울 0.78$km^2$이었다(F=4.193, P<0.05). 반달가슴곰의 행동권역중 약 38% 정도가 중첩되었고, 암컷간 12.5%, 수컷간 22.4% 정도가 중첩되었다. 서식지 평균 해발고도는 봄 744$\pm$236m, 여름 682$\pm$253m, 가을 937$\pm$218m, 겨울 975$\pm$137m로 분석되었다(F=8.526, P<0.001). 반달가슴곰의 행동권 크기와 위치는 주로 먹이의 분포와 생산량과 밀접한 관계가 있으며, 계절별 서식 환경특성, 연령 등에 따라서도 차이가 있음을 알 수 있었다.

The Effects of LaF3 Coating on the Electrochemical Property of Li[Ni0.3Co0.4Mn0.3]O2 Cathode Material

  • Yun, Su-Hyun;Kim, Seuk-Buom;Park, Yong-Joon
    • Bulletin of the Korean Chemical Society
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    • 제30권11호
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    • pp.2584-2588
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    • 2009
  • The effect of $LaF_3$ coating on the structural and electrochemical properties of $Li[Ni_{0.3}Co_{0.4}Mn_{0.3}]O_{2}$ cathodes was investigated using XRD, SEM, TEM, and a cycler. The coating layer consisted of nano-sized particles attached nonuniformly to the surface of pristine powder. Despite the surface coating treatment, phase difference by $LaF_3$ coating was not detected. The discharge capacities of coated electrodes were a little lower than that of pristine sample at a 1 C rate. However, as the C rate increases, the capacity retention of the coated sample becomes obviously superior to that of the pristine sample. The cyclic performances of the electrodes in the voltage range of 4.8 $\sim$ 3.0 V were also improved by the surface coating. Such enhancement is attributed to the presence of the $LaF_3$ coating layer, which effectively suppressd the reaction between electrodes and electrolytes on the surface of the $Li[Ni_{0.3}Co_{0.4}Mn_{0.3}]O_{2}$ electrode.

$(Zr_{0.65}, Sn_{0.35})Ti_{1.04}O_{4.04}$세라믹스의 NiO첨가에 따른 고주파 유전 특성 (Microwave dielectric properties according to the additions of NiO to $(Zr_{0.65}, Sn_{0.35})Ti_{1.04}O_{4.04}$ ceramics)

  • 윤중락;권정열;이헌용;김경용
    • E2M - 전기 전자와 첨단 소재
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    • 제8권5호
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    • pp.594-600
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    • 1995
  • Dielectric properties at microwave frequencies of ($Zr_{0.65}$, $Sn_{0.35}$) $Ti_{1.04}$ $O_{4.04}$ ceramics with additives, NiO as an agent to improve dielectric properties and $B_{2}$ $O_{3}$ as a firing agent were investigated. When 0.5 - 1.5 wt% of NiO is add, the grain growth is inhibited and the shape of the grain is uniformed, Dielectric constant(Fr) and bulk density are increased with raising amount of NiO at sintering temperature of 1330 - 1360.deg. C, but the temperature coefficient of resonant frquency(.epsilon.$_{r}$) decreased gradually as the NiO content increased. The value of Qx $f_{o}$ was increased as the amount of NiO was increased in the range of 0.5 to 1.0 wt% and the Qx $f_{o}$, was decreased slightly with raising sintering temperature. With NiO of 1.0 wt% and at sintering temperature of 1360.deg. C, this ceramics was found to have excellent microwave properties of .epsilon.$_{r}$=37.8, Qx $f_{o}$ = 48.600 and .tau.$_{f}$ = 7 ppm/.deg. C.C.. C.. C.C.. C.. C.

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산사(山楂)의 규격 기준 모니터링 및 HPLC 표준크로마토그램 연구 (Quality Monitoring of Specification of Crataegi Fructus in the Korean Pharmacopoeia and Studies HPLC Standard Chromatogram)

  • 김경희;김선미;이영종;백완숙
    • 대한본초학회지
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    • 제32권1호
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    • pp.55-62
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    • 2017
  • Objectives : Crataegi Fructus has been used as traditional medicines for more digestion action, amenorrhea due to blood stasis, and hyperlipemia. The aim of this study was to compare of Crataegi Fructus in South Korea collected during three years according to the standards in monographs of the Korean Pharmacopoeia Eleventh edition (KP 11). Methods : Crataegi Fructus was carried out identification test (Qualitative reaction, Thin layer chromatography), heavy metal test, and total ash registered at KP. Add to we tested loss on dry, contents of ethanol-soluble extracts, and HPLC profiling. Results : Identification test (TLC) was on comparing with ursolic acid standard solution in $R_f$ value, all samples showed red purple spot ($R_f$ value 0.9). Ursolic acid spot in $R_f$ value 0.35 showed by changing mobile phase condition. Heavy metals showed contents for Pb, Cd, As, and Hg range of 0.0 ~ 0.5 ppm, 0.0 ~ 0.2 ppm, 0.0 ~ 0.3 ppm, and 0.0 ~ 0.1 ppm. Loss on drying was ranged from 5.5 to 11.9 %, total ash was between the range 2.7 ~ 4.0 %. Contents of ethanol-soluble extracts was ranged from 17.8 to 44.9 %. The content of chlorogenic acid was ranged from 0.0 to 0.1 % based on the chlorogenic acid standard curve. Conclusion : We have verified the current specification standard of Crataegi Fructus and standard that is not set. We hope that it will help the standardization of Crataegi Fructus.

Synthesis, Structural and Electrical Characterizations of $Pr_{2-x}Ba_xNiO_{4{\pm}\delta}{^\$}$

  • 장영기;권영구;변송호
    • Bulletin of the Korean Chemical Society
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    • 제16권2호
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    • pp.120-125
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    • 1995
  • Solid solutions of Pr2-xBaxNiO4±δ with K2NiF4-type structure were prepared in air and characterized by powder X-ray diffraction, Rietveld refinements, iodometry titrations, and conductivity measurements. The range of the solid solution was 0 ≤ x < 0.5. The crystal structure changes from orthorhombic (Fmmm) for x ≤ 0.1 to pseudo-tetragonal (I4/mmm) for x ≥ 0.2. The orthorhombic structure of x=0.1 transforms to tetragonal at low temperature. The bond distances obtained from the Rietvel analyses did not vary significantly with the Ba content except that of Ni-O (parallel to the c-axis) which showed an abrupt increase from x=0.1 to 0.2. The excess oxygen content (δ) decreases from 0.241 to 0.03 with increasing substituted Ba contents within the solution range. The samples are all semiconductors at the temperature range 4 < T < 300 K.

Preoperative Nodal 18F-FDG Avidity Rather than Primary Tumor Avidity Determines the Prognosis of Patients with Advanced Gastric Cancer

  • Kwon, Hyun Woo;An, Liang;Kwon, Hye Ryeong;Park, Sungsoo;Kim, Sungeun
    • Journal of Gastric Cancer
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    • 제18권3호
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    • pp.218-229
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    • 2018
  • Purpose: This study investigated whether the metabolic avidity of primary tumors and/or metastatic lymph nodes (LNs) measured by $^{18}F$-fluorodeoxyglucose ($^{18}F-FDG$) positron emission tomography/computed tomography (PET/CT) was related to survival after surgery in patients with advanced gastric cancer (AGC). Materials and Methods: One hundred sixty-eight patients with AGC who underwent preoperative $^{18}F-FDG$ PET/CT and curative resection were included. The $^{18}F-FDG$ avidity of the primary gastric tumor and LNs was determined quantitatively and qualitatively. The diagnostic performance of $^{18}F-FDG$ PET/CT was calculated, and the prognostic significance of $^{18}F-FDG$ avidity for recurrence-free survival (RFS) and overall survival (OS) was assessed. Results: In all, 51 (30.4%) patients experienced recurrence, and 32 (19.0%) died during follow-up (median follow-up duration, 35 months; range, 3-81 months); 119 (70.8%) and 33 (19.6%) patients showed $^{18}F-FDG$-avid primary tumors and LNs, respectively. $^{18}F-FDG$ PET/CT showed high sensitivity (73.8%) for the detection of advanced pathologic T ($pT{\geq}3$) stage and high specificity (92.2%) for the detection of advanced pN (${\geq}2$) stage. $^{18}F-FDG$ avidity of LNs was significantly associated with RFS (P=0.012), whereas that of primary tumors did not show significance (P=0.532). Univariate and multivariate analyses revealed that $^{18}F-FDG$ avidity of LNs was an independent prognostic factor for RFS (hazard ratio=2.068; P=0.029). Conclusions: $^{18}F-FDG$ avidity of LNs is an independent prognostic factor for predicting RFS. Preoperative $^{18}F-FDG$ PET/CT can be used to determine the risk and prognosis of patients with AGC after curative resection.

수정 Forman 모델을 이용한 고성능 강재의 피로균열전파와 피로수명평가 (Fatigue Crack Propagation and Fatigue Life Evaluation of High-Performance Steel using Modified Forman Model)

  • 최성원;강동환;이종관;김태원
    • 대한기계학회논문집A
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    • 제35권11호
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    • pp.1361-1368
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    • 2011
  • 응력확대계수비와 하중 주파수가 각각 'R=0.1, f=0.1 Hz', 'R=0.3, f=0.3 Hz' 및 'R=0.5, f=0.5 Hz'인 세가지 하중 조건에서 피로균열전파 실험을 하였으며 이를 바탕으로 고성능 강재의 피로균열전파거동 분석과 피로수명평가를 수행하였다. 하중 조건에 따른 피로균열전파거동을 모사하기 위해 수정된 Forman 모델을 제안하였으며 제안된 모델은 하한 응력확대계수폭과 균열 닫힘 현상에 의한 유효 응력확대계수폭을 고려함으로써 거동의 전 영역을 모사할 수 있었다. 응력확대계수비와 하중 주파수가 0.1 인 경우, 균열이 약 5.0 mm 전파될 때 피로수명을 평가한 결과, Forman 모델은 8,814 cycles, 수정된 모델은 12,292 cycles 의 계산결과를 얻었으며, 이를 12,774 cycles 의 실제 실험결과와 비교할 때 수정된 Forman 모델이 실제 피로균열전파거동을 보다 효과적으로 모사하고 있음을 확인할 수 있었다.

중년 여성의 자아개념과 우울과의 관계 (Relationship between Self concept and Depression of Middle-Aged Women)

  • 성미혜
    • 보건교육건강증진학회지
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    • 제19권1호
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    • pp.171-184
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    • 2002
  • The purpose of this study was to investigate the relationship between self concept and depression of middle-aged women. The Subjects were 102 middle-aged women whose age range were 40-59 years old living in urban area. The instruments used in this study were self concept scale developed by Rosenberg and the depression scale developed by Zung. Data were collected done from July 1 to July 31, 2001 by a structured questionnaire. The Data were analyzed by the SPSS/PC+ program using t-test, ANOV A and Pearson Correlation Coefficient. The results of the study were as followed : 1. Mean score of self concept was 2.35. 2. Mean score of depression scale was 2.43 3. The relationship between self concept and depression was statistically negative correlation(r=-0.3769, P〈0.001). 4. There were statistically significant differences in the score of middle-aged women's self concept to the age(F=3.41, P〈0.05), education(F=2.97, P〈0.05), Occupation(t=1.84, P〈0.05). 5. General characteristics variables were significantly related to the level of depression were the age(F=3.12, P〈0.05), numbers of children(t=3.59,P〈0.05). Obstetrical characteristics variables were significantly related to the level of depression were age of menarche(F=4.03, P〈0.05), times of abortion(t=10.09, P〈0.001). In conclusion, this study revealed that self esteem was an important factor related to depression. I suggest that to decrease depression, it should be encouraged self esteem.

Effect of PbO on Microwave Dielectric Properties of (Pb, Ca) (Fe, Nb, Sn) O3 Ceramics

  • Yoon, Seok-Jin;Park, Ji-Won;Kang, Chong-Yun;Kim, Hyun-Jai;Jung, Hyung-Jin;Sergey Kucheiko;Cho, Bong-Hee
    • The Korean Journal of Ceramics
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    • 제4권3호
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    • pp.249-253
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    • 1998
  • The influence of PbO additive on dielectric properties and sintering behavior of $(Pb_{0.46}Ca_{0.55})$ {$(Fe__1/2}Nb_{1/2}){0.9}Sn_{{0.1}$}$O_3$ ceramics has been investigated. The incorporation of a limited excess PbO ($\leq$2.0 wt. %) in the starting materials is quite beneficial for densification in the temperature range of 1150~$1175^{\circ}C$ in air. At a small doping level (0.8 wt. %) the ceramics prepared from powders calcined at $900^{\circ}C$ showed the best dielectric properties. The dielectric constants ($\varepsilon_r$) and Q.f were found to be 85.8~85.6 and 8530~8600 GHz, respectively. The temperature coefficient of resonant frequency ($\tau_f$) varied in the range of -2~4 $ppm/^{\circ}C$. Examination of the microstructure as well as analysis of the second phases in these materials revealed the presence of the pyrochlore-type phase which is detrimental to the dielectrics.

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