• Preventive Nutrition and Food Science
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• 제2권4호
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• pp.296-300
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• 1997

Glucose syrup and lactose, mixed with citric acid as a polymerizing catalyst, was processed using twin screw extruder, in which 40 of L/D(length/diameter) ratio was designed to provide sufficient retention in extruder for polymerization of sugars. The polymerization yields of glucose syrup were 36.90%, 55.44% and 77.10% at 160, 180 and 20$0^{\circ}C$, respectively, while those of lactose were 26.45%, 38.16% and 45.86% at the same temperatures. Gel permeation chromatography exhibited that the higher molecular weight fractions were increased with extrusion temperature, which also led to increasing hydrodynamic intrinsic viscosity. Both uco-oligosaccharides and lacto-oligosaccharides produced by extrusion of glucose syrup and lactose were stable for thermal treatments over a wide range of pH3.0~11.0. In addition, $\alpha$-amylase and amyloglucosidase treatment of gluco-oligosaccharides did not affect the solution viscosity, indicating the random linkage rather than $\alpha$-1, 4 linkages of glucose and thus the potential applications as a dietary fiber. In this research it was clearly observed that twin screw extrusion can be successfully utilized to produce gluco-oligosaccharides and lacto-oligosaccharides rapidly and continuously in conjunction with selective control of polymerized composition.

• 한국정밀공학회지
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• 제18권7호
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• pp.179-185
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• 2001

Porthole die extrusion is profitable to manufacture long tube with hollow section. The material through portholes is gathered within chamber and welded under high pressure. This weldability which classifies the quality of tube product is affected by several variables and die shape. But, porthole die extrusion has been executed on the experience of experts due to the complicated die assembly and complexity of metal flow. Analytic approaches that are useful in profitable die design and in the improvement of productivity are inevitably demanded. Therefore, the objective of this study is respectively to analyze the behavior of metal flow and to determine welding pressure of hot extrusion product according to the various billet temperature, bearing length and tube thickness by FE analysis and its results are compared with tube expanding tests.

• 대한기계학회논문집A
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• 제33권4호
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• pp.440-446
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• 2009

This paper was designed to fabricate the miniature spur gear with pitch circle of 2.25mm using extrusion process of a mechanically alloyed Al-78wt%Zn powder. The mechanical alloying of the powder particles were performed for ball milled times of 4h, 8h, 16 and 32h by the planetary ball milling. The mechanical properties of these alloyed powders, which were compacted and sintered-cylindrical preforms, were estimated using compression test. The results showed that the alloyed powder with average particle size of $10{\mu}m$ milled for 32h has the highest compressive(fractured) strength(288MPa). Extrusions of the miniature spur gear using the alloyed powder were carried out at different extrusion temperatures. Extrusion temperature of $300^{\circ}C$ provided the spur gear with the highest relative density and Vickers hardness and without any surface defects.

• 소성∙가공
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• 제24권6호
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• pp.425-430
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• 2015

In the current paper, the effects of initial slug design on the earring of an Al rectangular battery case manufactured by impact extrusion were studied. During impact extrusion, non-uniform metal flow between the long and the short sides of the battery case leads to earring, which is subsequently trimmed. Process parameters such as friction, aspect ratio of the battery case, the die shape and the forming temperature tend to induce earring because they cause greater non-uniform metal flow. Large aspect ratio of the battery case and high friction between slug and die can greatly affect the earring of a rectangular battery case. To make a rectangular battery case without earring, it is necessary to control metal flow uniformly during impact extrusion. One of the ways to reduce the earring is to control the metal flow of slug at the initial upsetting stage. To analyze the effects of the initial slug design on earring, FE analysis was conducted using DEFORM 3D. Two types of initial slug designs were evaluated where volume was removed along either the width or thickness directions. The results show that the initial slug design can be effective in adjusting the uniformity of metal flow.

• Preventive Nutrition and Food Science
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• 제11권4호
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• pp.318-322
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• 2006

The objective of this experiment was to investigate the effect of extrusion of ginseng roots in twin screw extruder on susceptibility of ginseng starch toward hydrolysis by ${\alpha}-amylase$ BAN 480L (Novozyme, Denmark) and cellulase Celluclast 150L and saccharification by amyloglucosidase AMG-E (Novozyme, Denmark). The extrusion was conducted at 22% and 30% moisture contents of feed at screw speed 300 rpm. Barrel temperature at zone 1 was adjusted at $100^{\circ}C$ and $120^{\circ}C$. The results showed that extrusion process improved the ginseng ${\alpha}-amylase$ susceptibility as compared to traditionally dried ginseng (white and red ginseng). Reducing sugar of hydrolyzed extruded samples was 2,500% of its initial concentration, whereas the reducing sugar of hydrolyzed non-extruded sample was only 200% of its initial concentration. However, addition of cellulase during liquefaction lowered the saccharification yield of both non-extruded and extruded samples as well.

• 대한기계학회논문집A
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• 제32권11호
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• pp.1010-1015
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• 2008

In this study, the characteristics of aluminum tube hydroformed products at different extrusion type and heat treatment conditions were investigated. For the investigation, as-extruded, full annealed and T6-treated Al 6061 tubes at different extrusion type were prepared. To evaluate the hydroformability, free bulge test was performed at room temperature to $300^{\circ}C$. Also mechanical properties of hydroformed products at various pre- and post-heat treatments were estimated by hexagonal prototype hydroforming test at $250^{\circ}C$. And the tensile test specimens were obtained from hexagonal prototype hydroformed tube. As a results, hydroformability of full annealed tube is $5{\sim}8%$ higher than that of extruded and T6-treated tube. The tensile strength and elongation of T6-post heat treated indirect extrusion tube were more than 330MPa and 12%, respectively. However, T6 pre treated hydroformed product represents high strength, 330MPa and low elongation, 8%. Therefore, Hydroformability of Al6061 tube showed similar value for both extrusion types. However flow stress of direct tube showed $20{\sim}50MPa$ lower value than indirect tube.

• 한국주조공학회지
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• 제30권6호
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• pp.210-216
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• 2010

The aim of this study is to characterize a thixoextruded 7075 Al wrought alloy bar in terms of its isotropic behavior through the optical microscope, mechanical test and electron back scattered diffraction. It is also discussed of the extrudability improvement for 7075 Al wrought alloy by thixoextrusion, with emphasis on controlling thixoextrusion parameters. Hot extrusion shows that the maximum extrusion pressure depends on their characteristics in terms of flow stress and hot workability. In the contrary, thixoextrusion demonstrates that the maximum extrusion pressure is almost uniform regardless of the experimental parameters, such as initial ram speed, die bearing length and thixoextrusion temperature. The hot extruded microstructures become elongated to extrusion direction, while the thixoextruded microstructures are isotropic and homogeneously distributed due to the existence of liquid phase between solid grains during the process. The grain refinement due to dynamic recrystallization during thixoextrusion has been also occurred. Subsequent recrystallization would lead to the strengthening of mechanical properties, as observed in the study. The important point is that the values of tensile, yield strength and elongation of the thixoextruded bar without plastic deformation are similar to those of the hot extruded bar with severe plastic deformation.

• 한국식품과학회지
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• 제33권6호
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• pp.686-692
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• 2001

전곡립을 이용한 기능성 식품개발을 위하여 현미, 현미찹쌀, 보리, 현미율무를 온도 $110{\sim}130^{\circ}C$, 수분함량 $15{\sim}25%$, 스크류속도 $200{\sim}300rpm$의 조건에서 압출성형하고, 반응표면분석법(RSM)을 이용하여 최적조건을 분석하였다. 압출공정에 의한 전곡립의 수용화 효과는 수분용해지수(WSI), 농도(수율), 고유점도를 측정하였으며, 수율과 고유점도를 동시에 고려하여 새로운 무차원군의 최적인자인 $([\eta])$를 적용하여 최적조건을 찾고자 하였다. 각 조건별 실험결과를 반응표면분석을 실시하여 본 결과, 종속변수들에 대한 결정계수$(R^2)$는 $0.936{\sim}0.984$ 범위로 나타났다. 현미의 경우에는 수용화 수율, 현미찹쌀은 고유점도, 보리와 현미율무는 수용화 수율과 고유점도에 대해서 모델식이 유의성을 나타내었다. 특히 독립변수 중에서는 수분함량이 가장 큰 영향을 보였다. 최적인자인 $([\eta])$에는 고유점도가 더 큰 영향을 미치므로, 현미의 경우에서는 유의성을 보이지 않았다. 현미의 경우를 제외하고 최적화 인자로 설정한 $([\eta])$의 최적값을 찾기 위하여 회귀분석을 한 결과 임계점은 스크류 속도는 약 300rpm, 수분함량은 20%, 온도는 $120^{\circ}C$인 지점에서 나타났다.

• 한국식품영양과학회지
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• 제33권5호
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• pp.899-904
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• 2004

압출성형공법을 이용한 수삼의 전처리를 통한 추출수율의 향상과 최적조건에서 열수 추출한 인삼추출액의 첨가량을 달리하여 저온압출공정으로 제조한 구형과립의 입자분포, 마모율, 용적밀도, 진동밀도, 압축지수와 용출패턴을 결정하였다. 열수추출수율에서 수삼을 압출성형할 때 수분함량이 가장 유의적으로 영향을 미쳤다. 수분함량의 감소와 함께 스크류 회전속도가 증가할수록 압출성형 수삼의 추출수율이 크게 증가하였다. 추출수율이 최대가 되는 압출성형 공정변수는 수분함량 15%, 스크류 회전속도 250 rpm, 사출구 부위온도 13$0^{\circ}C$였다. 동일한 추출조건에서 15개 압출성형 수삼 시료의 평균 추출수율(43.5%)은 홍삼(38.3%)과 백삼(29.0%) 추출수율과 비교하여 크게 향상되었다. 저온압출공정으로 압출성형 수삼농축액(고형분함량 59.2%)의 농도를 5, 20, 30, 40, 50, 60%로 각각 증류수에 희석한 용액 200 mL과 200 g 미세결정 셀룰로오즈를 이용하여 과립화시킬 수 있는 압출성형 수삼추출액의 최대 농도는 60%였으며 추출액의 증가와 함께 입자수율의 증가, 마모율의 감소, 압출지수의 감소 등으로 입자의 물리적 특성은 구형과립을 젤라틴 캡슐에 포장하여 제품화할 수 있었다. 또한 압출성형 수삼 추출액을 포함한 구형과립으로부터 농축액 성분이 10분 이내에 쉽게 용출되므로 구형과립은 젤라틴 캡슐에 적합하다는 결론을 내릴 수가 있었다.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2008년도 추계학술대회 논문집
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• pp.199-202
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• 2008

In this study, we investigated the thermal properties of $Zr_{66.4}Nb_{6.4}Cu_{10.5}Ni_{8.7}Al_{8.0}$ by using a differential scanning calorimeter (DSC), and then analyzed the composition of dendrite phase by using X-ray diffraction (XRD). A series of uniaxial compression tests has been performed under the strain rates between $10^{-5}/s$ and $10^{-2}/s$ at room temperature and near SLR. This BMGC has higher high temperature strength than other Zr-based monolithic BMGs because in-situ formed crystalline phases hinder a feasible viscous flow of amorphous matrix. Warm formability is also estimated by laboratory-scale extrusion test within supercooled liquid region. It was found that BMGC has poor formability compared with nother Zr-based bulk metallic glass composite presumably due to large volume fraction of 'brittle' crystalline phases distributed within amorphous matrix.