• Title/Summary/Keyword: Extrusion Temperature

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Polymerization of Sugar by Extrusion

  • Hwang, Jae-Kwan;Kim, Chul-Jin;Chong-Tai, Kim
    • Preventive Nutrition and Food Science
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    • v.2 no.4
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    • pp.296-300
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    • 1997
  • Glucose syrup and lactose, mixed with citric acid as a polymerizing catalyst, was processed using twin screw extruder, in which 40 of L/D(length/diameter) ratio was designed to provide sufficient retention in extruder for polymerization of sugars. The polymerization yields of glucose syrup were 36.90%, 55.44% and 77.10% at 160, 180 and 20$0^{\circ}C$, respectively, while those of lactose were 26.45%, 38.16% and 45.86% at the same temperatures. Gel permeation chromatography exhibited that the higher molecular weight fractions were increased with extrusion temperature, which also led to increasing hydrodynamic intrinsic viscosity. Both uco-oligosaccharides and lacto-oligosaccharides produced by extrusion of glucose syrup and lactose were stable for thermal treatments over a wide range of pH3.0~11.0. In addition, $\alpha$-amylase and amyloglucosidase treatment of gluco-oligosaccharides did not affect the solution viscosity, indicating the random linkage rather than $\alpha$-1, 4 linkages of glucose and thus the potential applications as a dietary fiber. In this research it was clearly observed that twin screw extrusion can be successfully utilized to produce gluco-oligosaccharides and lacto-oligosaccharides rapidly and continuously in conjunction with selective control of polymerized composition.

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Prediction of Welding Pressure in the Non Steady state Porthole Die Extrusion of AI7003 Tubes (포트홀 다이 압출방식에 의한 AI7003 튜브의 접합강도예측)

  • Jo, Hyung-Ho;Lee, Sang-Gon;Lee, Seon-Bong;Kim, Byung-Min
    • Journal of the Korean Society for Precision Engineering
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    • v.18 no.7
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    • pp.179-185
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    • 2001
  • Porthole die extrusion is profitable to manufacture long tube with hollow section. The material through portholes is gathered within chamber and welded under high pressure. This weldability which classifies the quality of tube product is affected by several variables and die shape. But, porthole die extrusion has been executed on the experience of experts due to the complicated die assembly and complexity of metal flow. Analytic approaches that are useful in profitable die design and in the improvement of productivity are inevitably demanded. Therefore, the objective of this study is respectively to analyze the behavior of metal flow and to determine welding pressure of hot extrusion product according to the various billet temperature, bearing length and tube thickness by FE analysis and its results are compared with tube expanding tests.

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Extrusion of Spur Gear Using High-Energy Ball Milled Al-78Zn Powder (고에너지 볼밀법으로 제조된 Al-78Zn Powder를 이용한 스퍼기어의 압출)

  • Kim, Jin-Woo;Lee, Sang-Jin;Lee, Jung-Min;Kim, Byung-Min
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.33 no.4
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    • pp.440-446
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    • 2009
  • This paper was designed to fabricate the miniature spur gear with pitch circle of 2.25mm using extrusion process of a mechanically alloyed Al-78wt%Zn powder. The mechanical alloying of the powder particles were performed for ball milled times of 4h, 8h, 16 and 32h by the planetary ball milling. The mechanical properties of these alloyed powders, which were compacted and sintered-cylindrical preforms, were estimated using compression test. The results showed that the alloyed powder with average particle size of $10{\mu}m$ milled for 32h has the highest compressive(fractured) strength(288MPa). Extrusions of the miniature spur gear using the alloyed powder were carried out at different extrusion temperatures. Extrusion temperature of $300^{\circ}C$ provided the spur gear with the highest relative density and Vickers hardness and without any surface defects.

Effects of Initial Slug Design on the Earring of a Rectangular Battery Case During Impact Extrusion (충격압출 공정에서 초기 슬러그 디자인이 사각 배터리 케이스의 이어링에 미치는 영향 분석)

  • Lim, J. H.;Choi, S.;Chung, W. J.;Shin, J. H.;Lee, J.
    • Transactions of Materials Processing
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    • v.24 no.6
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    • pp.425-430
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    • 2015
  • In the current paper, the effects of initial slug design on the earring of an Al rectangular battery case manufactured by impact extrusion were studied. During impact extrusion, non-uniform metal flow between the long and the short sides of the battery case leads to earring, which is subsequently trimmed. Process parameters such as friction, aspect ratio of the battery case, the die shape and the forming temperature tend to induce earring because they cause greater non-uniform metal flow. Large aspect ratio of the battery case and high friction between slug and die can greatly affect the earring of a rectangular battery case. To make a rectangular battery case without earring, it is necessary to control metal flow uniformly during impact extrusion. One of the ways to reduce the earring is to control the metal flow of slug at the initial upsetting stage. To analyze the effects of the initial slug design on earring, FE analysis was conducted using DEFORM 3D. Two types of initial slug designs were evaluated where volume was removed along either the width or thickness directions. The results show that the initial slug design can be effective in adjusting the uniformity of metal flow.

Extrusion of Ginseng Root in Twin Screw Extruder: Pretreatment for Hydrolysis and Saccharification of Ginseng Extrudate

  • Han, Jae-Yoon;Kim, Mi-Hwan;Tie Jine;Solihin Budiasih W.;Ryu, Gi-Hyung
    • Preventive Nutrition and Food Science
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    • v.11 no.4
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    • pp.318-322
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    • 2006
  • The objective of this experiment was to investigate the effect of extrusion of ginseng roots in twin screw extruder on susceptibility of ginseng starch toward hydrolysis by ${\alpha}-amylase$ BAN 480L (Novozyme, Denmark) and cellulase Celluclast 150L and saccharification by amyloglucosidase AMG-E (Novozyme, Denmark). The extrusion was conducted at 22% and 30% moisture contents of feed at screw speed 300 rpm. Barrel temperature at zone 1 was adjusted at $100^{\circ}C$ and $120^{\circ}C$. The results showed that extrusion process improved the ginseng ${\alpha}-amylase$ susceptibility as compared to traditionally dried ginseng (white and red ginseng). Reducing sugar of hydrolyzed extruded samples was 2,500% of its initial concentration, whereas the reducing sugar of hydrolyzed non-extruded sample was only 200% of its initial concentration. However, addition of cellulase during liquefaction lowered the saccharification yield of both non-extruded and extruded samples as well.

A Study on the Characteristics of Aluminum Tube Hydroformed Products (알루미늄 튜브를 이용한 액압성형품 특성연구)

  • Yi, Hyae-Kyung;Lee, Gun-Yeop;Lee, Sung-Mun;Lee, Young-Seon;Moon, Young-Hoon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.32 no.11
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    • pp.1010-1015
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    • 2008
  • In this study, the characteristics of aluminum tube hydroformed products at different extrusion type and heat treatment conditions were investigated. For the investigation, as-extruded, full annealed and T6-treated Al 6061 tubes at different extrusion type were prepared. To evaluate the hydroformability, free bulge test was performed at room temperature to $300^{\circ}C$. Also mechanical properties of hydroformed products at various pre- and post-heat treatments were estimated by hexagonal prototype hydroforming test at $250^{\circ}C$. And the tensile test specimens were obtained from hexagonal prototype hydroformed tube. As a results, hydroformability of full annealed tube is $5{\sim}8%$ higher than that of extruded and T6-treated tube. The tensile strength and elongation of T6-post heat treated indirect extrusion tube were more than 330MPa and 12%, respectively. However, T6 pre treated hydroformed product represents high strength, 330MPa and low elongation, 8%. Therefore, Hydroformability of Al6061 tube showed similar value for both extrusion types. However flow stress of direct tube showed $20{\sim}50MPa$ lower value than indirect tube.

Isotropy Control of 7075 Al Wrought Alloy by Thixoextrusion (반용융 압출에 의한 A7075 합금의 등방성 제어)

  • Yoon, Young-Ok;Kim, Shae-K.
    • Journal of Korea Foundry Society
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    • v.30 no.6
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    • pp.210-216
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    • 2010
  • The aim of this study is to characterize a thixoextruded 7075 Al wrought alloy bar in terms of its isotropic behavior through the optical microscope, mechanical test and electron back scattered diffraction. It is also discussed of the extrudability improvement for 7075 Al wrought alloy by thixoextrusion, with emphasis on controlling thixoextrusion parameters. Hot extrusion shows that the maximum extrusion pressure depends on their characteristics in terms of flow stress and hot workability. In the contrary, thixoextrusion demonstrates that the maximum extrusion pressure is almost uniform regardless of the experimental parameters, such as initial ram speed, die bearing length and thixoextrusion temperature. The hot extruded microstructures become elongated to extrusion direction, while the thixoextruded microstructures are isotropic and homogeneously distributed due to the existence of liquid phase between solid grains during the process. The grain refinement due to dynamic recrystallization during thixoextrusion has been also occurred. Subsequent recrystallization would lead to the strengthening of mechanical properties, as observed in the study. The important point is that the values of tensile, yield strength and elongation of the thixoextruded bar without plastic deformation are similar to those of the hot extruded bar with severe plastic deformation.

Analysis of Whole Grains Extrusion by Response Surface Methodology (반응표면분석법에 의한 전곡립의 압출성형공정 분석)

  • Shin, Hae-Hun;Park, Bo-Sun;Lee, Hye-Lim;Choi, Moon-Jung;Hwang, Jae-Kwan
    • Korean Journal of Food Science and Technology
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    • v.33 no.6
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    • pp.686-692
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    • 2001
  • The effects of extrusion on solubilization of brown rice, glutinuous rice, barley and job's tear were analyzed by response surface methodology (RSM). Solubilization of whole grains by extrusion was characterized in terms of water solubility index (WSI), concentration of water soluble polysaccharides (C) and intrinsic viscosity $([\eta])$. Considering both concentration and intrinsic viscosity, a dimensionless target parameter $([\eta])$ was also included for analysing the extrusion effects on cereal extrusion. Response surface methodology analysis showed that the moisture content was the most significant contributor among screw speed, temperature and moisture content affecting the solubilizing phenomena of cereals processed with extrusion. Brown rice was not showed the significant relationship on $([\eta])$ because $([\eta])$ was more affected by intrinsic viscosity. The critical point of whole grains extrusion except brown rice was corresponded to screw speed of 300 rpm, moisture content of 20% and temperature of $120^{\circ}C$.

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Extraction Yield of Extruded Ginseng and Granulation of Its Extracts by Cold Extrusion-Spheronization (압출성형 수삼의 추출수율과 추출물의 저온압출 구형과립화)

  • ;J.P. Remon
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.33 no.5
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    • pp.899-904
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    • 2004
  • The objectives of the experiment were to examine the effects of extrusion process variables on the yield of extruded ginseng extract and to determine the effect of ratio of extruded ginseng extract and microcrystalline cellulose on characteristics of spheronized granules by cold extrusion-spheronization process. Extrusion process variables observed were feed moisture (15, 22, 29%), die temperature (90 110 13$0^{\circ}C$) and screw speed (150 200, 250 rpm). The results showed that moisture content of dried ginseng significantly affected extraction yield (P<0.05). The less moisture content of the feed resulted in the higher yield of the extract. Moisture content of 15%, screw speed of 250 rpm and die temperature of 13$0^{\circ}C$ gave the highest yield of ginseng extract. Mean extraction yield of extruded ginseng using hot water extraction was greatly improved by extrusion process The extract yield of extruded ginseng was 43.5% which was higher than that of red ginseng (38.3%) and white ginseng (29.0%) produced by traditional process. It was possible to make from the mixture of microcrystalline cellulose (200 g) mixed with different concentration of 200 mL solution (0, 5, 20, 30 40 50 60% of ginseng extract with 59.2% dry solid) by using cold extrusion spheronization. When the concentration of ginseng extract Increased, the granulation yield was improved but friability and compression index were reduced. Ginseng extract such as saponin was completely released from spheronized granules in distilled water within 10 min. It can be concluded that spheroniged granule with ginseng extract could be packed in gelatin capsule since granules Possessed proper physical properties and quick release of saponin.

Room and High Temperature Deformation Behaviors and Estimation on Formability of Zr-based Bulk Metallic Glass Composite (Zr-Nb-Cu-Ni-Al 비정질 복합 재료의 변형거동과 성형성)

  • Jun, H.J.;Lee, K.S.;Kuhn, U.;Eckert, J.;Chang, Y.W.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.10a
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    • pp.199-202
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    • 2008
  • In this study, we investigated the thermal properties of $Zr_{66.4}Nb_{6.4}Cu_{10.5}Ni_{8.7}Al_{8.0}$ by using a differential scanning calorimeter (DSC), and then analyzed the composition of dendrite phase by using X-ray diffraction (XRD). A series of uniaxial compression tests has been performed under the strain rates between $10^{-5}/s$ and $10^{-2}/s$ at room temperature and near SLR. This BMGC has higher high temperature strength than other Zr-based monolithic BMGs because in-situ formed crystalline phases hinder a feasible viscous flow of amorphous matrix. Warm formability is also estimated by laboratory-scale extrusion test within supercooled liquid region. It was found that BMGC has poor formability compared with nother Zr-based bulk metallic glass composite presumably due to large volume fraction of 'brittle' crystalline phases distributed within amorphous matrix.

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