• Title/Summary/Keyword: Extractives

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Uitlization of Ligno-cellulosic Biomass(I) - Manufacture of Explosion Apparatus and Composition of Explode Wood - (목질계(木質系) Biomass의 이용(利用)(I) - 폭쇄장치(爆碎裝置)의 제작(製作) 및 폭쇄재(爆碎材)의 조성(組成) -)

  • Lee, Jong-Yoon;Park, Sang-Jin;Lee, Seok-Gun;Cho, Nam-Seok;Chang, Jun-Pok;Ann, Byung-Jo
    • Journal of the Korean Wood Science and Technology
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    • v.17 no.2
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    • pp.65-73
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    • 1989
  • Steam explosion process is an efficient pretreatment method for sparating and utilizing wood main components has attracted attention in utilization of ligno-cellulosic biomass. In order to obtain the effective pretreatment condition. this study was made explosion apparatus. examined the composition. extraction of exploded wood. Wood chips of pine(Pinus densiflora oak (Quercus serrata) and birch wood (Belula platyphylla var. japonica) were treated with a high pressure steam(20-30 kg/$cm^2$, 2-6 minutes). The results can be summarized as follow; In analysis of exploded wood(EXW). It was found arabinose residues rapidly decreased with increasing of steaming time and pressure. Extractives of EXW with sodium hydroxide increased with increasing of steaming-time and- pressure especially extractives 1% sodium hydroxide has higher than other extracted method extractives of hard wood(oak, birch) has higher than pine wood. In EXW extracted with sodium hydroxide and methanol lignin was partially delignified alkali extraction was more delignified than methanol extraction hardwood than pine wood.

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Comparative Study of Processed (Shodhit) and Unprocessed Seeds of 'Gunja'-Abrus precatorius L.

  • Gautam, D.N. Singh;Singh, P.N.;Mehrotra, Shanta
    • Natural Product Sciences
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    • v.5 no.3
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    • pp.127-133
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    • 1999
  • 'Gunja' is attributable to the plant Abrus precatorius L. (Leguminosae). Three forms with red, brown and another with white seeds are known to occur in this species and are employed for different therapeutic uses viz. as purgative, emetic, aphrodisiac, tonic and also as an abortifacient. According to some Ayurvedic literature the seeds are poisonous and should be given to the patients after proper processing ('Shodhan'). A comparative study of various phytochemical parameters, namely, percentage of successive extractives, total proteins, tannins, total ash and acid insoluble ash of these three forms of the processed (with cow's milk and Kanji) and unprocessed seeds was done. TLC and densitometric scanning of successive extractives was also carried out to serve as markers for processed and unprocessed seeds. The percentage of proteins, tannins, alcohol and water soluble extractives decreased in the processed material. Besides, their acute toxicity, CNS activity were also studied in albino mice and it was found that white seeds are more toxic as compared to the red and brown. The toxic effect was reduced with the processing. Further, the 'Kanji' processed seeds are less toxic than the milk processed one.

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Extractives from the Needles of Torreya (벼자나무 잎의 추출성분)

  • Kim, Jin-Kyu;Bae, Young-Soo
    • Journal of the Korean Wood Science and Technology
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    • v.29 no.4
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    • pp.53-59
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    • 2001
  • The needles of torreya(Torreya nucifera S. et Z) were collected, extracted with acetone-$H_2O$(7:3, v/v), fractionated with hexane, chloroform and ethylacetate, and freeze dried to give some dark brown powder. The ethylacetate soluble mixture was chromatographed on a Sephadex LH-20 column using a series of aqueous methanol and ethanol-hexane mixture as eluents. Most of the needle extractives were flavan and its methyl ether compounds such as (+)-catechin, (-)-epicatechin, (+)-gallocatechin, (-)-epigallocatechin, 3'-O-methyl-(+)-catechin and 3'-O-methyl-(-)-epicatechin including protocatechuic acid, one of benzoic acids. $^1H$- and $^{13}C$-NMR, NOE and CI-MS analyses were performed to elucidate the structures of the isolated compounds.

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Studies on the Development of Traditional Korean Golden Varnish(Hwangchil)(I) - Anatomical Characterisitics and Chemical Composition of Wood and Exudates of Hwangchil-namu(Dendropanax morbifera)- (전통 황칠 도료 개발에 관한 연구(I) - 황칠나무와 황칠액의 해부학적 특성과 화학적 조성-)

  • Lim, Kie-Pyo;Kim, Yoon-Soo;Chung, Woo-Yang
    • Journal of the Korean Wood Science and Technology
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    • v.25 no.3
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    • pp.24-28
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    • 1997
  • As a way to revive the traditional technology of Korean golden varnish(Hwangchill), the exudates of D. morbifera, this study was carried out at first to investigate the anatomical characteristics and the chemical composition of D. morbifera stems and their exudates. Trees of more than 20 years old were harvested at Wando and Jejudo islands in the southwestern part of Korean peninsula during different physiological seasons of winter, spring, and summer, The results obtained are as follows: 1. In the anatomical aspect of wood, Hwangchil woods is ring-porous wood, has alternate inter-vessel pittings and horizontal intercellular canal in xylem. 2. In the chemical aspect of wood and bark, the general compositions appeared hot to differ from those of other hardwoods, and ash and alcohol-benzene extractives showed little increase with the increase of atmospheric temperature of harvesting season. 3. In the solvent-sequential extraction of bark, wood and exudate, the exudates was extracted up to 80% by ether, but the bark and wood contained a very small amount of ether extractives, about 2% in the bark and 0.5% in the xylem.

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Extermination of Rice Weevils of Kraft Paper Containing Garlic Extractives and Pine Leaf Powder (마늘 추출액과 솔잎 가루를 이용한 크라프트지의 쌀벌레 방제 효과)

  • Kim, Chul-Hwan;Sin, Tae-Gi;Kim, Gyeong-Yun;Jung, Ho-Gyeong;Huh, Jeong-Soo
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.39 no.3
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    • pp.60-69
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    • 2007
  • This study developed rice packaging paper with exterminating performance against rice weevils such as Tenebroides mauritanicus and Sitophilus oryzae. The exterminating performance of packaging paper was given by treatment of garlic extractives and pine-leaf powder, respectively. For the exterminating test, rice weevils were put in petri dish containing non-treated packaging paper and functional packaging paper for twenty days. Right after being put in the petri dish, the rice weevils moved fast toward the area in the non-treated paper escaping from that in the functional paper. The lethality of the rice weevils on the functional paper reached over 50 per cent. The physical properties of the functional packaging paper were rarely changed in spite of treatment of the exterminating agents.

A Study on the Natural Insectifuge for Food Wrapping Corrugated Board Using Tree Extractives (수목 추출성분을 이용한 식품포장용 골판지 천연 방충처리제 개발)

  • 배영수
    • Journal of Korea Foresty Energy
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    • v.20 no.2
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    • pp.9-19
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    • 2001
  • This study was carried out to investigate natural insectifuge materials from tree extractives in order to substitute for organic synthetic insecticides for food wrapping corrugated board. Tree samples were collected, extracted, fractionated with hexane, $CH_2Cl_2$, ethylacetate(EtOAc) and $H_2O$, and then freezed dried for further study. EtOAc or $H_2O$ fractions were chromatographed on a Sephadex LH-20 column for isolation and purification, and the isolated compounds were characterized by spectroscopic tools such as NMR and MS. Crude extractives of EtOAc and $H_2O$ fractions were added to the printing ink for corrugated board with the concentration of 2% or 3% based on the weight of the ink, then the prepared ink was printed on the corrugated board to be used for evasion test using larva of indian meal moth(Plodia interpunctella(Hubner)). Robtin, dihydrorobinetin and leucorobinetinidin were isolated from the wood extractives of black locust(Robinia pseudoacacia) and the bark of poplar(Populus alba $\times$ glandulosa) contained many kinds of compounds such as (+)-catechin, naringenin, aromadendrin, eriodictyol, sakuranetin and its glycoside, taxifolin, neosaturanin, salireposide, p-coumaric acid and aesculin. Much of (+)-catechin was isolated from the bark extractives of willow(Salix koreensis) in addition to (+)-gallocatechin and p-coumaric acid and the bark of weeping willow(Salix babylonica) also contained (+)-catechin, (+)-gallocatechin, dihydromyricetin and myricetin.

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Pharmacognostic Evaluation of Curcuma aeurigenosa Roxb.

  • Srivastava, Sharad;Nitin, Chitranshi;Srivastava, Sanjay;Dan, Mathew;Rawat, A.K.S.;Pushpangadan, Palpu
    • Natural Product Sciences
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    • v.12 no.3
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    • pp.162-165
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    • 2006
  • Curcuma aeruginosa Roxb. (FamilyZingeberaceae), commonly known as 'pink and blue giner' is widely used in Indian system of medicine since time immemorial. The plant is found well in wild habitat and cultivated in southern India. The plant is distinguished by red corolla lobes and ferruginous or greenish-blue rhizome. Rhizoma is used medicinally as anti-diarrheal, anti-fungal; external use as astringent for wounds. A detailed pharmacognostic evaluation of its rhizome showed total ash 6.1%, acid insoluble ash 1.20%, alcohol soluble extractives 3.70% , water soluble extractives 14.50%, sugar 20.93%, starch 41.85%, and tannins 0.68%. Oh hydro distillation, the rhizomes and sessile tubers yielded 0.17% oil.

Antimicrobial activity and cytotoxicity of Eclipta prostrata

  • Rahman, Mohammad S.;Rashid, Mohammad A.
    • Advances in Traditional Medicine
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    • v.8 no.1
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    • pp.47-52
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    • 2008
  • The plant Eclipta prostrata, a member of the Compositae family, has folkloric reputation of being used as a medicinal agent in Bangladesh. In the present investigation, attempt was taken to explore the antimicrobial potency and cytotoxicity of its extractives and purified compounds. The methanolic extract of the whole plant, its n-hexane, carbon tetrachloride, chloroform, aqueous soluble fractions and two purified compounds, eclalbasaponin I (1) and II (2), obtained from Eclipta prostrata were subjected to screening for inhibition of microbial growth by the disc diffusion method at 300 and 100 ${\mu}g$/disc for extracts and pure compounds, respectively. In this case, the carbon tetrachloride and chloroform soluble fractions of the methanolic extract appeared very potent in terms of both zone of inhibition and spectrum of activity. However, all the extractives were also subjected to brine shrimp lethality bioassay for preliminary cytotoxicity evaluation. Here, the carbon tetrachloride soluble fraction of methanolic extract revealed the strongest cytotoxicity having $LC_{50}$ of 1.318 ${\mu}g$/ml.

Studies on the Wood Extractivies (II) - Chemical Structures of Flavonoid Compound - (목재추출성분(木材抽出成分)에 관(關)한 연구(硏究) (II) - 플라보노이드화합물(化合物)의 화학구조(化學構造) -)

  • Hwang, Byung-Ho;Choi, Hyong-Joo;Yoon, Byung-Ho
    • Journal of the Korean Wood Science and Technology
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    • v.13 no.4
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    • pp.58-66
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    • 1985
  • In order to elucidate chemical structure of the wood extractives, softwood (Pinus koraiensis Sieb. et Zucc.) meal was extracted with 95% ethanol at room temperature for 72 hours. The extract was fractionated with organic solvents such as n-hexane, ether, ethylacetate, and acetone. From the n-hexane and ether soluble fraction of the wood extractives, four flavonoid compounds were isolated and identified as 5-hydroxy-7-methoxyflavone (I), 5-methoxy-7-hydroxyflavone (II), 5-hydroxy-7-methoxyflavanone (III), and 5-methoxy-7-hydroxyflavanone (IV) by UV, IR, $^1$H-NMR spectroscopy and MS spectrometry.

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