• Title/Summary/Keyword: Extraction system

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A study of thermolysis of irradiated diamide-containing extraction systems with nitric acid

  • Srvortsov, I.V.;Belova, E.V.;Sokolov, I.P.;Rodin, A.V.;Stefanovsky, S.V.;Mysoedov, B.F.
    • Nuclear Engineering and Technology
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    • v.50 no.8
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    • pp.1421-1425
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    • 2018
  • The dynamics of gas release at thermal oxidation of extraction systems on the basis of diamides of dicarbonic acids in fluorinated sulphones with 14 mol/L $HNO_3$ was investigated. The effect of preirradiation of the mixtures with accelerated electrons on the kinetics of their thermolysis was determined. The mixtures were heated in an autoclave at temperatures of 170 and $200^{\circ}C$ and irradiated using an electron accelerator to absorbed doses of 0.1, 0.5, and 1.0 MGy. It has been shown that no conditions for autocatalytic oxidation at thermolysis of extraction mixtures irradiated up to a dose of 1 MGy were developed.

Quantitative analysis of cordycepin in Cordyceps militaris under different extraction methods

  • Choi, Jungwon;Paje, Leo Adrianne;Kwon, Baekjun;Noh, Jaekyu;Lee, Sanghyun
    • Journal of Applied Biological Chemistry
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    • v.64 no.2
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    • pp.153-158
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    • 2021
  • Cordyceps militaris (CM) is one of the most important medicinal mushrooms known to possess various biological activities. Cordycepin (CP) is a bioactive compound present in the fruiting bodies of CM and is known to have anti-tumor, anti-metastatic immunomodulatory and anti-inflammatory activities. In this study, we aim to analyze CP quantitatively under various CM extraction conditions. CP was measured using high-performance liquid chromatography, quantified using a reversed phase column using a gradient elution system of water and acetonitrile, and detected with a UV absorbance wavelength of 260 nm. The CP content of CM was the highest in 100% ethanol extract of the fruiting bodies and 60% ethanol extract of the mycelium. This study provides an efficient analysis method to determine the optimal extraction conditions for CP that can be used as a basis for developing functional foods and pharmaceutical products derived from CM.

Simultaneous determination of saikosaponin derivatives in Bupleurum falcatum by HPLC-ELSD analysis using different extraction methods

  • Choi, Jungwon;Kim, Juree;Kang, Sam Sik;Lee, Sanghyun
    • Journal of Applied Biological Chemistry
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    • v.64 no.1
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    • pp.57-61
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    • 2021
  • Saikosaponin derivatives such as saikosaponins A, B1, B2, B3, B4, C, and D present in Bupleurum falcatum were analyzed by a high performance liquid chromatograph equipped with an evaporative light scattering detector, using different extraction solvents (water and 70% ethanol). The samples were injected into a YMC Pack Pro C18 column and separated using a gradient elution system with a mobile phase composed of acetonitrile and water at a flow rate of 1.1 mL/min. The content of saikosaponin derivatives was higher in 70% ethanol extract than in water extract. This study provides an efficient analytical method for determining the optimal conditions for extraction of saikosaponin derivatives, which can be used as a basis for development of functional foods and pharmaceutical products from B. falcatum.

A Simple Method for Determining Residual p-arsanilic Acid in Aquatic Products using EDTA-Assisted Solvent Extraction and LC-MRM

  • Min Kyeong Kwon;Ye Bin Shin;Young Min Kim;Jin Hwan Kim;Ji Seong Kim;Yong Seok Choi
    • Mass Spectrometry Letters
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    • v.14 no.2
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    • pp.36-41
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    • 2023
  • A simple method was developed to determine residual p-arsanilic acid (ASA), an organo-arsenic compound used as a feed additive, in aquatic products (eel, halibut, and shrimp) using EDTA-assisted solvent extraction and LC-MRM. The method was successfully validated in terms of specificity, linearity (coefficient of determination ≥ 0.995), accuracy (recovery or R, 72.72-78.73%), precision (the relative standard deviation of R, 2.08-6.98%), and sensitivity (the lower limit of quantitation, 5 ppb) according to CODEX guidelines (CAC-GL 71-2009). The use of EDTA in the extraction solvent and water with a suitable pH modifier as the reconstitution solvent may be the key factors for successful results. This is the first method that can be used for monitoring residual ASA in aquatic products using LC-MRM and could contribute to establishing a better aquatic product safety management system.

Surgical Extraction in Patient with McCune-Albright Syndrome: A Case Report

  • Dohee Kim;Jeong Joon Han;Hoon Myoung
    • Journal of Korean Dental Science
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    • v.16 no.1
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    • pp.99-103
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    • 2023
  • McCune-Albright syndrome (MAS) is a disease with clinical features such as fibrous dysplasia in which normal bone tissue is replaced with abnormal fibrous tissue, abnormalities in the endocrine system, and cafe-au-lait spots on the skin. Although MAS patients are generally known to have reduced bone healing ability, postoperative healing after invasive surgical extraction is still not clearly known due to its relatively rare occurrence. In this report, a 25-year-old female patient, who had been diagnosed with MAS and had a history of abnormal bone healing after fractures of her extremities, underwent surgical extraction of the mandibular third molar with surrounding bone removal. Postoperatively, the patient showed favorable soft tissue and bone healing at the surgical site without abnormal findings such as newly developed fibro-osseous lesions, postoperative infection, or osteomyelitis.

Online Digit Recognition using Start and End Point

  • Shim, Jae-chang;Ansari, Md Israfil
    • Journal of Multimedia Information System
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    • v.4 no.1
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    • pp.39-42
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    • 2017
  • Communication between human and machine is having been researched from last few decades and still it's a challenging task because human behavior is unpredictable. When it comes on handwritten digits almost each human has their own writing style. Handwritten digit recognition plays an important role, especially in the courtesy amounts on bank checks, postal code on mail address etc. In our study, we proposed an efficient feature extraction system for recognizing single digit number drawn by mouse or by a finger on a screen. Our proposed method combines basic image processing and reading the strokes of a line drawn. It is very simple and easy to implement in various platform as compare to the system which required high system configuration. This system has been designed, implemented, and tested successfully.

Extraction of Factors Effecting Surface Roughness Using the System of Experiments in the Ultra-precision Mirror Surface Finishing (실험 계획법을 이용한 초정밀 경면 연마 가공에서 표면 거칠기에 영향을 미치는 인자의 검출)

  • 배명일;김홍배;김기수;남궁석
    • Journal of the Korean Society for Precision Engineering
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    • v.15 no.2
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    • pp.53-60
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    • 1998
  • In this study, it is experimented to find factors effecting surface roughness using the system of experiments. in the mirror surface finishing system. (1) The film feed and oscillation frequency in $40{\mu}m$ abrasive film, grinding speed in $30{\mu}m$, and machining time in $15{\mu}m$15 are the main factors effecting the surface roughness. (2) Applying the optimal finishing condition to $40{\mu}m$, $30{\mu}m$, $15{\mu}m$ abrasive finishing film in sequence, it is possible to obtian about Ra 10 nm surface roughness on SM45C workpiece. (3) Application of the system of experments to the micro abrasive grain film finishing was very effective method in the extraction of main factor and optimal condition.

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Remediation of Contaminated Railroad Soils using by Hybrid Pilot System (Hybrid Pilot System을 이용한 철도 오염토양 복원)

  • 박덕신
    • Journal of the Korean Society for Railway
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    • v.3 no.3
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    • pp.101-108
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    • 2000
  • In this study, we tested hybrid pilot system combined with soil vapor extraction and bioventing methods on the contaminated railroad soil. So, we found out the remediability and operating conditions. Air permeability(k) and gas phase(O$_2$/CO$_2$/VOCs) level trend are very important to determine the remediation rate of the contaminated sites. Throughout hybrid pilot test on different conditions, the range of air permeability(k) was 1985∼1194 darcy. The tests results in hybrid system was appropriate on this test sites, and the suitable injection air flow rate was 3.5㎥/hr. So, we suggested a basic data for the remediation and management of contaminated railroad soil.

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Sasang Constitution Classification System by Morphological Feature Extraction of Facial Images

  • Lee, Hye-Lim;Cho, Jin-Soo
    • Journal of the Korea Society of Computer and Information
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    • v.20 no.8
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    • pp.15-21
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    • 2015
  • This study proposed a Sasang constitution classification system that can increase the objectivity and reliability of Sasang constitution diagnosis using the image of frontal face, in order to solve problems in the subjective classification of Sasang constitution based on Sasang constitution specialists' experiences. For classification, characteristics indicating the shapes of the eyes, nose, mouth and chin were defined, and such characteristics were extracted using the morphological statistic analysis of face images. Then, Sasang constitution was classified through a SVM (Support Vector Machine) classifier using the extracted characteristics as its input, and according to the results of experiment, the proposed system showed a correct recognition rate of 93.33%. Different from existing systems that designate characteristic points directly, this system showed a high correct recognition rate and therefore it is expected to be useful as a more objective Sasang constitution classification system.

Microwave-Assisted Extraction of Effective Constituents from Ginseng (마이크로파를 이용한 인삼으로부터 유효성분의 추출)

  • Lee, Dong-Won;Park, Young-Sin;Kim, Dok-Chan
    • Applied Chemistry for Engineering
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    • v.16 no.3
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    • pp.427-433
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    • 2005
  • The use of the microwave-assisted process for the extraction of effective constituents from ginseng was investigated at various operating conditions. The influence of solvent (ethanol-water, 50% v/v) to ginseng ratio, particle size and applied microwave power on the efficiency of extraction was examined. The microwave extraction system used was custom manufactured so that the intensity of microwave may be varied by using anode-voltage controller. It was found that the ratio of 6 : 1 (vol/mass) gave a good extraction efficiency. Small particle size gave high yield but it caused difficulties in the separation of solvent from the sludge. The higher power was no guarantee of the efficient extraction yield. The more important factor than the employed power was the adequate temperature under sufficient contact time. Using deionized-water as swelling agent, the degree of swelling of ginseng by microwave heating and conventional heating in water-bath was also studied. It was observed that the microwave heating enhanced the swelling much more than the conventional heating. It is believed that this enhanced swelling was responsible for the rapid microwave-assisted extraction rate.