• 제목/요약/키워드: Extraction Process

검색결과 2,471건 처리시간 0.041초

마그네슘함량이 높은 니켈 laterite광으로부터 습식공정에 의한 니켈과 코발트 회수 (Recovery of Nickel and Cobalt by a Hydrometallurgical Process from Nickel Laterite Ore with High Magnesium Content)

  • 이만승;김상배;최영윤;채종귀
    • 대한금속재료학회지
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    • 제48권1호
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    • pp.62-70
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    • 2010
  • Leaching and solvent extraction experiments have been performed to develop a hydrometallurgical process for the recovery of nickel and cobalt from nickel laterite ore with high magnesium content. Most of the nickel and magnesium in the laterite ore dissolved at leaching conditions of $80^{\circ}C$ and 100 g/L sulfuric acid concentration. while half of the cobalt and iron were leached at the same conditions. Solvent extraction experiments were carried out with D2EHPA and saponifed D2EHPA from a synthetic solution containing Ni, Co, and Mg. The extraction percentage of Co, Mg. and Ni by D2EHPA was very low in a pH range of 4.4 to 7.3. while the extraction percentage sharply increased by using saponified D2EHPA. The stripping percentage of the metals from the saponified D2EHPA increased with sulfuric acid concentration and reached 99.9% at 1 M $H_2SO_4$ solution.

초임계 이산화탄소와 에탄올 보조용매를 이용한 포도씨로부터의 페놀성 화합물의 추출 (Extraction of Phenolic Compounds from grape Seed Using Supercritical $CO_2$ and Ethanol as a Co-solvent)

  • 이원영;장규섭;최용희
    • 한국식품저장유통학회지
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    • 제7권2호
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    • pp.177-183
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    • 2000
  • A supercritical fluid extraction was performed for the extraction of phenolics from grape seeds which up to now have been discarded. The optimum condition for extraction process was predicted through response surface methodology using central composit experimental design. The extraction amount of grape seed phenolics was increased by increasing extraction temperature, pressure, and concentration of co-solvent (ethanol). The optimum extraction conditions were 84.83$^{\circ}$C, 51.50MPa and 1.27% ethanol. The yield of phenolics using SFE was higher with 3 folds than ethanol and 4 folds than hexane but less than 80% methanol. In the respects of food poisoning, the approved solvents were restricted to ethanol and hexane. So, SFE for extraction of phenolics could be powerful alternative method for solvent extraction.

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효소처리에 의한 천연 마카음료 개발을 위한 최적 추출 조건 (Optimization of Maca (Lepidium meyenii) Extraction for Natural Beverage Development using Enzyme Treatment)

  • 김정아;임무혁
    • 한국식생활문화학회지
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    • 제34권3호
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    • pp.361-368
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    • 2019
  • The purpose of this study was to establish the best optimized extraction condition for the optimal development of fresh maca beverage using low temperature extraction and enzyme treatment. Low temperatures were applied to prevent heat-related nutritional loss during the extraction process. Best extraction conditions were investigated based on the ratio of maca to water, the ratio of enzymes, extraction temperature and time, and agitation. The optimal enzyme conditions were also examined after the treatment of cellulase:pectinase mixture to maintain the original color and flavor, as well as to increase the extraction yield. When cellulase:pectinase was 1:1, the extraction rate ranged from 77.84 to 79.29%. In addition, the best extraction rate was found when maca was mixed with twice volume of water and incubated at $45^{\circ}C$ ($84.05{\pm}0.32%$) with 90 rpm ($87.13{\pm}0.46%$) agitation for 3 hours ($84.73{\pm}0.29%$). Furthermore, sensory evaluation showed a high score in flavor, sweetness, and overall acceptability after adding 3% jujube concentrate into a fresh maca beverage.

Multi-response Optimization for Unfertilized Corn Silk Extraction Against Phytochemical Contents and Bio-activities

  • Lim, Ji Eun;Kim, Sun Lim;Kang, Hyeon Jung;Kim, Woo Kyoung;Kim, Myung Hwan
    • 산업식품공학
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    • 제21권3호
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    • pp.256-266
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    • 2017
  • This study was designed to optimize ethanol extraction process of unfertilized corn silk (UCS) to maximize phytochemical contents and bioactivities. The response surface methodology (RSM) with central composite design (CCD) was employed to obtain the optimal extraction conditions. The influence of ethanol concentration, extraction temperature and extraction time on total polyphenol contents, total flavonoid contents, maysin contents, 2,2-diphenyl-1-picrylhydrazyl(DPPH) radical scavenging activities and tyrosinase inhibition were analyzed. For all dependable variables, the most significant factor was ethanol concentration followed by extraction temperature and extraction time. The following optimum conditions were determined by simultaneous optimization of several responses with the Derringer's desirability function using the numerical optimization function of the Design-Expert program: ethanol concentration 80.45%, extraction temperature $53.49^{\circ}C$, and extraction time 4.95 h. Under these conditions, the predicted values of total polyphenol contents, total flavonoid contents, maysin contents, DPPH radical scavenging activity and tyrosinase inhibition were $2758.74{\mu}g\;GAE/g$ dried sample, $1520.81{\mu}g\;QUE/g$ dried sample, 810.26 mg/100g dried sample, 56.86% and 43.49%, respectively, and the overall desirability (D) was 0.74.

잉크의 중첩인쇄순서에 기인하는 색차의 광학적 해석에 관한 연구 (A Study on Optical Analysis of the Color Difference Caused by the Overprinting Sequence of Ink)

  • 강상훈
    • 한국인쇄학회지
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    • 제16권1호
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    • pp.39-53
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    • 1998
  • The extraction rate of ginger from Korean-grown ginger root with supercritical carbon dioxide was measured as a function of flow rate of supercritical carbon dioxide, particle size, temperature and pressure. the extraction rate increased as the particle size decreased due to a decrease in the diffusion path. The extraction rate were independent of flow rate of supercritical carbon dioxide in a plot of ginger oil yield versus extraction time. This indicated that the extraction process is controlled by intraparticle diffusion within a particle of ginger root. In the case of temperature and pressure effect, the experimental results showed that the extraction rate decreased with an increase in temperature and increased with an increase in pressure.

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담배 주맥 바이오매스의 압착추출특성 연구 (Study on the Mechanical Extraction Properties of Tobacco Stem Biomass)

  • 성용주;한영림;이문수
    • 펄프종이기술
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    • 제40권2호
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    • pp.65-72
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    • 2008
  • This work evaluated the extractability of tobacco stem biomass for the papermaking type Reconstituted Tobacco Sheet(RTS). The effects of the soaking conditions on the hydration of stem biomass and the effects of the hydrated state on the mechanical extraction were investigated. In order to simulate the mechanical expression process of a papermaking type RTS mill, for example, the screw press process, the novel mechanical pressing analyzer was developed for this study. The hydration of stem biomass by soaking process was greatly affected by the soaking time and the soaking temperature. The longer soaking time and the higher soaking temperature resulted in the higher hydrated stem biomass. Since the higher hydrated stem had more combined water in the inner structure and resulted in the more flexible structure, the higher hydrated stem leaded to the more compressed filter cake and the higher water contents in the filter cake after the mechanical pressing. The pilot pulping experiments showed the difference in hydration and extractability between burley and bright tobacco stem. The bulkier structure of the burley stem resulted in the faster hydration by pilot pulping and leaded to the larger reduction in water soluble components. And the hydration process showed the major influence on the separation efficiency of water soluble components.

GSIS를 이용한 토지 특성의 자동추출에 관한 연구 (A study on the Auto-extraction of Land Characterictics Using a GSIS)

  • 박성규;임승현;박정남;조기성
    • 대한공간정보학회지
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    • 제6권2호
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    • pp.59-67
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    • 1998
  • 본 연구는 GSIS를 이용한 토지 특성의 자동추출에 관한 연구로서 현지 조사로서 토지 특성추출을 하고 있는 토지특성조사업무 전반에 걸친 과정을 GSIS를 이용하여 자동 수행할 수 있는 알고리즘 및 자동산정 프로그램개발을 통하여 토지특성 추출의 효율적인 방법을 모색하였다. 이를 위하여 일반적인 토지특성 항목 중 선행 연구에서는 접근하지 못했던 필지의 형상, 고저, 방위 및 도로접면조건 등의 항목에 대한 특성을 GSIS를 이용하여 효과적으로 자동추출할 수 있는 방안을 제시하였다. 본 연구에서 제시한 GSIS를 이용한 토지특성자동추출기법을 현행공시지가산정업무에 적용할 경우 종래 방법보다 효과적이고 과학적인 방법으로 지가산정업무 및 택지조성사업을 실시한 후 조성택지에 대한 가격산정등에 크게 기여할 것이라 판단된다.

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초임계 추출 공정의 압력 및 유량 제어계 구성 (Design of pressure and flowrate control systems for a supercritical extraction process)

  • 김원철;김홍식;이광순
    • 제어로봇시스템학회:학술대회논문집
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    • 제어로봇시스템학회 1988년도 한국자동제어학술회의논문집(국내학술편); 한국전력공사연수원, 서울; 21-22 Oct. 1988
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    • pp.471-475
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    • 1988
  • Pressure and flowrate control systems for a supercritical extraction process are designed and analyzed. To do this, the dynamic model was first set up using the performance equations of control valves, CO2 compressor and the state equation of the supercritical fluid. Using this model, optimum pairs of manipulated and controlled variable which give least steady stat interaction are determined though the relative gain analysis.

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토양증기추출공정 중 오염물의 거동평가기법에 관한 연구

  • 조현정;권태순;양중석;양지원
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2003년도 추계학술발표회
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    • pp.354-355
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    • 2003
  • In this study, a risk-based cleanup approach using the leaching potential was suggested for the soil vapor extraction (SVE) process. A multi-component model was adopted with local equilibrium assumption (LEA), and Raoult's law was applied to estimate the leaching potential for BTEX. Finally, a risk analysis was conducted based on the leaching pontential calculated. To complete the feasibility of this approach, more investigations and discussions will be required in future.

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해조류 파래로부터 지질 추출에 미치는 전처리 방법의 영향 (Effect of Pretreatment Method on Lipid Extraction from Enteromorpha intestinalis)

  • 정귀택;박돈희
    • KSBB Journal
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    • 제29권1호
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    • pp.22-28
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    • 2014
  • In this study, we investigate the effect of pretreatment method on lipid extraction from Enteromorpha intestinalis using physical, thermo-chemical, and enzymatic process such as ultrasonication, high temperature treatment, freezing, microwave irradiation, osmotic shock, pH shock, homogenizing, and enzymatic treatment. In pretreatment with separated lipid extraction, the high extraction yield was obtained by high temperature treatment ($121^{\circ}C$ for 5 min) with 0.1 N HCl, which is 1.4 times higher than that of control. In pretreatment with direct lipid extraction, the high extraction yields were obtained by 0.1 N HCl pretreatment, microwave irradiation (700W, 1 min with twice), and 10% NaCl pretreatment, which is 1.45 times higher than that of control. In the result of enzymatic pretreatment with 17 kinds of enzymes, Cellic CTec II showed the high extraction yield of 5.3%, and which is 1.9 times higher than that of control. Moreover, the extraction yield was increased by the increase of enzyme amounts. In 10% enzyme amount, about 5.8% yield was obtained.