• Title/Summary/Keyword: Experimental conditions

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Optimization of Benzene Synthesis for Radicarbon Dating by Response Surface Method

  • 나경임;강형태;김승원;최상원;김윤섭;김순옥
    • Bulletin of the Korean Chemical Society
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    • v.18 no.7
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    • pp.703-706
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    • 1997
  • Response surface method was applied to the predicting optimum conditions of benzene synthesis for radiocarbon dating. The weight of carbon dioxide, the temperature of lithium container for producing acetylene and the activation temperature of catalyst which was used for the cyclization of acetylene to benzene were used as experimental factors. The yields of benzene synthesis were measured from twelve experiments which were carried out under various experimental conditions. The polynomial equation was obtained by using three experimental factors and yields. The validity of polynomial equation was confirmed by comparing the calculated yields with the experimental ones.

Optimum process conditions for supercritical fluid and co-solvents process for the etching, rinsing and drying of MEMS-wafers (초임계 유체와 공용매를 이용한 미세전자기계시스템 웨이퍼의 식각, 세정을 위한 최적공정조건)

  • Noh, Seong Rae;You, Seong-sik
    • Journal of the Semiconductor & Display Technology
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    • v.16 no.3
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    • pp.41-46
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    • 2017
  • This study aims to select suitable co-solvents and to obtain optimal process conditions in order to improve process efficiency and productivity through experimental results obtained under various experimental conditions for the etching and rinsing process using liquid carbon dioxide and supercritical carbon dioxide. Acetone was confirmed to be effective through basic experiments and used as the etching solution for MEMS-wafer etching in this study. In the case of using liquid carbon dioxide as the solvent and acetone as the etching solution, these two components were not mixed well and showed a phase separation. Liquid carbon dioxide in the lower layer interfered with contact between acetone and Mems-wafer during etching, and the results after rinsing and drying were not good. Based on the results obtained under various experimental conditions, the optimum process for treating MEMS-wafer using supercritical CO2 as the solvent, acetone as the etching solution, and methanol as the rinsing solution was set up, and MEMS-wafer without stiction can be obtained by continuous etching, rinsing and drying process. In addition, the amount of the etching solution (acetone) and the cleaning liquid (methanol) compared to the initial experimental values can be greatly reduced through optimization of process conditions.

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The Correlation between Manufacturing Parameters and friction Characteristics of Automotive Friction Materials by Taguchi Robust Experimental Design (다구찌 로버스트 실험계획법에 의한 자동차용 마찰재의 성형조건과 마찰특성과의 상관관계에 환한 연구)

  • Kim, Kwang-Seok;Jang, Ho
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1999.11a
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    • pp.225-232
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    • 1999
  • The effect of manufacturing parameters such as molding and curing conditions on friction characteristics of friction materials was studied using a pad-on-disk type friction tester. Friction materials containing 15 ingredients were investigated for an optimal manufacturing condition for the best friction characteristics employing Taguchi robust experimental design. The main effects were different for mechanical properties and friction characteristics and were strongly influenced by manufacturing conditions. An optimum manufacturing condition was obtained to achieve the best friction characteristics concerning mechanical properties(hardness, porosity, wear resistance), friction stability, and change of rotor temperature.

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In-Situ Performance Test of a Wet Surface Finned-Tube Evaporator of an Air Source Heat Pump (공랭식 열펌프의 습표면 핀-관 증발기의 현장 성능 시험)

  • 백영진;장영수;김영일
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.13 no.9
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    • pp.818-826
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    • 2001
  • In this study, in-situ performance test of a wet surface finned-tube evaporator of an air source heat pump which has a rating capacity of 20RT is carried out. Since test conditions, such as indoor and outdoor air conditions cannot be controlled to satisfy the standard test conditions, experiments are done with the inlet air conditions as they exist, From the experimental data, air side heat and mass transfer coefficients were calculated by the well known heat and mass transfer analogy and tube-by-tube method. since current procedure underpredicted the experimental sensible heat factor(SHF), a proper empirical parameter was introduced to predict the experimental data with satisfactory results. This study provides the method of evaluating the heat and mass transfer coefficients of a wet surface finned-tube evaporator of which in-situ performance test in necessary.

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Effects of optimal operating conditions on 2-stage injection PCCI diesel engine using Response Surface Methodology (반응 표면법을 이용한 2 단 분사 PCCI 디젤엔진의 운전조건의 영향도 평가에 대한 연구)

  • Lee, Jae-Hyeon;Kim, Hyung-Min;Lee, Ki-Hyung
    • Proceedings of the KSME Conference
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    • 2008.11b
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    • pp.3044-3048
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    • 2008
  • It is well known that Premixed Charge Compression Ignition (PCCI) diesel engines according to many technologies such a change in injection timing, multiple injection strategy, cooled EGR, intake charging and SCV have the potential to achieve homogeneous mixture in the cylinder which result in lower NOx and PM as well as performance improvements. This may generate merely the infinite number of experimental conditions. The use of Response Surface Methodology (RSM) technique can considerably pull down the number of experimental set and time demand. This paper presents the effects of both fuel injection and engine operation conditions on the combustion and emissions in the PCCI diesel engine system. The experimental results have revealed that a change in fuel injection timing and multiple injection strategy along with various operating conditions affect the combustion, emissions and BSFC characteristics in the PCCI engine.

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Analysis of a Wet Surface Finned-tube Evaporator of an Air Source Heat Pump

  • Baik, Young-Jin;Chang, Young-Soo;Kim, Young-Il
    • International Journal of Air-Conditioning and Refrigeration
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    • v.10 no.4
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    • pp.211-219
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    • 2002
  • In this study, in-situ performance test of a wet surface finned-tube evaporator of an air source heat pump which has a rating capacity of 20 RT is carried out. Since test conditions, such as indoor and outdoor air conditions cannot be controlled to satisfy the standard test conditions, experiments are done with the inlet air conditions as they exist. From the experimental data, air side heat and mass transfer coefficients were calculated by the well known heat and mass transfer analogy and tube-by-tube method. Since current procedure underpredicted the experimental sensible heat factor (SHF), a proper empirical parameter was introduced to predict the experimental data with satisfactory results. This study provides the method of evaluating the heat and mass transfer coefficients of a wet surface finned-tube evaporator of which in-situ performance test is necessary.

Experimental Investigation of Porous Bearings Under Different Lubricant and Lubricating Conditions

  • Durak, Ertugrul
    • Journal of Mechanical Science and Technology
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    • v.17 no.9
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    • pp.1276-1286
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    • 2003
  • The performance of porous bearing under different lubricants and lubricating conditions was experimentally investigated in this study. In order to carry out the experiments, a new test rig was designed to determine the tribological properties of based sintered bronze journal bearings that were manufactured by powder metallurgy (P/M) techniques. To determine the effects of lubricating conditions with and without oil supplement (OS) on the tribological characteristics of these bearings under static loading and periodic loadings, some experiments were carried out using different lubricants. In the tests, pure base oil (SAE 20W50), two fully formulated commercial engine oils (SAE20W50) and lubricating oils with commercial additive concentration ratio of 3% were used. The worn surfaces of test bearings were examined using optical microscopy. Experimental results showed that the change in friction coefficient was more stable and in smaller magnitude under static loading than that of periodic loading. In addition, the friction coefficient and the wear rate conducted with base oil resulted in higher values than those of fully formulated oils with and without OS lubricating conditions. The experimental results obtained in this study indicated that the correct selection of lubricant and suitable running conditions were very important on the tribological characteristics of porous bearings.

An Improved Global Maximum Power Point Tracking Scheme under Partial Shading Conditions

  • Kim, Rae-Young;Kim, Jun-Ho
    • Journal of international Conference on Electrical Machines and Systems
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    • v.2 no.1
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    • pp.65-68
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    • 2013
  • A photovoltaic array exhibits several local and single global maximum power points under partial shading conditions. To track the global maximum power point precisely, a novel global maximum power point tracking scheme is proposed in this paper. In the proposed scheme, robustness of the tracking performance has been improved by enhancing searching profile. In addition, the paper addresses the tracking failure condition, and provides the experimental verification with several simulation and experimental results.

A Study of Measurement and Analysis of Flow Distribution in a Close-Coupled Catalytic Converter (근접장착식 촉매장치의 유동분포 측정 및 해석에 관한 연구)

  • Jo, Yong-Seok;Kim, Deuk-Sang;Ju, Yeong-Cheol
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.25 no.4
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    • pp.533-539
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    • 2001
  • In this study, results from an experimental and numerical study of flow distribution in a close-coupled catalytic converter (CCC) are presented. The experiments were carried out using a glow measurement system. Flow distribution at the exit of the first monolith in the CCC was measured using a pitot tube under steady and transient flow conditions. Numerical analysis was done using a CF D code at the same test conditions, and the results were compared with the experimental results. Experimental results showed that the uniformity index of exhaust gas velocity decreases as Reynolds number increases. Under the steady flow conditions, flow through each exhaust pipe concentrates on a small region of the monolith. Under the transient flow conditions, flow through each exhaust pipe with the engine firing order interacts with each other to spread the flow over the monolith face. The numerical analysis results support the experimental results, and help explain the flow pattern in the entry region of the CCC.

Wall slip of vaseline in steady shear rheometry

  • Song, Ki-Won;Chang, Gap-Shik;Koo, Ja-Seung
    • Korea-Australia Rheology Journal
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    • v.15 no.2
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    • pp.55-61
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    • 2003
  • The steady shear flow properties of vaseline generally used as a base of the pharmaceutical dosage forms were studied in the consideration of wall slip phenomenon. The purpose of this study was to show that how slip may affect the experimental steady-state flow curves of semisolid ointment bases and to discuss the ways to eliminate (or minimize) wall slip effect in a rotational rheometer. Using both a strain-controlled ARES rheometer and a stress-controlled AR1000 rheometer, the steady shear flow behavior was investigated with various experimental conditions ; the surface roughness, sample preparation, plate diameter, gap size, shearing time, and loading methods were varied. A stress-controlled rheometer was suitable for investigating the flow behavior of semisolid ointment bases which show severe wall slip effects. In the conditions of parallel plates attached with sand paper, treated sample, smaller diameter fixture, larger gap size, shorter shearing time, and normal force control loading method, the wall slip effects could be minimized. A critical shear stress for the onset of slip was extended to above 10,000 dyne/$\textrm{cm}^2$. The wall slip effects could not be perfectly eliminated by any experimental conditions. However, the slip was delayed to higher value of shear stress by selecting proper fixture properties and experimental conditions.