• 제목/요약/키워드: Evaporation Coating

검색결과 167건 처리시간 0.027초

뿜칠피복재를 사용한 고강도 콘크리트 부재의 내화피복두께에 관한 실험적 연구 (An Experimental Study on the Fireproof Covering Thickness of High Strength Concrete Members with Spray Coating)

  • 이태규
    • 한국화재소방학회논문지
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    • 제24권4호
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    • pp.41-46
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    • 2010
  • 고강도 콘크리트는 대형 사회기반 구조물로서 많이 활용되고 있다. 고강도 콘크리트는 우수한 재료적 성능과 내구성을 확보하고 있지만 반면에 화재에 대한 급작스러운 폭렬현상으로 인하여 구조적인 문제를 야기시키기도 한다. 따라서 본 연구에서는 콘크리트 피복두께에 추가하여 내화피복재를 사용함으로써 내화피복두께에 따른 콘크리트의 내화성능을 평가하고 최적의 내화피복두께를 산정하는 실험적 연구를 수행하였다. 내화피복재를 10mm 간격으로 증가시키면서 실험을 수행한 결과 콘크리트의 내화성능이 크게 향상됨을 볼 수 있었으며, 최적의 내화피복두께는 약 1~3mm로 산정되었다. 또한 폭렬에 의하여 급작스러운 콘크리트 내부의 온도상승 이후 기화열에 의한 열손실로 완만하게 온도가 상승되는 현상이 실험적으로 관측되었다. PP 섬유는 약 $200^{\circ}C$ 부근에서 용해되어 고온에서는 빈 채널만 남게 되므로 내부 증기압을 저감시켜주는 역할도 관측되었다.

Pd 나노입자가 코팅된 β-Bi2O3 나노와이어의 NO2 검출 특성 (NO2 Sensing Properties of β-Bi2O3 Nanowires Sensor Coated with Pd Nanoparticles)

  • 박성훈;강우승
    • 한국표면공학회지
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    • 제48권6호
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    • pp.303-308
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    • 2015
  • Pd-functionalized ${\beta}-Bi_2O_3$ nanowires are synthesized by thermal evaporation of Bi powder using VLS mechanism followed by Pd coating and annealing. In this study, sensing properties of Pd-functionalized ${\beta}-Bi_2O_3$ nanowires sensor to selected concentrations of $NO_2$ gas were examined. Scanning electron microscopy showed that the nanowires with diameters in a range of 100 - 200 nm and lengths of up to a few tens of micrometers. Transmission electron microscopy and X-ray diffraction confirmed that the products corresponded to the nanowires of ${\beta}-Bi_2O_3$ crystals and Pd nanoparticles. Pd-functionalized ${\beta}-Bi_2O_3$ nanowires sensor showed an enhanced sensing performance to $NO_2$ gas compared to as-synthesized ${\beta}-Bi_2O_3$ nanowires sensor. As synthesized and Pd-functionalized ${\beta}-Bi_2O_3$ nanowire sensors showed responses of 178% - 338% and 196% - 535% at $300^{\circ}C$, respectively, to 0.05 - 2 ppm $NO_2$. In addition, the underlying mechanism of the enhancement of the sensing properties of ${\beta}-Bi_2O_3$ nanowires by Pd-functionalization is discussed.

An Organic Electrophosphorescent Device Driven by All-Organic Thin-Film Transistor using Polymeric Gate Insulator

  • Pyo, S.W.;Shim, J.H.;Kim, Y.K.
    • Journal of Information Display
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    • 제4권2호
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    • pp.1-6
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    • 2003
  • In this paper, we demonstrate that the organic electrophosphorescent device is driven by the organic thin film transistor with spin-coated photoacryl gate insulator. It was found that electrical output characteristics in our organic thin film transistors using the staggered-inverted top-contact structure showed the non-saturated slope in the saturation region and the sub-threshold nonlinearity in the triode region, where we obtained the maximum power luminance that was about 90 $cd/m^2$. Field effect mobility, threshold voltage, and on-off current ratio in 0.45 ${\mu}m$ thick gate dielectric layer were 0.17 $cm^2/Vs$, -7 V, and $10^6$ , respectively. In order to form polyimide as a gate insulator, vapor deposition polymerization process was also introduced instead of spin-coating process, where polyimide film was co-deposited by high-vacuum thermal evaporation from 4,4'-oxydiphthalic anhydride (ODPA) and 4,4'-oxydianiline (ODA) and cured at 150${\sqsubset}$for 1hr. It was also found that field effect mobility, threshold voltage, on-off current ratio, and sub-threshold slope with 0.45 ${\mu}m$ thick gate dielectric films were 0.134 $cm^2/Vs$, -7 V, and $10^6$ A/A, and 1 V/decade, respectively.

메모리소자 응용을 위한 초박막의 제작 및 특성 평가 (Evaluation of the fabrications and properties of ultra-thin film for memory device application)

  • 정상현;최행철;김재현;박상진;김광호
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2006년도 하계학술대회 논문집 Vol.7
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    • pp.169-170
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    • 2006
  • In this study, ultra thin films of ferroelectric vinylidene fluoride-trifluoroethylene (VF2-TrFE) copolymer were fabricated on degenerated Si (n+, $0.002\;{\Omega}{\cdot}cm$) using by spin coating method. A 1~5 wt% diluted solution of purified vinylidene fluoride-trifluoroethylene (VF2:TrFE=70:30) in a dimethylformamide (DMF) solvent were prepared and deposited on silicon wafers at a spin rate of 2000~5000rpm for 30 seconds. After annealing in a vacuum ambient at $200^{\circ}C$ for 60 min, upper gold electrodes were deposited by vacuum evaporation for electrical measurement. X-ray diffraction results showed that the VF2-TrFE films on Si substrates had $\beta$-phase of copolymer structures. The capacitance on $n^+$-Si(100) wafer showed hysteresis behavior like a butterfly shape and this result indicates clearly that the dielectric films have ferroelectric properties. The typical measured remnant polarization (2Pr) and coercive filed (EC) values measured using a computer controlled a RT-66A standardized ferroelectric test system (Radiant Technologies) were about $0.54\;C/cm^2$ and 172 kV/cm, respectively, in an applied electric field of ${\pm}0.75\;MV/cm$.

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A/R 코팅 변화에 따른 200MHz AOM의 laser damage threshold 증가 (Laser Damage Threshold Increase of A/R Coating Films for 200MHz AOM)

  • 김용훈;이항훈;이진호;박영준;박정호
    • 한국재료학회지
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    • 제7권3호
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    • pp.213-217
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    • 1997
  • 200MHz 응향광변조기 (AOM: Acousto-Optic Modulator)는 제 2고조파(SHG: Second Harmonic Generation)녹색 레이저와 함께 DVDR(Digital Video Disk Recorder)에 적용되어 고밀도 광기록용으로 사용되었다. 이러한 고밀도 광기록 장치로써 사용되기 위해서는 고출력 레이저의 사용이 필수적이며, 레이저 빔이 통과하는 각 광학 소자들의 코팅막은 고출력 레이저 빔에 대해 높은 레이저 damage threshold를 가져야 한다. AOM의 음향공학재료로 사용되는 $TeO_{2}$단결정에 코팅막의 종류 및 증착조건을 변화시키며 E-beam 증착법으로 A/R코팅 시편을 준비하였다. 0.55W의 입력 power를 갖는Ar레이저를 사용하여 코팅의 광손상 정도를 확인하였다. $AI_{2}O_{3}$막에 비해 $ZrO_{2}$$SiO_{2}$막을 사용한 경우 레이저 damage threshold는 크게 향상되었다. 또한 AOM모듈을 제작 후 구동회로와 연결하여 약 20mW의 SHG power를 입력시키며 출력 power long term안정성을 측정하였다.

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Analysis on Design and Fabrication of High-diffraction-efficiency Multilayer Dielectric Gratings

  • Cho, Hyun-Ju;Lee, Kwang-Hyun;Kim, Sang-In;Lee, Jung-Hwan;Kim, Hyun-Tae;Kim, Won-Sik;Kim, Dong Hwan;Lee, Yong-Soo;Kim, Seoyoung;Kim, Tae Young;Hwangbo, Chang Kwon
    • Current Optics and Photonics
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    • 제2권2호
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    • pp.125-133
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    • 2018
  • We report an in-depth analysis of the design and fabrication of multilayer dielectric (MLD) diffraction gratings for spectral beam combining at a wavelength of 1055 nm. The design involves a near-Littrow grating and a modal analysis for high diffraction efficiency. A range of wavelengths, grating periods, and angles of incidence were examined for the near-Littrow grating, for the $0^{th}$ and $-1^{st}$ diffraction orders only. A modal method was then used to investigate the effect of the duty cycle on the effective indices of the grating modes, and the depth of the grating was determined for only the $-1^{st}$-order diffraction. The design parameters of the grating and the matching layer thickness between grating and MLD reflector were refined for high diffraction efficiency, using the finite-difference time-domain (FDTD) method. A high reflector was deposited by electron-beam evaporation, and a grating structure was fabricated by photolithography and reactive-ion etching. The diffraction efficiency and laser-induced damage threshold of the fabricated MLD diffraction gratings were measured, and the diffraction efficiency was compared with the design's value.

Capillarity-Driven Self-Assembly of Silver Nanowires-Coated Fibers for Flexible and Stretchable Conductor

  • Li, Yi;Chen, Jun;Han, Xiao;Li, Yinghui;Zhang, Ziqiang;Ma, Yanwen
    • Nano
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    • 제13권12호
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    • pp.1850146.1-1850146.9
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    • 2018
  • The rapid development of smart textiles requires the large-scale fabrication of conductive fibers. In this study, we develop a simple, scalable and low-cost capillary-driven self-assembly method to prepare conductive fibers with uniform morphology, high conductivity and good mechanical strength. Fiber-shaped flexible and stretchable conductors are obtained by coating highly conductive and flexible silver nanowires (Ag NWs) on the surfaces of yarn and PDMS fibers through evaporation-induced flow and capillary-driven self-assembly, which is proven by the in situ optical microscopic observation. The density of Ag NWs and linear resistance of the conductive fibers could be regulated by tuning the assembly cycles. A linear resistance of $1.4{\Omega}/cm$ could be achieved for the Ag NWs-coated nylon, which increases only 8% after 200 bending cycle, demonstrating high flexibility and mechanical stability. The flexible and stretchable conductive fibers have great potential for the application in wearable devices.

Browning technology for shiitake in sawdust using LED source

  • Koo, Jinmo;Lee, Sang-Hwa;Lee, Sung-Hak;Park, Woo-Ram;Hwang, Jae Soon;Kim, Minkyeong;Jun, Hyungseo;Jung, Hee-Young;Jo, Woo-Sik
    • 한국버섯학회지
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    • 제16권4호
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    • pp.331-333
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    • 2018
  • The incorporation of Shiitake culture into sawdust is a widely utilized technique that can assist in reducing the cost and time consumption associated with oak cultivation. In sawdust cultivation, browning of the surface mycelia is an important stage with respect to the utility and longevity of the sawdust media. Surface browning forms a protective coating on the substrate, which can inhibit the invasion of pathogens and suppress water evaporation. Several different light sources (red LED, white LED, blue LED, and fluorescent light) were used and the intensity of illumination was carefully controlled (1.5, 10.5, $20.5{\mu}mol/m^2s$ for LEDs and 10, 100, 300 lux for the fluorescent light) to induce browning. The light sources were regulated via a 1 h on/off cycle in a controlled room environment at a temperature of $20^{\circ}C$, 60% humidity, and 1200 ppm $CO_2$ concentration for 60days. The browning effect varied depending on the source and the intensity of illumination. This effect was most effectively induced at $1.5{\mu}mol/m^2s$ for the red and blue LEDs. All light sources induced less browning at the highest intensity of illumination. This indicates that intensity values higher than $20.5{\mu}mol/m^2s$ in the case of the LEDs and 300 lux for the fluorescent light are not effective. After harvesting of the fruit bodies, we measured the weight, length, and width of the pileus and stipe in addition to their chromaticity and hardness. Treatment with $1.5{\mu}mol/m^2s$ blue LED produced the best harvest with the highest average chromaticity, weight (21.2 g), stipe length (30.8 mm), and hardness (377.9 g), with a fine length and width of the pileus.

섬유 고분자의 수분 흡수에 따른 에너지 하베스팅 발전 소자 및 이를 위한 카본 블랙의 효율적인 코팅법 (Energy Harvesting System according to Moisture Absorption of Textile and Efficient Coating Method as a Carbon Black)

  • 최승진;채주원;이상오;이재웅
    • 한국염색가공학회지
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    • 제33권4호
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    • pp.280-287
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    • 2021
  • Generating electricity by using water in many energy harvesting system is due to their simplicity, sustainability and eco-friendliness. Evaporation-driven moist-electric generators (EMEGs) are an emergent technology and show great potential for harvesting clean energy. In this study, we report a transpiration driven electro kinetic power generator (TEPG) that utilize capillary flow of water in an asymmetrically wetted cotton fabric coated with carbon black. When water droplets encounter this textile EMEG, the water flows spontaneously under capillary action without requiring an external power supply. First carbon black sonicated and dispersed well in three different solvent system such as dimethylformamide (DMF), sodiumdedecylbenzenesulfonate (SDBS-anionic surfactant) and cetyltrimethylammoniumbromide (CTAB-cationic surfactant). A knitted cotton/PET fabric was coated with carbon black by conventional pad method. Cotton/PET fabrics were immersed and stuttered well in these three different systems and then transferred to an autoclave at 120 ℃ for 15 minutes. Cotton/PET fabric treated with carbon black dispersed in DMF solvent generated maximum current up to 5 µA on a small piece of sample (2 µL/min of water can induce constant electric output for more than 286 hours). This study is high value for designing of electric generator to harvest clean energy constantly.

Ti3O5/SiO2 다층박막를 이용한 협대역 칼라투과필터 제작 및 특성연구 (The Fabrication and Characteristic for Narrow-band Pass Color-filter Deposited by Ti3O5/SiO2 Multilayer)

  • 박문찬;고견채;이화자
    • 한국안광학회지
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    • 제16권4호
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    • pp.357-362
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    • 2011
  • 목적: $Ti_3O_5$$SiO_2$를 이용하여 중심파장이 500 nm에서 반치폭이 약 12 nm이고 투과율이 99%인 협대역 칼라투과필터를 제작하고, 이 칼라필터의 박막 특성을 연구하고자 한다. 방법: 두께 800 nm인 $Ti_3O_5$박막과 $SiO_2$박막의 투과율로부터 박막의 광학상수 n(굴절률)과 k(소멸계수)를 구하였고, Essential Macleod program을 이용하여 중심파장이 500 nm에서 반치폭이 약 12 nm이고 투과율이 99%인 협대역 칼라투과필터의 필터층과 AR 코팅층을 설계하였다. 또 한 electron beam evaporation 장치를 이용하여 $Ti_3O_5/SiO_2$ 다층막 칼라필터을 만든 후, 분광광도계를 이용하여 투과율을 측정하였고, SEM 사진에 의한 칼라필터의 단면으로부터 칼라필터의 박막두께와 층수를 알 수 있었고, XPS분석으로부터 박막 성분을 분석하였다. 결과: 칼라필터의 AR 코팅층의 최적조건은 6층으로 [air$|SiO_2(90)|Ti_3O_5(36)|SiO_2(5)|Ti_3O_5(73)|SiO_2(30)|Ti_3O_5(15)|$ glass]이며, 반치폭이 12 nm인 칼라필터의 필터층의 최적조건은 41층으로 [air$|SiO_2(20)|Ti_3O_5(64)|SiO_2(102)|Ti_3O_5(66)|SiO_2(112)|Ti_3O_5(74)|SiO_2(120)|Ti_3O_5(68)|SiO_2(123)|Ti_3O_5(80)|SiO_2(109)|Ti_3O_5(70)|SiO_2(105)|Ti_3O_5(62)|SiO_2(99)|Ti_3O_5(63)|SiO_2(98)|Ti_3O_5(51)|SiO_2(60)|Ti_3O_5(42)|SiO_2(113)|Ti_3O_5(88)|SiO_2(116)|Ti_3O_5(68)|SiO_2(89)|Ti_3O_5(49)|SiO_2(77)|Ti_3O_5(48)|SiO_2(84)|Ti_3O_5(51)|SiO_2(85)|Ti_3O_5(48)|SiO_2(59)|Ti_3O_5(34)|SiO_2(71)|Ti_3O_5(44)|SiO_2(65)|Ti_3O_5(45)|SiO_2(81)|Ti_3O_5(52)|SiO_2(88)|$ glass] 이었다. 위의 데이터를 이용하여 제작한 칼라필터는 SEM 사진에 의해 41층으로 확인되었으며, XPS 분석에 의해 $SiO_2$층이 맨 위층이며 $Ti_3O_5$층과 교번인 다층막으로 형성돼 있으며, $Ti_3O_5$박막 형성 시 TiO2 박막과 $Ti_3O_5$박막이 섞여 형성됨을 알 수 있었다. 결론: 41층의 $Ti_3O_5/SiO_2$ 다층박막을 이용하여 12 nm 반치폭을 갖으며 500 nm 중심파장에서 투과율은 99%인 협대역 칼라투과필터를 제작하였으며, 이 칼라필터는 $Ti_3O_5$박막 형성 시 TiO2 박막과 $Ti_3O_5$박막이 섞여 형성됨을 알 수 있었다.