• Title/Summary/Keyword: Environmental stability test

Search Result 499, Processing Time 0.036 seconds

The Homogeneity and Short-term Stability Test of Bio-matrix Reference Material for Total Mercury Analysis of Freshwater Fish (담수 어류 총수은 분석용 생물 표준물질 균질성, 안정성 시험평가)

  • Lee, Soo Yong;Lee, Jangho;Chung, David;Shim, Kyu-Young;Lee, Ha-Eun;Park, Ki-Wan
    • Journal of Environmental Science International
    • /
    • v.28 no.11
    • /
    • pp.1033-1040
    • /
    • 2019
  • The National Environmental Specimen Bank (NESB) has set up a plan to develop reference materials in the facility for assuring analytical quality and validating analytical methods for its monitoring samples. Some of the crucial characteristics that reference materials must consist of are homogeneity and stability of both intra and inter-bottles. In this study, we examined the homogeneity and stability of cryogenically-milled muscle samples, from Common Carp (Cyprinus carpio) for total mercury. Homogeneity was tested using ANOVA analysis and regression analysis was used to test short-term stability. The variations of total mercury concentration did not significantly differ between the intra and the inter-bottle (F=0.8, p=0.37). Additionally, relative standard deviation of the total mercury concentration showed low values (2.28%). For the short-term stability test, total mercury variations were not statistically significant as demonstrated by the result of the regression analysis (F ratio = 3.11, p = 0.18). This suggests that the cryogenic-milling process has statistically proven the degree of homogeneity and short-term stability for samples of carp muscles in the chemical analysis for total mercury.

Evaluation of Homogeneity and Stability of Korean Mussel (Mytilus coruscus) Standards for Cadmium Analysis (카드뮴 분석용 홍합(Mytilus coruscus) 표준물질의 균질성 및 안정성 시험평가)

  • Lee, Ha-Eun;Lee, Jangho;Chung, David;Lee, Soo Yong;Park, Ki-Wan;Shim, Kyu-Young
    • Journal of Environmental Science International
    • /
    • v.28 no.11
    • /
    • pp.1041-1045
    • /
    • 2019
  • In this study, the KS A ISO Guide 35 was applied to develop analytical standards for heavy metal cadmium using the Korean mussel (Mytilus coruscus) and to evaluate the homogeneity and stability of the sample. Some of the crucial characteristics that reference materials must consist include homogeneity and stability of both intra- and inter-bottles. We tested homogeneity using ANOVA analysis and short-term stability using regression analysis. The variations of cadmium concentrations did not significantly differ between intra- and inter-bottles (F=0.41, p=0.90). For short-term stability verification, cadmium analysis results were not statistically significant as a result of the regression analysis (significance F=0.51, p=0.53). This suggests that we can not dismiss the null hypothesis that there is no significant variation in concentrations of cadmium over time. These results indicated that the cryogenic-milling process has statistically proven the short-term stability for materials from mussels in the chemical analysis of cadmium. Therefore, we propose that the Korean mussel's reference material developed for the proficiency test could be used as a tool to evaluate reliability and consistency in laboratories.

An Experimental Study on IMO 2nd Generation Stability Assessment in Dead Ship Condition of 13K Chemical Tanker (13K Chemical Tanker의 기관 제어 불능상태 IMO 2세대 안정성 평가에 관한 실험적 연구)

  • Lee, Sang-Beom;Moon, Byung-Young
    • Journal of the Society of Naval Architects of Korea
    • /
    • v.59 no.2
    • /
    • pp.89-95
    • /
    • 2022
  • The stability of the existing ships has been evaluated through numerical calculations in the steady-state, but recently the IMO proposed a new stability assessment criteria that the stability is evaluated in the state in which environmental loads from such as waves and wind act like the loads under actual ship operating conditions. In this study, IMO 2nd generation stability assessment method and procedure were summarized for the dead ship condition, and Direct Stability Assessment (DSA) was performed on 13K chemical tanker through basin model test. The model test is performed in the ocean engineering basin to implement wave and wind loads, and environmental conditions for waves were set height and period of the incident wave, considering the regular wave and wind generation range reproducible in the ocean engineering basin. In addition, to consider the effect of wind speed, the Beaufort Scale for wind speed was applied in the model test.

Case Study of Environmental Segmental Retaining Wall(SRW) Using Greenstone Block (환경친화적 블록식 보강토옹벽의 설계 및 시공사례연구)

  • Han, Jung-Geun
    • Journal of the Korean Society of Environmental Restoration Technology
    • /
    • v.7 no.6
    • /
    • pp.19-28
    • /
    • 2004
  • Segmental Retaining Wall(SRW) has been variously applying in Civil and Architecture construction. Recently, the application of environmental element in all type's structures came to essential requirement, and the construction cases of retaining wall using reinforced soil and block are more increased than the past. But, this trend more widely was spread environmental element as landscape work for the backside of reinforced retaining wall as well as block itself. New environmental block, Greenstone Block, developed to apply of this tendency. The retaining wall system using Greenstone can be environmental constructing at both block itself and backside of retaining wall. The material tests, the axial compressive strength test of block and bending test of fiber-pipe, exercised to design and construction of vertical SRW, which were satisfied NCMA standard. Through this procedure, Rewall (ver 1.0) was developed, which can be automation design of SRW including internal stability, external stability and local stability. And these can be considered setback of retaining wall, as well the examples of vertical retaining wall using block presented to satisfying the follows; strength of reinforced geotextile, height of retaining wall, surcharge, types of backfill and groundwater level etc. Many problems investigated on after or before of construction were due to local failure, insufficiency of bearing capacity and groundwater level. Especially, the local failure was many occurred to during compaction or after construction, and the cases of SRW construction is similar to the results of model test on vertical SRW.

Real-time hybrid substructuring of a base isolated building considering robust stability and performance analysis

  • Avci, Muammer;Botelho, Rui M.;Christenson, Richard
    • Smart Structures and Systems
    • /
    • v.25 no.2
    • /
    • pp.155-167
    • /
    • 2020
  • This paper demonstrates a real-time hybrid substructuring (RTHS) shake table test to evaluate the seismic performance of a base isolated building. Since RTHS involves a feedback loop in the test implementation, the frequency dependent magnitude and inherent time delay of the actuator dynamics can introduce inaccuracy and instability. The paper presents a robust stability and performance analysis method for the RTHS test. The robust stability method involves casting the actuator dynamics as a multiplicative uncertainty and applying the small gain theorem to derive the sufficient conditions for robust stability and performance. The attractive feature of this robust stability and performance analysis method is that it accommodates linearized modeled or measured frequency response functions for both the physical substructure and actuator dynamics. Significant experimental research has been conducted on base isolators and dampers toward developing high fidelity numerical models. Shake table testing, where the building superstructure is tested while the isolation layer is numerically modeled, can allow for a range of isolation strategies to be examined for a single shake table experiment. Further, recent concerns in base isolation for long period, long duration earthquakes necessitate adding damping at the isolation layer, which can allow higher frequency energy to be transmitted into the superstructure and can result in damage to structural and nonstructural components that can be difficult to numerically model and accurately predict. As such, physical testing of the superstructure while numerically modeling the isolation layer may be desired. The RTHS approach has been previously proposed for base isolated buildings, however, to date it has not been conducted on a base isolated structure isolated at the ground level and where the isolation layer itself is numerically simulated. This configuration provides multiple challenges in the RTHS stability associated with higher physical substructure frequencies and a low numerical to physical mass ratio. This paper demonstrates a base isolated RTHS test and the robust stability and performance analysis necessary to ensure the stability and accuracy. The tests consist of a scaled idealized 4-story superstructure building model placed directly onto a shake table and the isolation layer simulated in MATLAB/Simulink using a dSpace real-time controller.

Stability of Environmental Disposition Validated Through a Shout Term Education -The Effect of 'Interior Design History' Course on Students' Environmental Disposition- (단기교육 영향에 대한 실내환경적 성향의 안정성 규명연구 -'실내디자인 양식사' 수강경험이 실내환경적 성향에 미치는 영향-)

  • 이연숙;이선미;이경은;민지희
    • Korean Institute of Interior Design Journal
    • /
    • no.20
    • /
    • pp.3-9
    • /
    • 1999
  • The purpose of this study was to verify the stability of environmental disposition through analyzing the short term effect of the 'Interior Design History' course on students environmental dispositions, especially their interior image preferences toward traditional/modern, female/masculine, and simple/complex characteristics. The pre-test post-test control group experimental design was used. The independent variable was the experience of the Interior Design History course, and the dependent variable was environmental disposition measured by IIPS(Interior Image Preference Scale). The measurements were done at both beginning and end of fall semester, 1997. Subjects were using 71 undergraduate students of Drafting course (control group) and 35 undergraduate students of Interior Design History course (experimental group) at Y University. Data were analyzed using frequency, percentage, mean, and F-test through ANOCOVA. This research revealed no effect of the Interior Design History course on students interior environmental dispositions. The stability of those environmental dispositions and also the validity of the IIPS were proved.

  • PDF

A Study on the Development of Soil-based PTMs for Analysis of BTEX (BTEX 분석용 토양 숙련도 표준시료(PTMs) 개발에 관한 연구)

  • Lee, Minhyo;Lee, Guntaek;Lee, Bupyoel;Lee, Wonseok;Kim, Gumhee;Hong, Sukyoung
    • Journal of Soil and Groundwater Environment
    • /
    • v.18 no.5
    • /
    • pp.15-25
    • /
    • 2013
  • In this study, two kinds of soil-based proficiency testing materials (PTMs), NICE-012L and NICE-012R were prepared and certified for Benzen, Toluene, Etylbenzene and Xylene with evaluation of uncertainties. In order to analyse BTEX (Benzen Toluene Etylbenzene Xylene) for the candidate materials, GC/MS was used after pretreatment according to methods of soil analysis by Ministry of Environment. For the homogeneity test among bottles in terms of candidate materials, ISO 13528 and IUPAC Protocol were used and according to the result, both candidate materials showed sufficient homogeneity. Also, the stability test over the candidate materials was accessed according to the ISO Guide 35 by classifying short-term and long-term stability and the result showed that both candidate materials showed decent stability. The reference values of the two candidate materials depending on BTEX components were derived from the average of the 11 samples that were used for verification of the samples' homogeneity. Uncertainty of measurement was combined by uchar that was caused by a characteristic value, $u_{bb}$ that was caused by between-bottle homogeneity, and $u_{stab}$ that was caused by stability, and then combined uncertainty ($u_{PTM}$) was multiplied to the coverage factor (k) derived from the effective degree of freedom from each factor that leads to expanded uncertainty (U) in about 95% of confidence level. The proficiency testing materials developed through this study were supplied to National Institute of Environmental Research (NIER) and utilized as an external proficiency testing materials for evaluating analysis capacity of soil agencies with specialty in terms of soil analysis approved by Minister of Environment.

Investigation of Statbility of Truncated Tetrahedron Type Amore Block (깍은 사면체형 소파블록의 안정성 평가)

  • Cho, Hong-Dong;Bae, Woo-Seok;Kim, Myeong-Kyun;Lee, Ho-Jin
    • Journal of the Korean Society of Safety
    • /
    • v.24 no.5
    • /
    • pp.43-47
    • /
    • 2009
  • Armor block is used to reduce wave energy. To do this, the stability of coastal structure is enhanced. It is very expensive to develop a new type armor block. So, the research of new type armor block is very short. We develope truncated tetrahedron type armor block(new type block) which have a hole in center part. In this study, the stability of new type armor block is investigated by hydraulic model test. In the result, the stability coefficient($K_D$) of new type armor block is 11.8. this value is more superior than value of tetrapod.

A Basic Study on Accelerated Life Test Method and Device of DSA (Dimensionally Stable Anode) Electrode (촉매성 산화물 전극 (DSA, Dimensionally Stable Anode)의 가속수명 테스트 방법과 장치에 관한 기초 연구)

  • Kim, Dong-Seog;Park, Young-Seek
    • Journal of Environmental Science International
    • /
    • v.27 no.6
    • /
    • pp.467-475
    • /
    • 2018
  • The lifetime of the electrode is one of the most important factors on the stability of the electrode. Since the lifetime of the DSA (Dimensionally stable anode) electrode is long, an accelerated lifetime test is required to reduce the test time. Beacuse there is no basis or standard method for accelerated lifetime testing, many researchers use different methods. Therefore, there is a need for basis and methods for accelerated lifetime testing that other researchers can follow. We designed a reactor system for accelerated lifetime testing and planned specific methods. Reactor system was circulating batch reactor. Reactor volume and cooling water tank were 12.5 L and 100 L, respectively. Electrode size was $2cm{\times}3cm$ (real electrolysis area, $5cm^2$). In order to maintain the harsh conditions, accelerated lifetime test was carried out in a high current density ($0.6A/cm^2$) and low electrolyte concentration (NaCl, 0.068 mol/L). Maintaining a constant temperature was an important operation parameter for exact accelerated lifetime test. As the accelerated lifetime test progressed, the active component of electrode surface was consumed and desorption occurred. At the point of 5 V rise, corrosion of the surface of the base material(titanium) also started.

A Study on the Development of Soil-based PTMs for Analysis of Benzo[a]pyrene - Focusing on the Evaluation of Homogeneity and Stability for the Certification of Benzo[a]pyrenecandidate Reference Materials - (Benzo[a]pyrene 분석용 토양 숙련도 표준시료 개발에 관한 연구 - 후보 표준물질의 인증을 위한 균질성, 안정성 평가를 중심으로 -)

  • Lee, Minhyo;Lee, Guntaek;Joo, Changkyu;Kim, Yonghun;Lee, Bupyoel;Choe, Sunghun;Kim, Myeongock;Hong, Sukyoung;Kim, Gumhee;Lee, Wonseok
    • Journal of Soil and Groundwater Environment
    • /
    • v.19 no.6
    • /
    • pp.49-58
    • /
    • 2014
  • This study was implemented as a part of the experiment to develop two kinds of soil-based Benzo[a]pyrene (BaP) proficiency testing materials (PTMs) for soil analysis. A test was carried out for the check of solubility of the reference material (high purity reagent) using several solvents. Another test was also conducted for the evaluation of homogeneity and stability of two kinds of candidate soil reference materials. The test analysis of BaP in terms of the candidate materials was conducted according to the Standard Soil Analytical Methods by Ministry of Environment. Dissolution of the reference material was shown to vary depending on solvent type and was higher in the order of Dichloromethane > Acetone > Acetone/MeOH (9 : 1) > N-hexane. In addition, the slope on calibration curve for BaP standard solutions was largest on BaP standard solutions prepared with dichloromethane of the tested solvents. Such tendency appeared egually in the commercial BaP standard solution. Therefore, it is thought to be reasonable to use dichloromethane as the solvent in case of the standard stock solution that is used for the measurement of BaP concentration in soil. ISO 13528 and IUPAC protocol were used for verification of homogeneity on the two kinds of soil candidate materials, Both candidate materials were sufficiently homogeneous. Stability assessment of the two candidate materials was made according to ISO Guide 35 and the result showed that both batches did not have any long-term and short term stability issues that might occur during shipping. However, monitoring results of BaP concentration in soil showed that BaP concentration of the two batches measured at 15 days after the sample preparation was reduced by about 24~37% compared with that of the samples measured on 0 day of the sample preparation. Identification was done with several treatments such as irradiation and sterilization etc. The major cause was shown to be irradiation to the samples.