• Bulletin of the Korean Chemical Society
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• v.29 no.1
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• pp.127-129
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• 2008

EPR spectroscopic technique was applied for a quantitative analysis of Eu(II) for a speciation of europium in a LiCl-KCl eutectic melt. By adopting the first absorption line of each isotopes (151Eu and 153Eu), a calibration plot was obtained. The calibration of the EPR intensity shows a good linearity according to the amount of Eu(II). The EPR intensity was identified to increase proportionally with a decrease of the attenuation parameter for EPR microwave power. The fluorescence technique was used qualitatively to find whether either of Eu(II) or Eu(III) ions exists in a molten salt sample. The ICP-AES technique was also adopted to determine the total concentration of europium in the sample, since EPR is only sensitive for detecting the Eu(II) ion. The extent of the reduction of Eu(III) in the LiCl-KCl eutectic melt at 723 K was determined by using this technique.

• Nuclear Engineering and Technology
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• v.35 no.3
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• pp.234-242
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• 2003

The full energy peak efficiency of a hyper pure germanium (HPGe) detector was calibrated in a wide energy range from 0.06 to 11 MeV. Both the experimental technique and the Monte Carlo method were used for the efficiency calibration. The measurement was performed using the standard radioisotopes in the low energy region of $60{\sim}1408$ keV, which was further extended up to 11 MeV by using the $^{14}N(n,r)\;and\;^{35}Cl(n,r)$ reactions. The GEANT Monte Carlo code was used for efficiency calculation. The calculated efficiency had the same dependency on the r-ray energy with the measurement, and the discrepancy between the calculation and the measurement was minimized by fine-tuning of the detector geometry. From the calculated result, the efficiency curve of the HPGe detector was reliably determined particularly in the high energy region above several MeV, where the number of measured efficiency points is relatively small despite the wide energy region. The calculated efficiency agreed with the measurement within about $7\%$. In addition to the efficiency calculation, the origin of the local minimum near 600 keV on the efficiency curve was analyzed as a general characteristics of a HPGe detector.

• Nuclear Engineering and Technology
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• v.55 no.1
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• pp.190-200
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• 2023

As the field of application of in-situ gamma spectroscopy is diversified, proficiency is required for consistent and accurate analysis. In this study, a program was developed to virtually create gamma energy spectra of artificial nuclides, which are difficult to obtain through actual measurements, for training. The virtual spectrum was created by synthesizing the spectra of the background radiation obtained through actual measurement and the theoretical spectra of the artificial radionuclides obtained by a Monte Carlo simulation. Since the theoretical spectrum can only be obtained for a given geometrical structure, representative major geometries for in-situ measurement (ground surface, concrete wall, radioactive waste drum) and the detectors (HPGe, NaI(Tl), LaBr₃(Ce)) were predetermined. Generated virtual spectra were verified in terms of validity and harmonization by gamma spectrometry and energy calibration. As a result, it was confirmed that the energy calibration results including the peaks of the measured spectrum and the peaks of the theoretical spectrum showed differences of less than 1 keV from the actual energies, and that the calculated radioactivity showed a difference within 20% from the actual inputted radioactivity. The verified data were assembled into a database and a program that can generate a virtual spectrum of desired condition was developed.

• 한국신재생에너지학회:학술대회논문집
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• 2010.06a
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• pp.199.2-199.2
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• 2010

The main purpose of the calibration procedure is to perform a one to one comparison of the reference pyranometer and the test pyranometer. In order to achieve this, both pyranometers need to be exposed to exactly the same irradiance, under the same circumstances. There are a number of error sources that could result in a wrong measurement. Most importantly Lamp instability, pyranometer offsets, thermal offsets of junctions, voltmeter offset, voltmeter instability, reference pyranometer instability, tilting of the pyranometers and differences in sensor height. Another sun-disc calibration procedure compares the computed vertical component of the direct irradiance as measured by a pyranometer with that measured by the pyranometer to be calibrated. Readings are taken with the levelled pyranometer on a clear day. Firstly the global irradiance and then the diffuse component are measured. Simultaneously measurement of direct irradiance is made with the pyrheliometer. The ways of performing the calibration and the subsequent calculation have been chosen such that the effect all these error sources has been eliminated as much as possible.

• Journal of Radiation Protection and Research
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• v.38 no.1
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• pp.37-43
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• 2013

In case of neutron dose measurement using TLDs (thermo-luminescence dosimeters), because the neutron energy dependence of the TLD is very high, the calibration of the energy response according to the characteristics of the neutron spectrum of workplace is required. In the present study, the ambient dose equivalent rates inside and around the Long-Counter (neutron detector) with narrow and complex inside in the neutron field of $^{252}Cf$ were evaluated. The calibration factors to account for the neutron energy dependence of TLDs were established for both the bare and $D_2O$ modulated $^{252}Cf$ neutron beams, respectively. The values of the TLD's measurement were compared with the computational results of the MCNPX (Monte Carlo N-Particles transport code). When using the two calibration factors of the TLD than a single calibration factor, the measured and the calculated values at the point of verification outside and inside the Long-Counter were in more good agreement. This results show that TLD should be calibrated in the reference neutron field similar to workplace situation.

• Proceedings of the Korean Radioactive Waste Society Conference
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• 2006.11a
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• pp.251-252
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• 2006

• Proceedings of the Korean Nuclear Society Conference
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• 2005.10a
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• pp.822-823
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• 2005

• Structural Engineering and Mechanics
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• v.49 no.2
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• pp.163-182
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• 2014

Safety factors proposed in codes CEB, B.A.E.L 91 and EUROCODE 1 cover a great number of uncertainties; making them inadequate for the assessment of existing structures. Suitable safety factors are established using a probabilistic assessment, once real dimensions, materials strength and existing structures deterioration mechanisms are taken into account. This paper presents a calibration method for safety factors using a typical set of RC bridges in France. It considers the principal stages of corrosion provoked by $CO_2$ and $Cl^-$ penetration and threshold indexes (${\beta}_0$) for existing structures. Reliability indexes are determined by the FORM method in the calibration method.

• Journal of The Korean Astronomical Society
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• v.39 no.4
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• pp.151-155
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• 2006

Long slit spectrometers are widely used in optical and infrared bands in astronomy. Absolute flux calibration for extended sources, however, is not straightforward, because a portion of the radiation energy from a flux calibration star is blocked by the narrow slit width. Assuming that the point spread function(PSF) of the star is circularly symmetric, we develop a robust method to extrapolate the detected stellar flux to the unobscured flux using the measured PSF along the slit-length direction. We apply this method to our long slit data and prove that the uncertainty of the absolute flux calibration is less than a few percents.

• Proceedings of the Korean Nuclear Society Conference
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• 1996.05d
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• pp.34-39
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• 1996

A series of measurements was peformed between KAERI and PNNL, U.S.A at KAERI secondary calibration laboratory to intercompare and verify the KAERI reference photon radiation fields by using air equivalent plastic walled ionization chambers, Different ionization chambers of two laboratories were used to determine the air kerma rate, free-in-air, at reference positions in the KAERI photon radiation fields, As the results, the agreement in the cross measurements between two laboratories was found to be within less than ${\pm}$ 3 %. This degree of consistency was considered to be encouraging, because each laboratory maintains independently its calibration traceablity with its national primary standard