• Progress in Superconductivity
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• v.9 no.1
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• pp.74-79
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• 2007

We characterized the highly refined boron precursor powders which were attrition milled for different milling times. $MgB_2$ powder precursor was formed from elemental crystalline Mg and amorphous B powder. The microstructure was investigated by SEM. SEM results indicate that the size of the milled powders was reduced with increasing milling time, which were varied from 0 to 8 hours. We also studied thermal behavior of the starting precursor by DSC as a function of milling time. The thermal behavior of the powder precursors was influenced by milling time. In order to determine the thermal events at DSC peaks, we annealed the milled powder mixture at $600^{\circ}C$ and $650^{\circ}C$ under protective gas and then analyzed the formation of $MgB_2$ by the XRD. We observed that superconducting $MgB_2$ phase was formed at lower temperature by the longer high energy milling. These results show that the high energy milling of the boron precursor powder can improve the reactivity for the formation of $MgB_2$.

• Korean Journal of Materials Research
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• v.9 no.4
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• pp.341-344
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• 1999

We reported compositional separation(CS) into Co-enriched and Cri-enriched components inside the grains of Co-Cr based thin films prepared by rf sputtering. CS strongly depends on the sputtering conditions of substrate temperature and target composition. Tuning the microstructure of the Co-Cr films is important in order to employ the CS for high-density magnetic recording. We investigated the origin of CS from thermodynamic viewpoint. We employ a spinodal decomposition-like model to describe the origin of the CS in Co-Cr films. We consider the total free energy of the Co-Cr films as the sum of several free energies of; 1) thermodynamic mixing entropy of a binary solid solution, 2) magnetic ordering interaction(MOI) energy below the Curie temperature, and 3) excess interaction energy(XS) caused by the sputtering process as a function of temperature and composition. Those energies distorted the total free energy like the spinodal decomposition and caused the compositionally separated fine microstructure inside the grains. If the second derivative of the total free energy with respect to Cr composition becomes negative at a given substrate temperature, we may observe a metastable compositional separation inside the Co-Cr alloy films. We expect to exploit the microstructure of CS for ultra-high density magnetic recording.

• Transactions of the Korean hydrogen and new energy society
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• v.18 no.4
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• pp.406-412
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• 2007

An experimental study on the design of a catalytic combustor for 1.6 kW MCFC system has been performed. The roles of the catalytic combustor are to completely burn anode off-gas and to supply sufficient $CO_2$ to cathode channels. In order to avoid hot spot or fuel slippage, flow uniformity at the catalyst inlet was achieved by installing two crossing perforated plates between the catalyst and the mixing chamber with minimal pressure drop. A Pd/Ce/Ni-$Al_2O_3$ catalyst was used for complete combustion of the off-gas at GHSV=36,000.

• Transactions of the Korean hydrogen and new energy society
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• v.17 no.3
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• pp.317-323
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• 2006

Electric conductive material should be homogeneously mixed with sulfur in sulfur electrode fabrication of lithium/sulfur battery, because sulfur is electric insulator. In this paper electrochemical properties of Li/S battery was studied with various compositions of sulfur electrodes. When content of sulfur changed from 40 wt.% to 80 wt.%, the 60 wt.% sulfur electrode showed the maximum capacity of 1489 mAh/g-sulfur. Electrochemical properties of Li/S battery using 60 wt.% sulfur was also investigated with various carbon contents. The discharge capacity changed as a function of carbon contents. The optimum composition was 25 wt.% carbon for 60 wt.% sulfur electrode.

• Advanced Composite Materials
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• v.18 no.2
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• pp.121-134
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• 2009

The present study investigated, both experimentally and numerically, the improvement of low-velocity impact damage resistance of carbon fiber reinforced plastic (CFRP) laminates due to through-the-thickness stitching. First, we conducted drop-weight impact tests for stitched and unstitched laminates. The results of damage inspection confirmed that stitching did improve the impact damage resistance, and revealed that the improvement effect became greater as the impact energy increased. Moreover, the stitching affected the through-the-thickness damage distribution. Next, we performed FEM analysis and calculated the energy release rate of the delamination crack using the virtual crack closure technique (VCCT). The numerical results revealed that the stitching affected the through-the-thickness damage distribution because the stitch threads had a marked effect on decreasing both the modes I and II energy release rate around the bottom of the laminate. Comparison of the results for models that contained delaminations of various sizes revealed that the energy release rate became lower as delamination size increased; therefore the stitching improved the impact resistance more effectively when the impact energy was higher.

• Journal of Biosystems Engineering
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• v.40 no.1
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• pp.1-9
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• 2015

Purpose: The objective of this study was to understand the operating mechanism of the rock-drill drifter, to explain how to setup an experimental test system and measure the strain of the drifter's rod, and to evaluate the drifter's performance with respect to the impact energy and blow frequency. Methods: The structure of the rock-drill drifter and its operating principle regarding the impact process were analyzed. Static calibration was carried out to calculate the correction factor using a drifter rod as the first step of the experimental test. The impact energy and blow frequency were then calculated based on strain measurements of the drifter's rod. Results: Experimental results showed that the tested drifter elicited a blow frequency of 3330 BPM (Blows Per Minute) and generated impact energy of 170 J/blow. This indicates that the drifter elicits a higher percussion speed and results in a lower impact energy compared to the hydraulic breaker at the same input power. Conclusions: The study proposed methodologies that deal with the experimental setup and the evaluation of the performance of the rock-drill drifter. These methodologies can be extensively used for validating and improving the percussion performance of the drilling equipment.

• The Mathematical Education
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• v.41 no.1
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• pp.19-34
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• 2002

The 7th national mathematics curriculum lays emphasis on an interrelation of several subjects and a connection between mathematics and real life. In this reason, this study focuses on the enhancement of sound understanding nuclear energy which is one of important factor(concepts or contents) dealt with in the other subjects such as science, environment, social studies, etc.. Recently, even though it is insistent that nuclear energy be so important and request in the future society, there are still strong pro and cons regarding the use of it. In this study, teaching-and-learning materials were developed dealing with using nuclear energy, and consequently they might be used in math class for the purpose of enhancement of mathematical learning ability and of recognition on nuclear energy. In this study, Material 1 included a matter of the necessity for nuclear power plants using the ratio concept, and Material 2 did on a matter of the efficiency of nuclear energy and the unclear of nuclear power plants using ratio-graph, in the elementary and upper school mathematics. Material 3 focused on a matter of the principles of nuclear power plants using the properties of exponential law in high school mathematics. Ultimately, it is hoped in the study that more diverse instructional materials dealing with diverse situations inside and outside mathematics would be developed.

• Korean Journal of Materials Research
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• v.26 no.7
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• pp.359-362
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• 2016

Mineral filler is used for resin compounds, because it increases the stiffness and thermal stability of a resin compound, and it also cuts down the cost. Calcium carbonate, silica, magnesium oxide, and others are used as filler materials in general, and the type of filler material, the size, and content can affect the physical properties of compounds. Those factors also influence the viscosity of resin mixtures and the workability, and should be adjusted by changing the contents of the filler, which depends on the size. In this study, five kinds of ground calcium carbonate, which were different in size, were used to produce polyester compounds ; the physical properties were compared with the filler size and contents. The mechanical properties were measured by bending strength and tensile strength, and the heat deflection temperature was obtained for thermal stability.

• Korean Journal of Materials Research
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• v.18 no.8
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• pp.406-410
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• 2008

The properties of pyrolytic carbon (PyC) deposited from $C_2H_2$ and a mixture of $C_2H_2/C_3H_6$ on $ZrO_2$ particles in a fluidized bed reactor were studied by adjusting the deposition temperature, reactant concentration, and the total gas flow rate. The effect of the deposition parameters on the properties of PyC was investigated by analyzing the microstructure and density change. The density could be varied from $1.0\;g/cm^3$ to $2.2\;g/cm^3$ by controlling the deposition parameters. The density decreased and the deposition rate increased as the deposition temperature and reactant concentration increased. The PyC density was largely dependent on the deposition rate irrespective of the type of the reactant gas used.

• Land and Housing Review
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• v.3 no.1
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• pp.83-88
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• 2012

In this study, physical characteristics of cement and/or concrete materials that are typically used for energy-foundation (EF) structures have been studied. The thermal conductivity and structural integrity of the cement-based materials were examined, which are commonly encountered in backfilling a vertical ground heat exchangers, cast-in-place concrete piles and concrete lining in tunnel. For this purpose the thermal conductivity and unconfined compression strength of cement-based materials with various curing conditions were experimentally estimated and compared. Hydration heat generated from massive concrete in the cast-in-place concrete energy pile was observed for 4 weeks to estimate its dissipation time in the underground. The hydration heat may mask the in-situ thermal response test (TRT) result performed in the cast-in-place concrete energy pile. It is concluded that at least two weeks are needed to dissipate the hydration heat in this case. In addition, a series of numerical analysis was performed to compare the effect of thermal property of the concrete material on the cast-in-place pile.