• Journal of the Korean Magnetics Society
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• v.11 no.6
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• pp.272-277
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• 2001

A spin valve structure of Ta/NiFe/CoFe/Cu/CoFe/Ru/CoFe/FeMn/Ta which has a synthetic antiferromagnet (CoFe/Ru/CoFe), was fabricated by using a magnetron sputtering system. The thickness and composition of magnetic free and pinned layers affect the magnetic properties such as exchange interaction strength of each layer and so on. Even though Rutherford Backscattering Spectrometry (RBS) has advantages of quantitative and non-destructive analysis, it is almost impossible to determine the thickness and composition of magnetic thin films using lBS because of its poor mass resolution for a higher atom number (Z>20). In this study, quantitative analysis of the element composition and thickness for the spin valve sample was performed by combining both Proton Induced X-ray Emission Spectrometry (PIXE), which is one of element specific analysis techniques, and grazing-exit RBS with a highly improved depth resolution and absolute quantitative analysis. For the quantitative analysis, standardization of PIXE was carried out with NiFe, CoFe, and FeMn layers, which are one of constituent layers of spin valve films. Through PIXE standardization and the aid of PHE experimental results of the spin valve sample, ire overlapped signal in a grazing-exit RBS spectrum were successfully resolved and the thickness of the Ru layer was determined with a resolution of ∼1 .

• Analytical Science and Technology
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• v.20 no.6
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• pp.516-523
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• 2007

Purification of silica mineral has been investigated by acid leaching of pulverized silica. A series of studies has been carried out on the effect of leaching silica powder as a function of the leaching time at the constant temperature of $80^{\circ}C$ in oxalic acid, aqua regia, and two mixed acids of HF/HCl, $HF/HNO_3$. The impurities of silica and leachantes were measured by neutron activation analysis (NAA), inductively coupled plasma atomic emission spectrometry (ICP-AES), atomic absorption spectrometry, x-ray fluorescence (XRF) method and wet analysis (WA). Certain metals, such as sodium, calcium, iron, aluminium and titanium, have been found in concentrations of hundreds or even thousands of mg/kg. Comparison of purification processes of silica and analytical methods of impurities in the silica was conducted in this study.

• Journal of Radiation Protection and Research
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• v.38 no.2
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• pp.119-123
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• 2013

A simple laboratory-made radioactive source to check the integrity of a gamma spectrometry system with HPGe detector was developed. The check source consists of radium-riched soil which was ground in size of less than 0.154mm and contained in air tight cylinderical vial, and provides photons with 12 distinct energies. The spectra of the check source were measured once a month during one year, analyzed the charactreictics of their peaks. When the gamma spectrometry system was in normal state, the areas and FWHMs of the gamma rays with more than 3% gamma emission rate in radium and its decay products was constant within standard deviation 2% and 3%, respectively, except 77 keV peak. And it was found that this check source can play a sufficient role to check the integrity of a gamma spectrometry system using 10 peaks in the range of 77 to 2202 keV.

• Journal of the Korean Chemical Society
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• v.45 no.2
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• pp.183-188
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• 2001

• Journal of the Korean Chemical Society
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• v.48 no.2
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• pp.203-206
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• 2004

• Proceedings of the Korea Air Pollution Research Association Conference
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• 2000.04a
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• pp.323-324
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• 2000

최근 대기 중에 부유하는 입자상 물질의 농도와 인간의 질병 및 사망률에 관한 역학적 조사가 진행되면서 대기 중 입자상 물질 측정에 많은 관심이 집중되고 있다. 이러한 입자상 물질 중 $Cl^{-}$, $Br^{-}$ 등, 할로겐족의 분석은 일반적으로 이온크로마토그래피법(IC)으로 수행되고 있으나, 최근에는 금속원소 분석에 사용되는 ICP-AES(Inductively Coupled Plasma Atomic Emission Spectrometry)를 이용하여 분석하기도 하는 것으로 알려져 있다. (중략)

• Bulletin of the Korean Chemical Society
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• v.25 no.6
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• pp.913-916
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• 2004

• Journal of the Korean Chemical Society
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• v.38 no.11
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• pp.800-807
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• 1994

A method to determine the iron and steels employing a Direct Reading Atomic Emission Spectrometer was investigated. Matrix effect was removed by two correction methods which utilize linear and curvilinear functions. Although two methods gave different sets of matrix correction coefficients, the analytical results by the two methods gave the same results. The analytical results obtained by the present work were well agreed with those obtained by inductively coupled plasma spectrometry.

• Proceedings of the Korean Vacuum Society Conference
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• 2014.02a
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• pp.206.2-206.2
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• 2014

Recently, particle induced X-ray emission (PIXE) analysis system was installed at the 2MV ion acceleration system in Korea institute science and technology (KIST). This installation is for complement to low atomic resolution of heavy atoms at Rutherford backscattering spectrometry (RBS) system. For quantitative analysis, a mass calibration of the PIXE set-up has been done with thin film standards and. The GUPIX software package has been used to process the PIXE spectra and the results are compared with the values from RBS system. Therefore, the instrumental constant H (solid angle and correction factor) is determined relying completely on the GUPIX data base (cross-sections, fluorescence and Coster-Kronig probabilities, stopping powers and attenuation coefficients) for a large set of elements. These H values can be used in future analysis.

• Bulletin of the Korean Chemical Society
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• v.20 no.9
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• pp.1040-1044
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• 1999

A micro porous PTFE membrane desolvator (MMD) was built and evaluated for the on-line removal of organic solvents to facilitate the determination of trace metal contaminants in the solvents by ICP-AES. Three organic solvents, isopropyl alcohol (IPA), methanol, and dimethy sulfoxide (DMSO) were studied. The MMD reduced organic solvent concentration in the sample aerosol stream by 82% to 89%, as indicated by monitoring C(I) emission. Net signal intensity of Fe, Al, and Cu was increasing with higher organic solvent concentration, with the rate of increase being solvent dependent. The signal intensities for Mg and Pb followed the trend with the C(I) signal. Changing the sweep gas flow rate affected the optimum signal intensity. Wine samples were analyzed by the method of standard addition. The concentrations of B, Al, and Mg were determined with a relative precision of less than 2.3%.