• Title/Summary/Keyword: Dyeing rate

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Characteristic Changes of Disposable Clothes Fabric on Printing using Natural Dyeing (천연염재를 활용한 일회용 작업복 소재의 기능성 특성 평가)

  • Shin Jung-Sook
    • The Research Journal of the Costume Culture
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    • v.12 no.6 s.53
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    • pp.1010-1020
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    • 2004
  • The purposes of this study were to investigate characteristic changes on nonwoven fabric by the charcoal and the yellow soil printing. It separate the grind charcoal and the yellow soil as two different size of particles $45{\sim}52{\mu}m\;and\;53{\sim}65{\mu}m$ for hand screen printing on three kind of nonwoven fabrics. To examine the effect of the charcoal and the yellow soil printing on nonwoven fabric were to observe surface changes by a scanning electron microscope, dyeability by using spectrophotometer, moisture regain by oven method, deodorization and antibacterial activity. The results were as follows: When the charcoal and the yellow soil powder concentration increased from 3 to $9\%$ or from 5 to $10\%$, K/S value also increased from 3.06 to 8.55 or from 1.14 to 1.80. The charcoal and the yellow soil moisture regain also increased. In same concentration, moisture regain occurred higher as particle of small size. In concentration of charcoal $3\%$, rate of deodorization measured as $89\%,\;83\%\;and\;87\%,\;and\;9\%$ concentration caused $96\%,\;86\%\;and\;93\%$ of high deodorization. In concentration of 5, $10\%$ of yellow soil, rate of deodorization measured as $85\%$ over. Antibacterial activity examination in nonfinished nonwoven fabric resulted range of $60\%$, however, $3\%\;and\;9\%$ concentration finished nonwoven fabric resulted $99.9\%$ of excellent antibacterial activity. Also $5\%,\;10\%$ yellow soil concentration was appeared same resoult.

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Natural Dyeing of Silks Dyed Singly with Caesalpinia sappan, Dactylopius coccus, Combination-Dyed with Caesalpinia sappan and Phellodendron Amurense Rupr., and with Dactylopius coccus and Phellodendron Amurense Rupr. (소목 및 코치닐로 단독 염색한 견직물, 그리고 소목과 황벽 및 코치닐과 황벽으로 복합 염색한 견직물의 천연염색)

  • Jung, Jin Soun
    • The Journal of the Convergence on Culture Technology
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    • v.6 no.4
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    • pp.275-281
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    • 2020
  • We studied the dyeability and functionality of silks dyed singly with Caesalpinia sappan, Dactylopius coccus, combination-dyed with Caesalpinia sappan and Phellodendron Amurense Rupr., and with Dactylopius coccus and Phellodendron Amurense Rupr.. The color of silk dyed singly with Caesalpinia sappan was Red with Hue of 2.2 R, the color of silk dyed singly with Dactylopius coccus was Reddish Purple with Hue of 3.0 RP, The color of silk combination-dyed with Caesalpinia sappan and Phellodendron Amurense Rupr. was 2.7YR being in the Orange family, and the color of silk combination-dyed with Dactylopius coccus and Phellodendron Amurense Rupr. was Red with Hue of 4.3R. In the case of antimicrobial activity, except for silk dyed only with Dactylopius coccus, the other three types of dyed silk showed excellent antimicrobial activity against Staphylococcus aureus achieving higher than 91.1% of bacteria reduction rate. Against Klebsiella pneumoniae, silk combination-dyed with Dactylopius coccus and Phellodendron Amurense Rupr., and with Caesalpinia sappan and Phellodendron Amurense Rupr. presented very excellent antimicrobial property achieving bacteria reduction rate of 99.9%.

The Effects of Cultivars and DAPs(Days After Planting) of Kenaf Plants on Lignin Contents and Dyeability of Their Fibers (품종과 재배기간이 다른 케나프 섬유의 리그닌 함량과 염색성)

  • Rhie, Jeon-Sook;Yoo, Hye-Ja;Ladisch, Christine M.
    • Journal of the Korean Society of Clothing and Textiles
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    • v.31 no.12
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    • pp.1682-1688
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    • 2007
  • The effects of cultivar and DAPs on the lignin content and dyeability of the kenaf fibers were investigated. Four kenaf fiber samples were prepared from two cultivars, Tainung 2 and Everglades 41, and their 60 and 120 DAPs(days after planting) for the experiments. The lignin contents of the kenaf fibers of Tainung 2(T2) and Everglades 41(E41) were $11.29{\sim}12.78%$. Both T2 and E41 kenaf fibers had comparable amount of lignin, and klason lignin of the fibers was $2.5{\sim}3$ times as much as much as acid-soluble lignin. In both T2 and E41, 120 DAPs kenaf have 1% more lignin than 60 DAPs kenaf. The moisture regains of the four kenaf fiber samples were almost the same as $10.25{\pm}0.05%$. The absorbances of residual solution after dyeing for $1{\sim}180$ minutes with Red 81 at maximum wavelength 520 nm and Green 26 at 600 nm were measured. Comparing to Green 26, the dyeing rate of Red 81 was rapid and equilibrium state was reached in 12 minutes. The CIE $L^*,\;a^*, \;b^*,\;{\Delta}E$ and K/S values of the kenaf fibers dyed with Red 81 and Green 26 were measured as well. The dye exhaustion ratio of 60 DAPs kenaf was higher than that of 120 DAP.

Optimization of Wool Dyeing with Yellow Dye from Carthamus Tinctorius L. (홍화 황색소를 이용한 모염색의 최적화)

  • Shin, Youn-Sook;Son, Kyung-Hee;Yoo, Dong-Il
    • Journal of the Korean Society of Clothing and Textiles
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    • v.33 no.12
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    • pp.1971-1978
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    • 2009
  • This study investigated the adsorption of safflower yellow dye on wool protein fiber and the optimum dyeing conditions to test color reproducibility. In addition, the effects of mordants on dye adsorption, color, fastness, and photofading rate were also studied. The prepared dye in powder form was characterized with UV-vis spectroscopy and FT-IR spectrometric analysis. The color of dyed fabrics was characterized by CIE $L^*a^*b^*$ coordinates, H V/C, and K/S values. The color reproducibility of the dyed wool fabrics was examined. The amount of dye adsorption increased and also, the shade of the dyed wool fabrics became deeper and more saturated with increasing temperature, time, and dye concentration. The maximum color strength was obtained at pH 3.0. The shade of dyed wool fabrics ranged from light yellow to dark mustard yellow as the pH of the dye bath shifted from alkaline to acidic. Color reproducibility was reliable with color differences in the range of 0.53~1.75. Fastness to dry cleaning was relatively good at 4/5 rating irrespective of mordanting. Fe and Cu mordants showed the least color change of the dyed wool fabrics after exposure to light. Mordants did not contribute to improve dye uptake and color fastness, although they made variations in color tone. Safflower yellow dye can be used satisfactorily without mordants and will not cause damage to the environment.

Methacrylamide graft polymerization on silk fibroin dyed with reactive dyestuffs (반응염색견(反應染色絹)의 Methacrylamide graft 중합(重合))

  • Rhee, In Jeon;Lee, Dong Soo
    • Current Research on Agriculture and Life Sciences
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    • v.12
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    • pp.83-95
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    • 1994
  • Fixation rate of reactive dyes on silk fibroin showed the same tendency to absorption rate. Fixation rate of Yellow 179 and Blue 71 was quite slow and Black 5, Blue 49, Blue 4, Blue 19 and Blue 21 was relatively fast. Weight increase by MAA graft polymerization onto filk fibroin was decreased, on the whole, according to the the increase of dye fixation, but weight increase of silk fibroin dyed with Blue 71 and Blue 21 was much higher than that of silk fibroin. And weight increase of silk fibroin dyed with Yellow 179 was similar to that of silk fibroin and in case of Blue 19, weight increase was about 12%, constantly. Weight increase of silk fibroin dyed with Blue 71 and Blue 21 was higher and the others were lower than of silk fibroin. And weight increase was diminished according as the dyeing temperature rises. The color was a little changed by MAA graft polymerization.

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Optimization of Catalytic Reaction for Synthesis of 2-Methyl-4-methoxydiphenylamine (2-Methyl-4-methoxydiphenylamine 합성을 위한 촉매반응의 최적화)

  • Cho, Jeong-Woo;Kim, Eun-Seok;Kim, Kiseok;Kim, Seong-Hoon
    • Applied Chemistry for Engineering
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    • v.10 no.2
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    • pp.293-298
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    • 1999
  • Reaction mechanism was elucidated and reaction condition were optimized for the catalytic reaction synthesizing 2-methyl-4-methoxy-diphenylamine (MMDPA) which is an intermediate of Fluoran heat-sensitive dyestuff. Reactants consisted of 2-methyl-4-methoxyaniline (MMA), 3-methyl-4-nitroanisole (MNA), and cyclohexanone, and 5 wt % Pd/C was used as a catalyst. Experiments were run in an open slurry reactor equipped with reflux condenser, and products were analyzed by means of GC/MS and NMR. MMDPA yield of 90 mole % could be obtained after reaction time of 8~10 hours under the optimal reaction conditions comprising the reaction mass composition of MMA : MNA : cyclohexanone = 1 : 2 : 150 based on MMA input of 0.01 gmoles in xylene solvent, reaction temperature of $160^{\circ}C$, and catalyst amount of 0.5 g. It was found that the rate-determining step of overall reaction was dehydrogenation of the intermediate product obtained from condensation of MMA and cyclohexanone. Overall reaction rate and MMDPA yield were enhanced owing to hydrogen transfer reaction by introducing MNA together with MMA in the reaction mass. Excess cyclohexanone in the reaction mass played an important role of promoting the condensation of MMA and cyclohexanone.

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Effects of Scarification, Temperature and Sulfuric Acid Treatments on Seed Germination of White Lotus (Nelumbo nucifera) (백련(Nelumbo nucifera) 종자의 발아에 미치는 종피의 파상, 온도 및 황산처리 효과)

  • Im, Myung-Hee;Kim, Byoung-Woon;Park, Yong-Seo;Yang, Seung-Yul;Song, Chyae-Eun;Heo, Buk-Gu
    • Korean Journal of Plant Resources
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    • v.25 no.1
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    • pp.7-13
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    • 2012
  • This study was conducted to determine the effects of scarification temperature, and sulfuric acid treatments on seed germination of white lotus collected from the Muan districts, Jeonnam in Korea. Without scarification, white lotus seeds were not germinated at all at 15 days after seeding. However, seeds sacrificed at basal parts showed 100% germination rate at $25^{\circ}C$ 6 days after seeding. All the seeds floated (0.90 g) and soaked (1.18 g) in the water were completely germinated. Especially, the lotus seeds soaked in the water at $25^{\circ}C$ showed high germination rate. Seeds treated with 80% sulfuric acid for 40-160 hours were germinated completely within 6 days after seeding. No difference in seed germination rate of white lotus stored up to 0, 12 and 24 months after harvest was observed. Overall results would be useful means for propagation and production of white lotus.

Development of Mono Layer Cell Adsorption Apparatus to Create a Slide for Microscopic Diagnosis (현미경 진단용 슬라이드 제작을 위한 단층세포 흡착장치 개발)

  • Oh, H.Y.;Mun, M.G.;Kim, S.H.;Kim, D.W.;Kang, S.M.;Sung, R.G.;Kim, H.C.
    • Journal of Biomedical Engineering Research
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    • v.36 no.1
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    • pp.1-6
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    • 2015
  • This study aims to design a monolayer cell adsorption apparatus that would help to produce high-quality slides for Liquid-Based Cytology (LBC) of an early cancer diagnosis for human bodies. The LBC collects exfoliated cells of human bodies and spreads the cells on the slides. Through processes of dyeing and cytological examination, the LBC screens for cancers in early stage. In this study, both of a cell suction module and a cell adsorption module, which are the key elements of the monolayer cell adsorption apparatus, were developed, and using those modules, the study set, first, conditions to help both GYN and NON-GYN apply principal cells without de-endothelialization before conducting its own analysis on the utility. As a results, for GYN, apparatus was determined to be able to produce high-quality slides under the condition of 4 and for NON-GYN, the apparatus would come up with other slides of high-quality under the condition of 2. The study carried out a repetitive test on selected conditions and proved 96% of the repetitive success rate. By the results of what has been learned so far, the study presents that the apparatus has a possibility to replace device from South Korea as one of those other currently-applied systems to run the LBC and that the system will also present a new paradigm for cancer diagnosis as it makes a contribution to the improvement in the LBC.

The Degumming and Sericin Recovery of the Silk fabric Using the Electrolytic Water (전해수를 이용한 견섬유 정련 및 세리신 회수 (I))

  • 배기서;하헌주;박광수
    • Textile Coloration and Finishing
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    • v.14 no.4
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    • pp.249-258
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    • 2002
  • Natural silk is formed by two proteins : the crystalline fibroin (inside the silk thread) and amorphous sericin (as a tube outside the thread). The degumming process is used to eliminate the external sericin prior to dyeing ; generally it makes use of soaps at about pH 10. Sericin is the protein constituent that "gums"together the fibroin filaments of cocoon silk. It constitutes about 25% of the weight of the cocoon, is soluble in hot water and "gels" on cooling. The removal of sericin from raw silk, known as degumming, is a simple but important process usually employing hot dilute soap or alkaline solution and occasionally dilute acids or enzymic methods. During degumming, alkali is taken up by the sericin and the free acid from the soap is formed ; this may be deposited on the fiber, reducing the rate of degumming and protecting it from hydrolysis. Alkali is often added to maintain or restore the pH of the baths, but it is rarely used alone, since it leaves the silk rather harsh in handle. If complete sericin removal is required as for printing, sodium carbonate may be added. If the pH of the bath exceeds 11, the fibroin is attacked. Recently, According to the development of electrolysis, we can be obtained the electrolytic reduction water(above pH 11.5) and electrolytic oxidation water (below pH 3). The aim of this work was to study a degumming process using electrolytic water and a possibility of sericin recovery. The new degumming process used electrolytic water operates at $95^\circ{C}$ for 2hr. without any reagents. The wastewater of this process are formed by a solution of sericin in water. This conditions suggest the study of a possible recovery of this protein (sericin) which has an amino acid composition suitable for many used in cosmetics, textile finishing agents, animal feeding, etc. The degumming process using electrolytic water is available to reduce treatment costs and pollute and at the same time to recover sericin.

Effect of No-Tillage on Soybean Yield and Weed Emergence in Drained Paddy Field Condition in Jeonnam Province (전남지역 논 조건에서 무경운 재배가 콩의 생육, 수량 및 잡초 발생에 미치는 영향)

  • Kim Dong-Kwan;Chon Sang-Uk;Heo Buk-Gu
    • The Korean Journal of Community Living Science
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    • v.17 no.3
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    • pp.89-97
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    • 2006
  • This study was conducted to compare soybean growth and yield and the degree of weed emergence according to no-tillage and conventional tillage system in two different drained paddy fields, loam of Chilgok series and silty clay loam of Deokpyeong series. In both soil conditions, the maturing time of the soybeans by the no-tillage system was two days earlier than that by the conventional tillage system. In the loam of Chilgok series, the stem length of the soybeans in the no-tillage system was 5.7 cm longer than that in the conventional tillage system. The miss-planted rate and diseased plants of black root rot (Calonectria iliacola) in the no-tillage system were 9.2% and 2.8% lower, respectively than those in the conventional tillage system. Also, the nodulation and seed yield in the no-tillage system were 32% and 13% more, respectively, than those in the conventional tillage system. In the silty clay loam of Deokpyeong series, the stem length of the soybeans in the no-tillage system was 4.6cm shorter than in the conventional tillage system. The diseased plants of black root rot (Calonectria iliacola) in the no-tillage system were 4.2% lower than those in the conventional tillage system. Also, no significant difference in the seed yield between the no-tillage and conventional tillage systems was observed. On the other hand, there was a lower occurrence of weed in the no-tillage system than in the conventional tillage system, and the income increased by 19% owing to yield increase and reduced management costs.

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