• Textile Coloration and Finishing
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• v.12 no.4
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• pp.248-255
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• 2000

Polyester fibers and fabrics have been dyed with disperse dyes in alkaline dyebath such as alkaline buffer and alkaline auxiliary(JPH-95) comparing a traditional acidic dyeing. After dyeing the samples were extracted with 100% DMF, and washing and rubbing fastnesses were measured. In dyeing at $100^\circ{C}$ the dyeing rate increased with decreasing fiber denier, regardless of dye baths, whereas the dyeing rates of the same denier fiber increased in the order of alkaline dyeing>acidic dyeing>JPH-95 dyeing. In dyeing at $130^\circ{C}$ the dyeing rate of PET fiber in JPH-95 dye bath decreased compared with the other two types of dye baths. In the time and temperature curve the dye uptake of JPH-95 dyeing was higher than the other two types of dye baths in the range of low temperature$(95~115^\circ{C})$. The equilibrium dye uptake increased in the order of 0.52d>2.04d>0.05d fiber. Washing fastness had no change in all three types of dye baths. But rubbing fastness was not good for alkaline dyeing except black dyes.

• Textile Coloration and Finishing
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• v.25 no.3
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• pp.194-205
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• 2013

In this study, we report dyeing properties and functionality of cotton and silk fabrics dyed with methanol extract from Juniperus chinensis heartwood. Non-aqueous dye of Juniperus chinensis heartwood extracted with methanol was expressed reddish color. It showed relatively good affinity to silk than cotton. Dye uptake of cotton and silk continued to increase according to the increase of the dye concentration. Cotton was not affected by the dyeing temperature and time, however, dye uptake of silk was increased as the dyeing time and temperature were increased. Dye uptake of cotton and silk were the highest at pH 8 and pH 6 respectively. Dyed fabrics showed various colors depending on mordant types and mordant concentration. Washing, light and perspiration fastness were not good. However, rubbing and dry cleaning fastness showed relatively good grade. Dyed fabrics of ultraviolet-cut ability and deodorant ability were improved. Also, dyed fabrics showed very good antimicrobial abilities of 99.9%.

• Textile Coloration and Finishing
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• v.22 no.1
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• pp.71-76
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• 2010

In this study the optimum dyeing conditions and blocking effect of UV deodorization efficiency of Ligustrum japonicum Thunb were investigated. Colorants were water-extracted from Ligustrum japonicum Thunb fruit and freeze-drided to obtain colorants powder. The effects of dye concentration, dyeing temperature, dyeing time, and the number of dipping count were studied. Fastness to dry cleaning, rubbing, perspiration, and light were measured according to KS K 0644, KS K 0650, KS K 0715 and KS K 0700, respectively. In order to examine the dyeability according to dyeing conditions, reflectance of fabrics were measured by using UV/VIS spectrophotometer. The bath ratio was 1:20. Dyeing concentration was 100, 200, 300, 400 and 500% on the weight of fiber. Dyeing time was 20, 40, 60, and 80 minutes. Dyeing temperature was 20, 40, 60, 80, and $100^{\circ}C$. The infrared high pressure dying machine was used. As dyeing concentration increased, dye adsorption increased up to 400% and it slowed down. Dye uptake was increased with raising themperature up to $80^{\circ}C$ and it slowed down. Dye adsorption occurred rapidly at first 20 minutes and then it slowed down and reached almost maximum dye uptake at 60 min. Dye uptake increased by repeated dyeing. Therefore, it is considered that optimum dyeing condition is 400%(o.w.f.), $80^{\circ}C$, 60 min. And repeated dyeing improves dye uptake. Color fastness to dry cleaning and rubbing was good, but light fastness and perspiration fastness was not good. Blocking effect of ultraviolet radiation and deodorization efficiency was good.

• Proceedings of the Korea Contents Association Conference
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• 2004.05a
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• pp.473-477
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• 2004

Cotton fabric was treated with Cationon UK(tertiary ammonium salt) to improve the dyeability to black tea colorants. In order to investigate the efficacy of Cationon UK for improving dyeing properties of cotton fabric, the effect of Cationon UK treatment conditions and dyeing conditions on dye uptake of the cotton fabrics treated with Cationon UK were examined and the colorfastness to washing, perspiration, rubbing and light was also evaluated for practical uses. Cationized cotton treated with Cationon UK showed high dye uptake at lower dyeing concentration and shorter dyeing time, compared with untreated. Dyeing temperature did not affect significantly dye uptake and the maximum dye uptake was obtained at pH 5. Most colorfastness was relatively good, showing 4/5∼5 rating.

• Journal of Fashion Business
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• v.18 no.5
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• pp.69-81
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• 2014

Fabric made of 100% silk was dyed with Undaria pinnatifida extracts under different conditions such as varing colorant concentration, temperature, time and dyebath pH. The dye uptake (K/S, value), CIE L*,a*,b* and Munsell values of the dyed samples and mordanted samples were measured. Colorfastness, antibacterial property and UV protection property were also evaluated. As colorants concentration increased, the dye uptake increased progressively and maximum color strength was obtained at 100% V/V. Dye uptake also increased with increasing temperature and time, and the maximum color strength was obtained at $80^{\circ}C$ and 60min. With pre-mordanting, the color of the Al and Fe mordanted silk fabrics was yellow on the Munsell color system, while the Cu mordanted fabric was a greenish color. Al and Fe post-mordanted fabrics had a yellow tone, and the Cu post-mordanted fabric had a yellow greenish tone. The light fastness property of the Cu mordanted silk fabric was relatively good, The effect of Al and Fe mordanting on fastness was insignificant. The antibacterial activity of dyed and unmordanted silk fabric was excellent, whereas fabric dyed and mordanted with Undaria pinnatifida extract demonstrated superior ultraviolet protection.

• Journal of Fashion Business
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• v.23 no.4
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• pp.100-111
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• 2019

In this study, the dyeing properties and functionalities of Crataegi fructus extract were investigated for the purpose of application to new natural dye resources. The effects of dyeing conditions(concentration of dye, dye bath temperature, dyeing duration and dye bath pH) and mordanting on dye uptake and color changes were also examined. The study also estimated the colorfastness, antibacterial properties, and ultraviolet protection properties of the dyed and mordanted silk fabrics. The dye uptake increased in tandem with the dye concentration and dye bath temperature. The highest K/S values were obtained at the following conditions: a dye concentration of 100%(v/v), a dyeing period of 60 minutes, a dye bath temperature of $90^{\circ}C$, and a dyeing pH of 3. The colorfastness of the material when dry cleaned or rubbed ranged from good to excellent and fastness to light was rated at grade 2-3. The change in the color grade when exposed to washing was not good; however, the stain of washing fastness was good at a range of 4-5. In regards to the functional property aspects, the dyed and mordanted fabrics exhibited excellent results with a 99.9% reduction rate, and excellent ultraviolet protection factors.

• Journal of the Korean Society of Clothing and Textiles
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• v.35 no.4
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• pp.466-475
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• 2011

The dyeing properties of protein fiber with pine needles colorants were studied through an investigation of the effect of dyeing conditions such as dye concentration, dyeing temperatures and time on dye uptakes, effect of mordants, and color change. In addition, the various colorfastness of dyed silk and wool fabrics were evaluated for practical use. The antimicrobial ability, ultraviolet-cut ability, and deodorant ability were also estimated. The dye uptake increased as the dyeing concentration increased and this enabled the obtainment of the Langmuir absorption isotherm. The dye uptake increased as the dyeing time and temperature increased. Pine needles colorants showed relatively good affinity to protein fiber and produced a yellow color. Post-mordanting was more effective than the pre-mordanting, and the dye uptake of fabrics improved by mordanting. Except for washing, the colorfastness of dyed fabrics showed a low rating. However, the colorfastness to light and the dry cleaning of fabrics mordanted with N.Cu, and the friction fastness of fabrics mordanted with Cu improved. The guide fabrics showed very good antimicrobial abilities of 99.9%; in addition, the ultraviolet-cut ability and deodorant ability improved in fabrics dyed with pine needles extracts.

• Journal of the Korean Society of Clothing and Textiles
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• v.35 no.3
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• pp.336-346
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• 2011

Dyeing properties of protein fiber with bamboo colorants were studied by investigating the effect of dyeing conditions such as dye concentration, dyeing temperatures, times on dye uptakes, effect of mordants, and color change. The various colorfastness of dyed fabrics were evaluated for practical use. In addition, the antimicrobial ability, ultraviolet-cut ability, and deodorant ability were estimated. The dye uptake increased as the dyeing concentration increased. Bamboo colorants showed relatively good affinity to protein fiber and produced a yellow color. Dye uptake increased as the dyeing time and temperature increased. Post-mordanting was more effective than pre-mordanting. Mordants, Fe and N.Fe, were effective for increasing dye uptake. The color of fabric mordanted with Cu and N.Cu changed to GY. Colorfastness of dyed fabrics showed a relatively good rating, and mordanting had no significant effect on colorfastness. Dyed silk fabric showed very good antimicrobial abilities of 99.9%. Also, ultraviolet-cut ability and deodorant ability were improved in silk fabric dyed with bamboo extracts.

• Textile Coloration and Finishing
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• v.32 no.1
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• pp.1-8
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• 2020

The objective was to study the efficiency of Houttuynia cordata extract colorants as eco-friendly and functional dye for wool fabrics. Effects of dyeing conditions and mordanting on dye uptake, color change, and colorfastness were investigated. Also, antimicrobial activity and deodorization performance were evaluated. The Houttuynia cordata colorants showed good affinity to wool fabrics and produced YR Munsell color. The optimum condition of dyeing was 2.0% of colorants concentration(o.w.b.) at 100℃ for 60 minutes under pH 5.3. Regardless of the mordant type and mordanting method, mordants improved dye uptake and the increase in dye uptake by Fe mordant was higher than that of Al mordant. Al post-mordanting and Fe mordanting changed the color of dyed fabrics with Y Munsell color. The colorfastness of un-mordanted and Al post-mordanted fabrics were excellent above grade 4. Bacteria reduction rate(Staphylococcus aureus) of wool fabrics dyed with Houttuynia cordata colorants was excellent at 98.2%. Also, the deodorization was good at 81%. The results show Houttuynia cordata colorants can be used as a functional natural dye for wool fabrics.

• Journal of the Korean Society of Clothing and Textiles
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• v.35 no.10
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• pp.1228-1241
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• 2011

This research compares the change in berberine content in liquid dye and the color and dye uptake of amur cork tree dyed silk upon thermal degradation treatment. Thermal degradation of amur cork tree extract and liquid dye of standard berberine was carried out at room temperature, $4^{\circ}C$ refrigeration, and $100^{\circ}C$ oven conditions for 0-192 hours. Amur cork tree dyed silk was treated in a $100^{\circ}C$ oven for 0-240 hours. The berberine content in liquid dye was measured by the relative abundance of the berberine peak in the HPLC-MS chromatograms. The color and dye uptake of dyed silk was measured using K/S value and colorimetric data. The berberine content in standard berberine dye was 2.4 times that of the amur cork tree extract. A similar result was observed between the K/S value of standard berberine dyed silk and that of amur cork tree dyed silk. The berberine dyed silk showed the highest dye uptake after 120 hours in a $100^{\circ}C$ oven. This result was similar to the change in a berberine content in liquid dye in a $100^{\circ}C$ oven treatment. The change of the K/S value of amur cork tree dyed silk and berberine content of amur cork tree extract was similar up to 24 hours. The result suggests that there is a direct relationship between the color change of amur cork tree dyed silk and the berberine content in amur cork tree dye.