• 한국분말재료학회지
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• 제20권4호
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• pp.253-257
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• 2013

Freeze drying for porous Mo was accomplished by using $MoO_3$ powder as the source and camphor-naphthalene eutectic system as the sublimable material. Eutectic composition of camphor-naphthalene slurries with the initial $MoO_3$ content of 5 vol%, prepared by milling at $55^{\circ}C$ with a small amount of oligomeric dispersant, was frozen at $-25^{\circ}C$. The addition of dispersant showed improvement of dispersion stability in slurries. Pores were generated subsequently by sublimation of the camphor-naphthalene during drying in air for 48 h. To convert the $MoO_3$ to metallic Mo, the green body was hydrogen-reduced at $750^{\circ}C$, and sintered at $1100^{\circ}C$ for 2 h. The sintered samples, frozen by heated Teflon cylinder, showed large pores with the size of about 40 ${\mu}m$ which were aligned parallel to the sublimable vehicles growth direction. The formation of unidirectionally aligned pores is explained by the rejection and accumulation of solid particles in the serrated solid-liquid interface.

• 한국재료학회지
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• 제23권1호
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• pp.67-71
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• 2013

Porous $Al_2O_3$ dispersed with nano-sized Cu was fabricated by freeze-drying process and solution chemistry method using Cu-nitrate. To prepare porous $Al_2O_3$, camphene was used as the sublimable vehicle. Camphene slurries with $Al_2O_3$ content of 10 vol% were prepared by milling at $50^{\circ}C$ with a small amount of oligomeric polyester dispersant. Freezing of the slurry was done in a Teflon cylinder attached to a copper bottom plate cooled to $-25^{\circ}C$ while unidirectionally controlling the growth direction of the camphene. Pores were subsequently generated by sublimation of the camphene during drying in air for 48 h. The green body was sintered in a furnace at $1400^{\circ}C$ for 1 h. Cu particles were dispersed in porous $Al_2O_3$ by calcination and hydrogen reduction of Cu-nitrate. The sintered samples showed large pores with sizes of about $150{\mu}m$; these pores were aligned parallel to the camphene growth direction. Also, the internal walls of the large pores had relatively small pores due to the traces of camphene left between the concentrated $Al_2O_3$ particles on the internal wall. EDS analysis revealed that the Cu particles were mainly dispersed on the surfaces of the large pores. These results strongly suggest that porous $Al_2O_3$ with Cu dispersion can be successfully fabricated by freeze-drying and solution chemistry routes.

• 한국재료학회지
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• 제25권1호
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• pp.27-31
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• 2015

This paper proposes a novel way of fabricating aligned porous Sn by freeze-drying of camphene slurry with stannic oxide ($SnO_2$) coated Sn powders. The $SnO_2$ coated Sn powders were prepared by surface oxidation of the initial and ball-milled Sn powders, as well as heat treatment of tin chloride coated Cu powders. Camphene slurries with 10 vol% solid powders were prepared by mixing at $50^{\circ}C$ with a small amount of oligomeric polyester dispersant. Freezing the slurry was done in a Teflon cylinder attached to a copper bottom plate cooled at $-25^{\circ}C$. Improved dispersion stability of camphene slurry and the homogeneous frozen body was achieved using the oxidized Sn powder at $670^{\circ}C$ in air after ball milling. The porous Sn specimen, prepared by freeze-drying of the camphene slurry with oxidized Sn powder from the heat-treated Sn/tin chloride mixture and sintering at $1100^{\circ}C$ for 1 h in a hydrogen atmosphere, showed large pores of about $200{\mu}m$, which were aligned parallel to the camphene growth direction, and small pores in their internal walls. However, $100{\mu}m$ spherical particles were observed in the bottom part of the specimen due to the melting of the Sn powder during sintering of the green compact.

• Journal of the Korean Wood Science and Technology
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• 제43권6호
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• pp.746-756
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• 2015

본 논문에서는 목재 수축률에 관한 1976-2015년도에 발표된 목재공학회지 논문을 정리하였다. 국내산 낙엽송(Larix kaempferi) 수축률을 측정한 연구자들간에 접선방향 수축률은 4.21%-9.79%, 방사방향 수축률은 2.09%-4.67%, 섬유방향 수축률은 0.17%-0.33%로 접선방향 2.3배, 방사방향 2.2배, 섬유방향 1.9배로 연구자들마다 측정 값에 차이가 나타났다. 소나무(Pinus densiflora) 시편 크기가 $20{\times}20{\times}20mm$에서 $100{\times}100{\times}100mm$로 증가함에 따라 접선방향, 방사방향, 부피수축률은 2.61%, 1.32%, 0.80% 감소하였다. 아피통(Dipterocarpus grandiflorus)을 밀폐건조, 오븐건조, 실온건조 하였을 때 부피수축률은 31.6%, 26.5%, 21.0%로 건조방법에 따라 5.5%-10.6% 차이가 나타났으며 건조온도가 $115^{\circ}C$, $120^{\circ}C$, $125^{\circ}C$로 증가함에 따라 낙엽송의 수축률은 일정한 증가, 감소 경향이 보이지 않았다. $20mm^3$ 크기의 삼나무(Cryptomeria japonica) 시편을 한국산업규격(KS F 2203, 2004)에서 제시하는 정밀도 0.01 mm의 길이측정도구로 수축률을 측정하였을 때, 방사, 섬유방향 수축률 측정오차는 1.97%, 35.7%로 크게 나타났다. 목재의 수축률은 시편 크기, 건조방법, 측정방법에 영향을 받는 것으로 나타났다.

• 동력기계공학회지
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• 제21권5호
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• pp.55-62
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• 2017

In this study, the water content and the low calorific value of the dried sludge are analyzed by using a vertical cylinder type indirect heating type dryer for evaluatation of energy source value. The vertical cylindrical thin film dryer was an Okadora Pilot Plant, and the dryer was indirect heating vertical thin film type. The internal standard consisted of 500 mm in diameter and 700 mm in height. In the drying experiment, 10 kg of dehydrated sewage sludge was added to the dryer and the total amount of the sludge was adjusted to 27 times by variable of the time, the number of revolutions and the steam temperature. The results of analysis of the 27th experiment component of the dried product showed that the average low calorific value of about 11.2 MJ/kg and the water content of 6%. This is satisfy the fuel use standard of the thermal power plant of the sludge.

• Journal of Biosystems Engineering
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• 제9권2호
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• pp.89-96
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• 1984

This study was intended to search the thermal properties of rice which are necessary in preventing qualitative and quantitative losses in the drying and milling processes. First, the coefficient of cubical thermal expansion of brown rice was measured, which is required for analyzing the internal stress of rice, and then theoretical thermal and moisture stresses were calculated. The results are summarized as follows: 1. The coefficient of cubical thermal expansion of brown rice was about $2.81{\times}10^{-4}/^{\circ}C$ in the temperature range of $10^{\circ}C-60^{\circ}C$. 2. When the shape of brown rice was assumed to be a sphere or a cylinder, maximum thermal stress due to temperature change of $20^{\circ}C-60^{\circ}C$ was in the range of $25-100kg/cm^2$. And maximum moisture stress was in the range of $450-650kg/cm^2$ when the drying temperature was $35^{\circ}C$, initial and final moisture contents of brown rice were 20% and 14% (w.b.), and the moisture diffusion coefficient was assumed to be $6.79{\times}10^{-4}cm^2/hr$. 3. Consequently, it was concluded that crack formation in a rice kernel is mainly caused by moisture stress.

• 펄프종이기술
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• 제39권2호
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• pp.1-8
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• 2007

To examine the feasibility of dry forming technology for papermaking, a dry forming mold (DFM) was developed and evaluated. Main fanning section of DFM was a cylindrical tube, and at the top of the mold a stirring equipment was placed to disperse dry fibers. These fibers were screened using a hole type screen plate placed just under the stirring equipment and dropped freely on the fanning wire located 0.9 m below of the screen plate to form a dry fiber pad. The vertical and horizontal velocity of air flow in the forming cylinder were evaluated and analyzed to find the most effective method of air flow control in the cylinder. Humidification and pressing conditions to obtain a decent dry fanned papers were examined. Results showed dry fanned papers can be prepared with this dry forming mold. And this mold can be used to examine the effect of the papermaking process factors including pressing pressure, drying temperature, humidification on sheet quality of dry formed papers.

• 원예과학기술지
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• 제19권2호
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• pp.179-185
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• 2001

원예용 배지의 물리화학적 특성을 파악하기 위해 전세계적으로 다양한 분석 방법이 사용되고 있다. 유럽은 배지 분석방법의 표준화 연구를 지속적으로 수행해왔다. 유럽표준화 위원회에서는 유럽표준방법으로 CEN methods를 최종안까지 제출하였으며 사실상 유럽표준 배지분석방법의 제정을 확립하는 단계에 있다. 물리적 특성 중 건물함량과 수분함량은 건조 후 분석하였고, 실험 가밀도는 일정한 부피에 채워진 시료의 무게로 측정하였다. 가밀도, 진밀도, 공극률, 액상, 기상, 부피 감소율은 double ring과 sand suction table이라는 장치를 사용하여 배지를 포화, 배수시킨 후 건조시켜 분석하였다. 화학적 특성 중 pH와 EC는 부피 기준 1:5로 침출하여 분석하였다. 유기물과 회분함량은 건조와 연소 과정을 통해 분석하였다. CEN methods는 유럽표준방법으로 확립을 앞두고 있으나 더 지속적인 연구가 필요할 것이다.

• 한국작물학회지
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• 제31권2호
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• pp.150-155
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• 1986

콩을 탈곡기로 탈곡할 때 종실손상율이 낮으면서 발아율이 높은 종실의 수분함량과 탈곡기의 적정 급동속도를 구명하여 기웅탈곡시에 필요한 기초자료로 활용코자 시험을 실행하여 얻어진 결과를 요약하면 다음과 같다. 1. 성숙시 식물체 각 부위별 수분함량은 대입종인 황금콩의 경우 줄기, 종실, 콩깍지 순으로 소입종인 단엽콩은 줄기, 콩깍지, 종실 순으로 많았다. 2. 황금콩과 단엽콩의 성숙후 식물체 부위별 수분함량과 수분함량 감소정도는 줄기 및 종실에서는 비슷하였으나 콩깍지는 소입종인 단엽콩이 성숙후 7 일까지는 황금콩보다 높았고 그 후에는 차이가 없었다. 3. 성숙후 7 일의 일중의 줄기, 종실, 콩깍지의 수분함량 변이는 시간이 경과함에 따라 수분함량이 감소하는 경향이며 성숙후 14일에는 오전 11시까지 꼬투리의 수분함량이 종실의 수분함량보다 높았으나 그 이후에는 종실의 수분함량이 더 높았다. 4. 콩 탈곡시 탈곡기의 급동속도가 빨라지거나 종실수분함량이 많아질수록 종실보상율은 증가는 경향이며 대입종인 황금콩이 소입종인 단엽콩보다 종실 보상입율이 높았다. 5. 보상입율과 발아율을 고려할 때 탈곡기의 적정급동속도는 11 m/sec.가 적당한 것 같았다. 6. 탈곡에 알맞는 종실의 수분함량은 수량, 보상입율, 발아율, 작업속도 및 건조작업 등을 고려할 때 종실의 수분함양이 15∼20%가 적당한 것 같았다.

• 한국농공학회:학술대회논문집
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• 한국농공학회 2001년도 학술발표회 발표논문집
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• pp.65-68
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• 2001

This study was conducted to develop a soil moisture meter using capacitance probe. A parallel cylinder type capacitance probe (C-probe) was fabricated The 5 MHz of crystal oscillator was constructed to detect the capacitance change of the C-probe with moist soil. A third order polynomial regression model for volumetric water content having oscillation frequency changes at 5 MHz as independent variables presented the determination coefficient of 0.979 and root mean square error of $0.031\;cm^{3}cm^{3}$ for all soil samples. A prototype soil moisture meter consisting of the sample container, C-probe, oscillator, frequency counter and related signal procession units presented the correlation coefficient of 0.987 and the root mean square error of $0.032\;cm^{3}cm^{3}$ as compared with the oven drying method for unknown soil samples.