• Journal of the Korean Applied Science and Technology
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• v.22 no.2
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• pp.168-174
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• 2005

Aluminum tri-butoxide was mixed with the water/ethanol solution and then chloroplatinic acid was added to the solution. The solution was dried at $100^{\circ}C$ for 15hrs to remove the solvent and water then it was calcined at $500^{\circ}C$. The catalyst was activated with a gas mixture. During the activation, the temperature was increased from $150^{\circ}C$ to $500^{\circ}C$. The necessary amount of urea was dissolved in 50mL water and injected. Aqueous urea solution was then mixed with the feed gas stream. At low temperatures, nitrogen containing compounds of urea decomposition are used as reductants in the reducton of $NO_X$. However at high temperatures the nitrogen containing compounds are oxidized to NO and $NO_2$ by oxygen instead of being used in the reduction. The activity of the catalyst was dependent on urea concentration in the feed stream when there was not adequate water vapor in the feed. The maximum conversion was shifted from $250^{\circ}C$ to $150^{\circ}C$ when water concentration was increased from 2 to 17%. It seems that the maximum temperature shifts to lower temperatures because the hydrolysis rate of HNCO increases with water, resulting in higher amounts of $NH_3$.

• Journal of Powder Materials
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• v.9 no.4
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• pp.227-234
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• 2002

For the austenitic stainless steel (304L) manufactured by metal injection molding(MIM), the effects of copper content and sintering temperature on the mechanical properties, antibacterial activities, corrosion resistance, and electric resistances were investigated. The specimens were prepared by injection molding of the premixed powders of water-atomized 304 L and Cu with poly-acetyl binders. The green compacts were prepared with various copper contents from 0 to 10 wt.% Cu, which were debound thermally at 873 K for 7.2 ks in $N_2$gas atmosphere and subsequently sintered at various temperatures from 1323 K to 1623 K for 7.2 ks in Ar gas atmosphere. The relative density and tensile strength of the sintered compacts showed the minimum values at 5 and 8 wt.% Cu, respectively. Both the relative density and the tensile strength of the specimen with 10 wt.% Cu sintered at 1373 K showed the highest values, higher than those of copper-free specimen. Antibacterial activities investigated by the plastic film contact printing method for bacilli and the quantitative analysis of copper ion dissolved in water increased as the increase of the copper content to stainless steels. It was also verified by the measurement of pitting potential that the copper addition in 304 L could improve the corrosion resistance. Furthermore the electric conductivity increased with the increase of copper content.

• Analytical Science and Technology
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• v.18 no.5
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• pp.376-380
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• 2005

Quantitative analysis of silver from the thermal decomposition of chlorinated polymer contained nano silver is described. The chlorine contained in the chlorinated polymer (e.g. PVC) is liberated as hydrochloric acid gas by heating and a lot of silver produces AgCl. $HNO_3$ and $NH_4OH$ were used for dissolving the Ag and the AgCl. The silver complex was formed by $NH_4OH$. Then the complex was decomposed to silver by heating at $500^{\circ}C$ and the Ag was dissolved by dilute $HNO_3$. Recovery of silver in PVC material was 99.0%.

• Journal of Soil and Groundwater Environment
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• v.18 no.2
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• pp.36-44
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• 2013

The objectives of this study were to identify the characteristics of shallow groundwater from the oil-contaminated site for a long period and to evaluate the applicability of biopile technology to treat the soil excavated from it. The eight monitoring wells were installed in the contaminated site and pH, Electrical Conductivity (EC), Dissolved Oxygen (DO), Oxidation Reduction Potential (ORP), Temperature and the concentrations of major ions and pollutants were measured. The VOCs in soil gas were monitored during biopile operation and TPH concentration was analyzed at the termination of the experiment. The pH was 6.62 considered subacid and EC was 886.19 ${\mu}S/cm$. DO was measured to be 2.06 mg/L showing the similar characteristic of deep groundwater. ORP was 119.02 mV indicating oxidation state. The temperature of groundwater was measured to be $16.97^{\circ}C$. The piper diagram showed that groundwater was classified as Ca-$HCO_3$ type considered deep groundwater. The ground water concentration for TPH, Benzene, Toluene, Xylene of the first round was slightly higher than that of the second round. The concentration of carbon dioxide of soil gas was increased to 1.3% and the concentration of VOCs was completely eliminated after the 40 days. The TPH concentration showed 98% remediation efficiency after the 90 days biopile operation.

• Journal of Sensor Science and Technology
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• v.10 no.2
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• pp.118-124
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• 2001

When particles are dissolved in solution, they have different zeta-potentials depending on pH. Zeta-potential has an influence on particle separation, which can control particle size. And the size of $WO_3$ particle affects the sensitivity of $WO_3$ sensor for detecting NO gas. Therefore we study influence of pH on NO-sensing $WO_3$ gas sensor fabricated by Sol-Coprecipitation method. As pH increases from 2 to 7, dynamic mobility of $WO_3$ precursor was increased. When pH was 7, it showed the largest distribution separation. It means when pH is 7, we can make $WO_3$ powder which has smaller particle size. And it is confirmed by particle size analysis of $WO_3$ powder, X-ray diffration result of $WO_3$ sensing layer and surface morphology. It also affect NO sensing characteristics of $WO_3$ gas sensor. The sensing film synthesized at pH 7 showed the largest sensitivity.

• Proceedings of the KIEE Conference
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• 1999.07d
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• pp.1608-1610
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• 1999

To find effective diagnostic method for Transmission OF cables, various characterizations were carried such as DGA (dissolved gas analysis), water contents, total acidity and AC breakdown voltage. It was found that the result was varied by sampling and container. The results from those characterization method showed the present condition and history very well and could be used to estimate the degree of degradation of cables.

• Proceedings of the KIEE Conference
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• 2011.07a
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• pp.1554-1555
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• 2011

안정적인 전력공급을 위해 전력설비 진단이 중요시 되고 있고 이를 위해 변전기기인 변압기의 초기고장 검출을 통한 예방진단 기술을 필요로 하고 있다. 변압기 예방진단 기술 중에서도 유중가스진단은 가장 오래되고 신뢰성이 입증된 기술이다. 기존의 유중가스진단법들은 가스비분석법을 이용하고 있는데 대상 가스들이 절연유에의 열화에 의해 발생하는 가스들이고 주위 운전환경에 대한 고려가 부족하여 진단이 불가능하거나 진단오류가 발생한다. 본 연구에서는 절연유뿐만 아니라 고체절연물에 대한 열화를 고려하기 위하여 변압기 내부 결함 모의 시험 쳄버를 제작하고 시험 결과를 바탕으로 진단 알고리즘을 개발하고자 한다.

• Proceedings of the KIEE Conference
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• 1999.07c
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• pp.1493-1495
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• 1999

본 논문에서는 변압기 유중 가스 분석 자료와 고장에 관련된 특징을 학습시킨 신경 회로망을 이용하여 전력용 유입 변압기의 새로운 고장 진단 방법을 제안하였다. 본 논문에서 제안한 신경 회로망을 이용한 고장 진단 방법(유중 가스 분석 방법)은 입력으로 가스 구성비 분석(IEC 기준) 및 주요 가스 분석(한국 전력 공사 기준) 자료를 채택하였다. 또한, 출력으로 전력용 유입 변압기의 고장 유무 및 고장 종류의 특징을 신경 회로망으로 추출하였다. 따라서 입력된 유중 가스 분석 결과에 따라 전력용 유입 변압기의 진단 결과(고장 유무 인식 및 해석)가 제시되도록 구성하였다. 제안된 신경회로망을 이용한 변압기 고장 진단 방법은 한국 전력 공사의 변압기 유중 가스 기록으로 효용성을 입증하였다. 따라서 유중 가스 분석만으로 현실성 있는 변압기 진단 및 상태 추정이 가능하게 되었고, 이것의 적용으로 적절한 유지 및 보수 대책 방안을 제시할 수 있게 되었다.

• The Transactions of the Korean Institute of Electrical Engineers P
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• v.65 no.1
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• pp.41-46
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• 2016

It has been proven that the dissolved gas analysis (DGA) is the most effective and convenient method to diagnose the transformers. The DGA is a simple, inexpensive, and non intrusive technique. Among the various diagnosis methods, IEC 60599 has been widely used in transformer in service. But this method cannot offer accurate diagnosis for all the faults. This paper proposes a fault diagnosis method of oil-filled power transformers using IEC code based neuro-fuzzy model. The proposed method proceeds two steps. First, IEC 60599 method is applied to diagnosis. If IEC code can't determine the fault type, neuro-fuzzy model is applied to effectively classify the fault type. To demonstrate the validity of the proposed method, experiment is performed and its results are illustrated.

• 제어로봇시스템학회:학술대회논문집
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• 2001.10a
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• pp.127.2-127
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• 2001

A transformer is one of the most important elements in the power network. Transformer faults could cause costly repairs and be dangerous to personnel. To avoid this, its reliable operation has great significance and, therefore, the diagnosis system of the transformer is necessitated. The dissolved gas-in-oil analysis (DGA) is the worldwide popular method of detecting faults such as a hot spot or partial discharges inside the transformer. DGA, however, is not a reliable technique to identify aging phenomena and mechanical faults including insulation failure, inter-turn short, etc. To overcome the drawbacks of DGA, the transfer function method is used to identify effectively these kinds of the mechanical faults. The transformer has a unique transfer function independent of the shape of the input waveform, which can be evaluated through sweep test. This transfer function changes by winding ...