• 제목/요약/키워드: Dislocation density

검색결과 225건 처리시간 0.024초

GaAs기판의 표면 Offcut각도가 InGaP 에피막의 전위밀도에 미치는 영향 (Effects of Surface Offcut Angle of GaAs Substrate on Dislocation Density of InGaP Epilayers)

  • 이종원;박경수;이종식
    • 마이크로전자및패키징학회지
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    • 제9권3호
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    • pp.49-56
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    • 2002
  • 본 연구에서는 평탄형 (exact) GaAs 기판과 $2^{\circ}$, $6^{\circ}$, $10^{\circ}$ 경사형 (offcut) GaAs 기판 등 네 종류의 기판에 유기금속 기상성장장치를 이용하여 InGaP 에피막을 성장시켰고, 기판경사도에 따른 계면의 탄성특성이 InGaP 에피막의 전위밀도에 미치는 영향에 대하여 최초로 연구하였다. 탄성변형은 TXRD의 격자부정합과 격자 misfit등을 고려하여 산출되었고, 전위밀도는 에피막의 x-선 반치폭을 이용하여 계산되었다. 기판경사도가 $6^{\circ}$일 때 계면의 탄성특성이 가장 양호하였고, x-선 반치폭은 가장 낮았다. 11 K PL측정 결과, 기판경사도 증가에 따라 PL 발진파장은 감소하였고, 기판경사도가 $6^{\circ}$에서 PL 강도 역시 가장 높았다. 에피막의 TEM 관측 결과, 회절패턴은 전형적인 zincblende 구조를 보였고, 기판경사도 $6^{\circ}$에서 전위밀도가 가장 낮게 관측되어 TXRD 및 저온 PL측정 결과와 부합되었다. 본 연구의 결과와 소자제작 특성 및 빔특성을 종합적으로 고려해 볼 대, 광전소자용 InGaP/GaAs 이종접합구조에서 최적의 기판경사도는 $6^{\circ}$임을 밝혔다.

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Cu와 Cu-Zn 합금의 저주기피로 동안 발달한 미세조직 평가를 위한 비파괴기술 (Nondestructive Techniques for Characterization of Microstructural Evolution during Low Cycle Fatigue of Cu and Cu-Zn Alloy)

  • 김정석;장경영;현창용
    • 비파괴검사학회지
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    • 제31권1호
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    • pp.32-39
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    • 2011
  • 본 연구에서는 Cu와 Cu-Zn 합금의 저주기 피로 동안 발달한 전위 하부조직의 변화를 비파괴적으로 구분하고 평가하고자 하였다. 비파괴시험으로 초음파속도, 전기비저항 그리고 양성자소멸시간을 측정하였다. 서로 다른 적층결함 에너지를 갖는 Cu와 Cu-Zn에 대해 반복피로시험을 수행하고 이들 재료에서의 전위거동과 비파괴평가 파라미터와의 상관성을 연구하였다. Cu는 전위셀 하부구조를 형성하였지만, Cu-Zn 합금은 피로 사이클에 따라서 전위밀도는 증가하고 단지 평면배열의 전위구조를 형성하였다. 상온에서의 반복적인 피로에 의해 발달한 격자결함인 전위와 공공으로 인해 초음파속도의 감소, 전기비저항의 증가 그리고 양성자 소멸시간이 증가하였다. 비파괴평가파라미터의 지속적인 변화를 보이는 평면배열의 전위구조를 갖는 Cu-Zn에서와 달리, Cu에서는 전위셀구조가 발달하면서 더 이상의 큰 변화를 보이지 않았다.

전기비저항 측정에 의한 구리와 구리합금의 미시적 열화평가 (Evaluation of Microscopic Degradation of Copper and Copper Alloy by Electrical Resistivity Measurement)

  • 김정석;남승훈;현창용
    • 비파괴검사학회지
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    • 제30권5호
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    • pp.444-450
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    • 2010
  • 본 연구에서는 전류 4단자 전위차법을 이용한 전기비저항을 측정하여 반복피로손상을 받은 구리와 구리합금의 미시적 열화를 평가하였다. 서로 매우 다른 적층결함 에너지를 갖는 구리(Cu)와 구리합금(Cu-35Zn)에 대해 반복피로손상을 가하고 이들 재료에서 발달한 전위구조와 전기비저항 간의 관계를 연구하고자 하였다. Cu는 전위셀 하부구조를 형성하였지만, Cu-35Zn 합금은 피로사이클에 따라서 전위밀도는 증가하고 평면배열의 전위구조를 형성하였다. 전기비저항은 두 재료 모두에서 피로변형 초기 단계에서 급격하게 증가하였다. 더욱이, 피로시험 후 구리는 약 7 % 그리고 구리 합금은 약 6.5 % 변하였다. 이러한 일관적인 결과들로부터, 반복적인 피로에 의해 발달한 전위 셀구조는 평면배열의 전위구조보다도 전기비저항에 매우 민감한 것으로 판단된다.

나노 구리 분말의 냉간정수압 공정에 대한 치밀화 거동 해석 (Analysis of Densification Behavior of Nano Cu Powders during Cold Isostatic Pressing)

  • 윤승채;김형섭;이창규
    • 한국분말재료학회지
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    • 제11권4호
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    • pp.341-347
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    • 2004
  • In the study, a hybrid constitutive model for densification of metallic powders was applied to cold isostatic pressing. The model is based on a pressure-dependent plasticity model for porous materials combined with a dislocation density-based viscoplastic constitutive model considering microstructural features such as grain size and inter-particle spacing. Comparison of experiment and calculated results of microscale and nanoscale Cu powders was made. This theoretical approach is useful for powder densification analysis of various powder sizes, deformation routes and powder processing methods.

직교이방성 판 내의 다중 곡선균열 해석 (Analysis of Multiple Curved Cracks in An Orthotropic Plate)

  • 김만원;박재학
    • 대한기계학회논문집A
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    • 제27권6호
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    • pp.969-980
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    • 2003
  • The interactions between curved cracks are examined in an orthotropic plate and the effects of rectilinear anisotropy on the stress intensity factors are analyzed. The finite element alternating method (FEAM) is used in this study to get the stress intensity factors for the multiple curved cracks. To obtain analytical solutions, which is necessary in FEAM, the curved cracks are modeled as continuous distributions of dislocations, and integral equations are formulated for unknown dislocation density functions to satisfy the given resultant forces on the crack surfaces. Several basic problems are solved to verify the accuracy and efficiency of the proposed method and it can be found that present results show good agreements with the previously published results.

Interaction fields based on incompatibility tensor in field theory of plasticity-Part I: Theory-

  • Hasebe, Tadashi
    • Interaction and multiscale mechanics
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    • 제2권1호
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    • pp.1-14
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    • 2009
  • This paper proposes an interaction field concept based on the field theory of plasticity. Relative deformation between two arbitrary scales, e.g., macro and micro fields, is defined which can be implemented in the crystal plasticity-based constitutive framework. Differential geometrical quantities responsible for describing dislocations and defects in the interaction field are obtained, based on which dislocation density and incompatibility tensors are further derived. It is shown that the explicit interaction exists in the curvature or incompatibility tensor field, whereas no interaction in the torsion or dislocation density tensor field. General expressions of the interaction fields over multiple scales with more than three scale levels are derived and implemented into the present constitutive equation.

Theoretical analysis of overlay resisting crack propagation in old cement concrete pavement

  • Pan, Baofeng;Gao, Yuanyuan;Zhong, Yang
    • Structural Engineering and Mechanics
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    • 제52권4호
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    • pp.829-841
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    • 2014
  • The main purpose of this study is to determine the effect of overlay on the crack propagation. In order to simplify the problem, a cement concrete pavement is modeled as an elastic plate on Winkler foundation. To derive the singular integral equations, the Fourier transform and dislocation density function are used. Lobatto-Chebyshev integration formula, as a numerical method, is used to solve the singular integral equations. The numerical solution of stress intensity factor at the crack tip is derived. In order to examine the effect of overlay for resisting crack propagation, numerical analyses are carried out for a cement concrete pavement with an embedded crack and a concrete pavement with an asphalt overlay. Results show the significant factors that influence the crack propagation.

미세구조 분석을 이용한 저밀도 결함을 가진 GaN계 반도체 연구 (The study of GaN-based semiconductors with low-defect density by microstructural characterization)

  • 조형균
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2003년도 하계학술대회 논문집 Vol.4 No.1
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    • pp.424-427
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    • 2003
  • We have investigated the microstructural analysis of epitaxial lateral overgrowth (ELO), pendeoepitaxy (PE), and superlattice structures used as technology for the reduction of structural defects like dislocation in nitride semiconductors using transmission electron microscopy. We confirmed that the regrowth process such as ELO and PE is very effective technique on the reduction of threading dislocation (less than $10^6/cm^2$) in the specific area. However, to decrease the defect density in the whole nitride films and the suppress the generation of defect by regrowth, we should find the optimized conditions. Besides, the process using double PE and AlGaN/GaN superlattice structure showed no effect on the defect reduction up to now.

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열간 유동응력 예측을 위한 물리식 기반 동적 재결정 모델 (A Physically Based Dynamic Recrystallization Model for Predicting High Temperature Flow Stress)

  • 이호원;강성훈;이영선
    • 소성∙가공
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    • 제22권8호
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    • pp.450-455
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    • 2013
  • In the current study, a new dynamic recrystallization model for predicting high temperature flow stress is developed based on a physical model and the mean field theory. In the model, the grain aggregate is assumed as a representative volume element to describe dynamic recrystallization. The flow stress and microstructure during dynamic recrystallization were calculated using three sub-models for work hardening, for nucleation and for growth. In the case of work hardening, a single parameter dislocation density model was used to calculate change of dislocation density and stress in the grains. For modeling nucleation, the nucleation criterion developed was based on the grain boundary bulge mechanism and a constant nucleation rate was assumed. Conventional rate theory was used for describing growth. The flow stress behavior of pure copper was investigated using the model and compared with experimental findings. Simulated results by cellular automata were used for validating the model.

Al-Cu-Mg 합금에 있어서의 2차 결함조직 (The Secondary Defect Structure in Al-Cu-Mg Alloy)

  • 조현기;우기도
    • Applied Microscopy
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    • 제16권2호
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    • pp.14-24
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    • 1986
  • The interrelation of secondary defects, intermediate S' phase and aging condition in Al-2.0 wt% Cu-1.1 wt% Mg alloy is studied by transmission electron microscope. The results obtained in this study are as follows. 1. High density of dislocation loops, helices and stacking faults are observed in this specimen with aging treatment. 2. The number of dislocation loops and the width of loop free zone (LFZ) are increased with aging time. 3. The intermediate S' phase precipitates and grows on the dislocations and secondary defects. 4. The misfit dislocations are formed around intermediate S' phase. 5. It is thought that the helices appear to be produced by the climb of screw dislocations, while the dislocation loops appear to be formed both by condensation of vacancies into collapsed discs and by interaction of helices with screw of opposite sign.

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