• Title/Summary/Keyword: Direct solid analysis

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A Review on the Analytical Techniques for the Determination of Fluorine Contents in Soil and Solid Phase Samples (토양 및 고체시료 중 불소함량 측정기법)

  • An, Jinsung;Kim, Joo-Ae;Yoon, Hye-On
    • Journal of Soil and Groundwater Environment
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    • v.18 no.1
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    • pp.112-122
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    • 2013
  • Current status of soil contamination with fluorine and its source were investigated. The basic principles and procedures of various techniques for the analysis of fluorine contents in soil and solid phase samples were summarized in this review. Analysis of fluorine in solid matrices can be achieved by two types of techniques: (i) UV/Vis spectrophotometer or ion selective electrode (ISE) analysis after performing appropriate extraction steps and (ii) direct solid analysis. As the former cases, the standard method of Korean ministry of environment, alkali fusion-ISE method, pyrohydrolysis, oxygen bomb combustion, aqua regia digestion-automatic analysis, and sequential extraction-ISE method were introduced. In addition, direct analysis methods (i.e., X-ray fluorescence spectrometry and proton induced gamma-ray emission spectrometry) and atomic spectrometry combining with the equipment for introducing solid phase sample were also reviewed. Fluorine analysis techniques can be reasonably selected through site-specific information such as matrix condition, contamination level, the amount of samples and the principles of various methods for the analysis of fluorine presented in this review.

고상미량추출장치(SPME)를 이용한 유류 오염 지하수 평가 기법 연구

  • 조현정;백기태;박지연;양지원
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2001.09a
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    • pp.148-150
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    • 2001
  • Solid-phase microextraction (SPME) was investigated to understand the BTEX extraction behavior of SPME in groundwater. Analytical procedure was conducted In both conventional and headspace mode. And the conventional direct extraction method and the headspace analysis method were compared. Data obtained with direct and headspace SPME were very similar and showed successful results. In headspace analysis, the linearity was better and RSD (relative standard deviation, %) was smaller than direct extraction.

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A Cooling Roll Design and Prediction of Initial Conditions for Direct Rolling Process of Molten Metal (용탕직접압연공정의 초기조건예측 및 냉각로울 설계)

  • 강충길;김영도
    • Transactions of Materials Processing
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    • v.4 no.3
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    • pp.233-244
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    • 1995
  • Rolling force in the direct rolling(or twin-roll strip continuous casting) process fo semi-solid material has been computed using rigid-viscoplastic finite element method. Temperature distributions for calculations of rolling force and roll deformation are obtained from thermofluid analysis. Three dimensional roll deformation analysis has also been performed by using commercial package ANSYS. From the results, behavior of metal flow, rolling force and roll deformation have been investigated according to the process conditions of semi-solid direct rolling.

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Performance analysis modeling of axial direction direct flame rotary kiln reactors (축방향 직접화염 가열방식 로터리킬른 성능모형)

  • Hahn, Taekjin;Choi, Sangmin
    • 한국연소학회:학술대회논문집
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    • 2013.06a
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    • pp.59-60
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    • 2013
  • Rotary kiln furnace is one of the most widely used gas-solid reactors in the industrial field. Although the rotary kiln is a versatile system and has different size, approach to the reactor modeling can be generalized in terms of flow motion of the solid and gas phase, heat transfer and chemical reactions on purpose. In this paper, a performance analysis example case of axial direction direct flame rotary kiln is introduced.

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Finite element analysis of flow and heat transfer in solid particle moving beds of heat exchanger (고체입자를 이용한 열교환기에서의 유동 및 열전달의 유한요소해석)

  • Lee, Wan-Sul;Youn, sung-kie;Park, Sang-Il
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.22 no.4
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    • pp.743-752
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    • 1998
  • Numerical analysis for the flow and heat transfer in solid particle moving beds of heat exchangers is presented. The solid particle flow through the bundle of heat source tubes by the gravitational force. The heat energy is transferred through the direct contact of particles with the heat source tubes. The viscous-plastic fluid model and the convective heat transfer model are employed in the analysis. The flow field dominantly influences the total heat transfer in a heat exchanger. As the velocities of solid particles around the heat source tubes increase, the amount of heat transfer from the tubes increases. Some examples are presented to show the performance of the numerical model. The flow effect on the heat transfer is also studied through the examples.

Stress analysis of a postbuckled laminated composite plate

  • Chai, Gin-Boay;Chou, Siaw Meng;Ho, Chee-Leong
    • Structural Engineering and Mechanics
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    • v.7 no.4
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    • pp.377-386
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    • 1999
  • The stress distribution in a symmetrically laminated composite plate subjected to in-plane compression are evaluated using finite element analysis. Six different finite element models are created for the study of stresses in the plate after buckling. Two finite element modelling approaches are adopted to obtain the stress distribution. The first approach starts with a full model of shell elements from which sub-models of solid elements are spin-off The second approach adopts a full model of solid elements at the beginning from which sub-models of solid elements are created. All sub-models have either 1-element thickness or 14-element thickness. Both techniques show high interlaminar direct and shear stresses at the free edges. The study also provides vital information of the distribution of all components of stresses along the unloaded edges in length direction and also in the thickness direction of the plate.

Analysis of Ion Beam-Solid Interactions for Nano Fabrication (나노 패터닝을 위한 이온빔-고체 상호작용 분석)

  • Kim H.B.;Hobler G.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.10a
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    • pp.581-584
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    • 2005
  • Ion beam processing is one of the key technologies to realize mastless and resistless sub 50nm nano fabrication. Unwanted effects, however, may occur since an energetic ion can interact with a target surface in various ways. Depending on the ion energy, the interaction can be swelling, deposition, sputtering, re-deposition, implantation, damage, backscattering and nuclear reaction. Sputtering is the fundamental mechanisms in ion beam induced direct patterning. Re-deposition and backscattering are unwanted mechanisms to avoid. Therefore understanding of ion beam-solid interaction should be advanced for further ion beam related research. In this paper we simulate some important interaction mechanisms between energetic incident ions and solid surfaces and the results are compared with experimental data. The simulation results are agreed well with experimental data.

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Direct Solid Sample Analysis in the Moderate Power He Mip with the Spark Generation

  • S. R. Koirtyohann;Yong-Nam Pak
    • Bulletin of the Korean Chemical Society
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    • v.15 no.8
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    • pp.622-627
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    • 1994
  • Conducting solid samples are successfully analyzed with the spark ablation combined to the moderate power (500W) Helium Microwave Induced Plasma (He MIP). The relative standard deviations are in the range of 3-10% and the detection limits are around 50 ${\mu}$g $g^-1$. These values are higher than those of Ar MIP or Ar Inductively Coupled Plasma. Spark ablated particles are examined to investigate the analytical characteristics of the system.

Thermal Analysis for Solid Rocket Motor exposed to Fast Cook Off (급속가열 상황에 있는 고체 추진기관에 대한 열해석)

  • Doh, Young-Dae;Yoo, Ji-Chang;Kim, Chang-Kee;Lee, Do-Hyung;Ham, Hee-Cheol
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2009.05a
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    • pp.196-199
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    • 2009
  • The most important thing is to analyze the Fast Cook Off problem of the solid motor case exposed to direct flame is a heat transfer analysis. Heat causes degradation and ignition of the propellant. To archive an acceptable reaction level in Fast Cook Off, the rocket motor case generally must fail structurally prior to propellant ignition. We investigate the responses of the solid motor case exposed to Fast Cook Off by using finite element method for the thermal analysis.

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