• Title/Summary/Keyword: Dip-coated

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Anti-Corrosion Performance and Applications of PosMAC® Steel

  • Sohn, Il-Ryoung;Kim, Tae-Chul;Ju, Gwang-Il;Kim, Myung-Soo;Kim, Jong-Sang
    • Corrosion Science and Technology
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    • v.20 no.1
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    • pp.7-14
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    • 2021
  • PosMAC® is a brand of Zn-Mg-Al hot-dip coated steel sheet developed by POSCO. PosMAC® can form dense surface oxides in corrosive environments, providing advanced corrosion resistance compared to traditional Zn coatings such as GI and GA. PosMAC® 3.0 is available for construction and solar energy systems in severe outdoor environments. PosMAC®1.5 has better surface quality. It is suitable for automotive and home appliances. Compared to GI and GA, PosMAC® shows significantly less weight reduction due to corrosion, even with a lower coating thickness. Thin coating of PosMAC® provides advanced quality and productivity in arc welding applications due to its less generation of Zn fume and spatters. In repeated friction tests, PosMAC® showed lower surface friction coefficient than conventional coatings such as GA, GI, and lubricant film coated GA. Industrial demand for PosMAC® steel is expected to increase in the near future due to benefits of anti-corrosion and robust application performance of PosMAC® steel.

Effect of nano size $Y_2O_3$ addition on the superconducting properties and microstructure of YBCO thin film prepared by TFA-MOD method. (TFA-MOD 방법에 의한 YBCO 박막제조에서 nano size $Y_2O_3$ 첨가효과)

  • Park Jin-A;Kim Byung-Joo;Hong Gye-Won;Lee Hee-Gyoun;Yoo Jai-Moo;Kim Young-Kuk
    • Progress in Superconductivity and Cryogenics
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    • v.8 no.3
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    • pp.13-17
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    • 2006
  • The effect of the addition of the nano size $Y_2O_3$ powder on the microstructurte and superconducting properties of YBCO thin film deposited on LAO single crystalline substrate by TFA-MOD method was studied. Nano size $Y_2O_3$ powder was added to the stoichiometric precursor solution with a cation ratio of Y : Ba . Cu = 1 : 2 : 3 prepared using TFA as chelating agent. Precursor solutions with and without $Y_2O_3$ addition were coated on $LaAlO_3(100)$ single crystalline substrates by dip coating method. Calcination and conversion heat treatments were performed in controlled atmosphere containing moisture Current carrying capacity(Jc) of YBCO film was enhanced about 50% by $Y_2O_3$ doping and it is thought to be due to the better connectivity of YBCO grains and/or the flux pinning by the $Y_2O_3$ particles embedded in YBCO grains.

Solution deposition planarization for IBAD-MgO texture template

  • Ko, Kyeong-Eun;Kwon, O-Jong;Bea, Sung-Hwan;Yoo, Ja-Eun;Park, Chan;Oh, Sang-Soo;Park, Young-Kuk
    • Progress in Superconductivity and Cryogenics
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    • v.12 no.4
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    • pp.17-19
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    • 2010
  • In this work, the optimized process condition of chemical solution deposition which is used to planarize the surface of the metal tape (which is used to grow IBAD-MgO texture template) was investigated. $Y_2O_3$ films were dip-coated on the surface of the unpolished metal tape as the seed and barrier layer. The effects of $Y_2O_3$ concentration of the solution (0.5wt.%, 1.3wt.%, 2.8wt.%, 5.6wt.%) and the number of coatings on the surface morphology and barrier capability against the diffusion from the metal tape were examined. The surface morphology and the thickness of the film were observed using the scanning electron microscope and the atomic force microscope. The presence of elements in metal tape on the film surface was analyzed using the auger electron spectroscopy. The $Y_2O_3$ film thickness increases with increasing the $Y_2O_3$ concentration in the solution, and the surface became smoother with increasing the number of coating cycles. The best result was obtained from the $Y_2O_3$ film coated 4 cycles using 2.8wt.% solution.

Preparation and Properties of Y2O3-Doped ZrO2 Films on Etched Al Foil by Sol-Gel Process

  • Chen, Fei;Park, Sang-Shik
    • Korean Journal of Materials Research
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    • v.25 no.2
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    • pp.107-112
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    • 2015
  • The oxide films formed on etched aluminum foils play an important role as dielectric layers in aluminum electrolytic capacitors. $Y_2O_3$-doped $ZrO_2$ (YZ) films were coated on the etched aluminum foils by sol-gel dip coating, and the electrical properties of YZ-coated Al foils were characterized. YZ films annealed at $450^{\circ}C$ were crystallized into a cubic phase, and as the $Y_2O_3$ doping content increased, the unit cell of $ZrO_2$ expanded and the grain size decreased. The etch pits of Al foils were filled by YZ sol when it dried at atmospheric pressure after repeating for several times, but this step could essentially be avoided when being dried in a vacuum. YZ-coated foils indicated that the specific capacitance and dissipation factor were $2-2.5{\mu}F/cm^2$ and 2-4 at 1 kHz, respectively, and the leakage current and withstanding voltage of films approximately 200 nm thick were $5{\times}10^{-4}A$ at 21 V and 22 V, respectively. After being anodized at 500 V, the foils exhibited a specific capacitance and dissipation factor of $0.6-0.7{\mu}F/cm^2$ and 0.1-0.2, respectively, at 1 kHz, while the leakage current and withstanding voltage were $2{\times}10^{-4}-3{\times}10^{-5}A$ at 400 V and 420-450 V, respectively. This suggests that YZ film is a promising dielectric that can be used in high voltage Al electrolytic capacitors.

The Preparation of High $J_c$ YBCO Films by DCA-MOD Method (DCA-MOD 법에 의한 High $J_c$ YBCO 박막의 제조)

  • Kim, Byeong-Joo;Kim, Hye-Jin;Yi, Keum-Young;Lee, Jong-Beum;Kim, Ho-Jin;Lee, Hee-Gyoun;Hong, Gye-Won
    • Progress in Superconductivity
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    • v.8 no.1
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    • pp.59-64
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    • 2006
  • High $J_c\;YBa_2Cu_3O_x$ superconducting films were fabricated by MOD method using fluorine-free dichloroacetic acid(DCA) as chelating solvent for preparing precursor solution. Coating solutions were prepared by dissolving Y-, Ba- and Cu-acetates in DCA solvent followed by drying in rota vapor to obtain the blue gel that is diluted in methanol and 2-methoxyethanol for adjusting the cation concentration. DCA-MOD precursor solution was coated on a single crystal(001) $LaAlO_3(LAO)$ substrate by a dip coating method with a speed of 25 mm/min. Coated films were calcined at lower temperature up to $500^{\circ}C$ in flowing oxygen atmosphere with a 7.2% humidity. Conversion heat treatment was performed at various temperatures of $780{\sim}810^{\circ}C$ for 2 h in flowing Ar gas containing 1000 ppm oxygen with a humidity of 9.45%. SEM observations showed that films have very dense microstructures for the films prepared at the temperature higher than $800^{\circ}C$ regardless of diluting solvent; methanol or 2-methoxyethanol. X-ray diffraction analysis showed that YBCO grains grew with a (001) preferred orientation. A High critical current density($J_c$) of 1.28 $MA/cm^2$(@77 K and self-field) was obtained id. the YBCO film prepared using 2-methoxyethanol as a solvent.

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Effect of heat-treatment parameter of YBCO film by TFA-MOD process (TFA-MOD법에 의한 YBCO 박막의 열처리변수 효과)

  • Jang, Seok-Hern;Lim, Jun-Hyung;Kim, Kyu-Tae;Lee, Jin-Sung;Yoon, Kyung-Min;Joo, Jin-Ho;Lee, Hee-Gyoun;Hong, Gye-Won
    • Progress in Superconductivity
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    • v.7 no.2
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    • pp.135-139
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    • 2006
  • We fabricated YBCO coated conductors (CCs) by TFA-MOD process and evaluated microstructure, texture formation, and critical temperature ($T_c$) and current ($I_c$). YBCO precursor solution was synthesized using metal-trifluoroacetates and dip coated on $LaAlO_3$(LAO) substrate. The phase formation and microstructure was characterized by X-ray diffraction and scanning electron microscopy (SEM) and the degree of texture was evaluated by pole-figure analysis. The CC was heat-treated in various calcining temperatures ($370^{\circ}C-460^{\circ}C$) and firing temperatures ($750^{\circ}C-800^{\circ}C$). As fired at $775^{\circ}C$ for 4h, the CC had the highest $T_c$ of 89.5 K and $I_c$ of 40 A/cm-width ($J_c=2.0\;MA/cm^2$). Microstructural observation indicated that the YBCO film was dense and homogeneous and had a strong cube texture without formation of second phase and its in-plane full-width at half-maxima; $5.2^{\circ}$ under optimum condition.

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A Study on the Slitting Working by Finite Element Analysis (유한요소해석에 의한 슬리팅가공에 관한 연구)

  • Han, K.T.;Seo, J.K.
    • Journal of Power System Engineering
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    • v.5 no.3
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    • pp.56-63
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    • 2001
  • A slitter is a sort of machinery to cut sheet materials in rolls continuously in the longitudinal direction. Recently slitter line users have requiring higher quality and precision in products in addition to high productivity. A finite element analysis has been performed to investigate the effect of processing factors on shear planes in the slitting of Shrinkage Band(S,K.B.). For the analysis, Hot-dip 55% aluminum-zinc alloy-coated steel sheets and coils(SAZCC) is selected as a material. The results obtained are that deformation was concentrated along the very narrow zone and the maximum slitting load decreases by increasing the knife clearance. Also effective strain decreases according to the clearance increases.

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Dense Ceramic-metal Composite Inorganic Membranes for Oxygen Separation (산소 분리를 위한 무공성 세라믹- 금속 복합 무기막)

  • 김진수
    • Proceedings of the Membrane Society of Korea Conference
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    • 2002.05a
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    • pp.35-41
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    • 2002
  • Dense oxygen ionic conducting materials can be used for oxygen separation membranes at high temperatures. However, they show relatively low permeation flux because of their large resistances. To reduce resistances and improve the oxygen permeation flux, thin dense yttria-stabilized-zirconia (YSZ)/Pd composite dual-phase membranes were fabricated by a new approach that combines the reservoir method and chemical vapor deposition (CVD). A thin porous YSZ layer was coated on a porous alumina support by dip-coating the YSZ suspension. A continuous Pd phase was formed inside pores of the YSZ layer by the reservoir method. The residual pores of the YSZ/Pd layer were plugged with yttria/zirconia by CVD to ensure the gas tightness of the membranes. The oxygen permeation fluxes through these composite membrane were 2.0$\times$10$^{-8}$ mol/cm$^2$.s and 4.8$\times$10$^{-8}$ mol/cm$^2$.s at 105$0^{\circ}C$ when air and oxygen were used as the permeate gases, respectively. These oxygen permeation values are about 1 order of magnitude higher than those of pure YSZ membranes prepared under similar conditions.

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Energy Saving Properties of Sol Gel Dip Coated Indium Tin Oxide Films on a Glass Pane (창유리 위에 졸겔 담금 방법으로 코팅된 인듐 주석 산화막의 에너지 절약 특성)

  • 정형진;이희형;이동헌;이전국
    • Journal of the Korean Ceramic Society
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    • v.29 no.1
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    • pp.48-52
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    • 1992
  • Indium tin oxide (ITO) layers are of considerable interest on account of the combination of properties they provide high electrical conductivity, high infrared reflection with high solar energy transmission, high transmission in the visible range. We are concerned about the variation of the spectral transmittances and sheet resistances as the thickness of SiO2-ZrO2 barrier layer and ITO layers and heat treating conditions are changed. Transmittances and reflectivities were studied by measuring UV-VIS-NIR-, FT-IR spectroscopy. ITO films are crack free, homogeneous and of polycrystalline cubic structure. The microstructure of good ITO films shows a narrow grain size distribution and mean value of 100 nm. The selectivity of absorbing properties is improved by increasing the thickness of ITO films. The increase of sheet resistance of ITO films are due to the increase in the reaction between films and glass substrate.

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Sloshing Flow of Highly-Viscous Fluid in a Rectangular Box (사각용기에서 발생하는 고점성 유체의 슬로싱 유동)

  • park, Jun Sang
    • Journal of the Korean Society of Visualization
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    • v.17 no.3
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    • pp.39-45
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    • 2019
  • A study on the sloshing flow of highly-viscous fluid in a rectangular box was made by both of theoretical approach and experimental visualization method. Assuming a smallness of external forcing to oscillate the container, it was investigated a linear sloshing flow of highly-viscous fluid utilizing asymptotic analysis by Taylor-series expansion as a small parameter Re (≪1) in which Re denotes Reynolds number. The theory predict that, during all cycles of sloshing, a linear shape of free surface will prevail in a bulk zone and it has confirmed in experiment. The relevance of perfect slip boundary condition, adopted in theoretical approach, to the bulk zone flow at the container wall was tested in experiment. It is found that quasi-steady coated thin film, which makes a lubricant layer between bulk flow and solid wall, is generated on the wall and the film makes a role to perfect slip boundary condition.