• Asian Journal of Atmospheric Environment
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• 제11권4호
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• pp.283-299
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• 2017

An analytical method using high-performance liquid chromatography (HPLC) with fluorescence (FL) detection was developed for simultaneously analyzing 10 polycyclic aromatic hydrocarbons (PAHs) and 18 nitro-derivatives of PAHs (NPAHs). The two-dimensional HPLC system consists of an on-line clean-up and reduction for NPAHs in the 1st dimension, and separation of the PAHs and the reduced NPAHs and their FL detection in the 2nd dimension after column-switching. To identify an ideal clean-up column for removing sample matrix that may interfere with detection of the analytes, the characteristics of 8 reversed-phase columns were evaluated. The nitrophenylethyl (NPE)-bonded silica column was selected because of its shorter elution band and larger retention factors of the analytes due to strong dipole-dipole interactions. The amino-substituted PAHs (reduced NPAHs), PAHs and deuterated internal standards were separated on polymeric octadecyl-bonded silica (ODS) columns and by dual-channel detection within 120 min including clean-up and reduction steps. The limits of detection were 0.1-9.2 pg per injection for PAHs and 0.1-140 pg per injection for NPAHs. For validation, the method was applied to analyze crude extracts of fine particulate matter ($PM_{2.5}$) samples and achieved good analytical precision and accuracy. Moreover, the standard reference material (SRM1649b, urban dust) was analyzed by this method and the observed concentrations of PAHs and NPAHs were similar to those in previous reports. Thus, the method developed here-in has the potential to become a standard HPLC-based method, especially for NPAHs.

• Structural Engineering and Mechanics
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• 제20권2호
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• pp.143-160
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• 2005

Modal analysis of cracked cantilever composite beams, made of graphite-fibre reinforced polyamide, is studied. By using the finite element and component mode synthesis methods, a numeric model applicable to investigate the vibration of cracked composite beams is developed. In this new approach, from the crack section, the composite beam separated into two parts coupled by a flexibility matrix taking into account the interaction forces. These forces are derived from the fracture mechanics theory as the inverse of the compliance matrix calculated with the proper stress intensity factors and strain energy release rate expressions. Numerical results are obtained for modal analysis of composite beams with a transverse non-propagating open crack, addressing the effects of the location and depth of the crack, and the volume fraction and orientation of the fibre on the natural frequencies and mode shapes. By means of modal data, the position and dimension of the defect can be found. The results of the study confirmed that presented method is suitable for the vibration analysis of cracked cantilever composite beams. Present technique can be easily extended to composite plates and shells.

• 한국정보처리학회:학술대회논문집
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• 한국정보처리학회 2003년도 추계학술발표논문집 (하)
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• pp.1363-1366
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• 2003

기존 연구에서 3차원 공간 위상 관계 연산자를 정의하는 방법은 2차원 공간 위상 관계 정의를 위해 주로 사용되는 공간 교차 방법을 단순히 3차원으로 확장해서 정의하는 방식이다. 그러나 기존의 방법에 의해 정의된 3차원 위상 관계 연산자로는 3차원 데이터베이스를 이용한 실제 응용시스템에서 고려되어야 하는 특수한 위상 관계 분석을 수행하기 어렵다. 따라서 이 논문에서는 실제 응용에서 적용 될 수 있는 특수한 3차원 위상 관계를 정의하기 위하여 x,y 좌표와 z좌표를 분리해서 고려하는 새로운 기법을 제안한다. 또한 제안한 방법을 이용하여 새로운 3차원 공간 위상 관계 연산자들을 정의하고 구체적인 알고리즘을 제시한다.

• Asian-Australasian Journal of Animal Sciences
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• 제24권2호
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• pp.272-278
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• 2011

Bovine whey protein expression patterns of colostrum are much different from that of milk. Moreover, bovine colostrum is an important source of protective, nutritional and developmental factors for the newborn. However, to our knowledge, no research has been performed to date using a comparative proteomic method on the changes in the bovine whey proteome during the transition from colostrum to milk. This study therefore separated whey protein of days 1, 3, 7 and 21 after calving using two dimension electrophoresis. Differentially expressed proteins at different collection times were identified using high-performance liquid chromatography in tandem with mass spectrometry (LC/MS) and validated by enzyme-linked immunosorbent assay (ELISA) in order to understand the developmental changes in the bovine whey proteome during the transition from colostrum to milk. The expression patterns of whey protein of days 1 and 3 post-partum were similar except that immunoglobulin G was down-regulated on day 3, and four proteins were found to be down-regulated on days 7 and 21 compared with day 1 after delivering, including immunoglobulin G, immunoglobulin M, albumin, and lactotransferrin, which are involved in immunity and molecule transport. The results of this study confirm the comparative proteomic method has the advantage over other methods such as ELISA and immunoassays in that it can simultaneously detect more differentially expressed proteins. In addition, the difference in composition of milk indicates a need for adjustment of the colostrum feeding regimen to ensure a protective immunological status for newborn calves.

• Wind and Structures
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• 제38권1호
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• pp.1-13
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• 2024

In order to effectively simulate nonstationary stochastic turbulent wind fields, four separation hybrid (SEP-H) models are proposed in the present study. Based on the assumption that the lateral turbulence component at one single-point is uncorrelated with the longitudinal and vertical turbulence components, the fluctuating wind is separated into 2nV-1D and nV1D nonstationary stochastic vector processes. The first process can be expressed as double proper orthogonal decomposition (DPOD) or proper orthogonal decomposition and spectral representation method (POD-SRM), and the second process can be expressed as POD or SRM. On this basis, four SEP-H models of nonstationary stochastic turbulent wind fields are developed. In addition, the orthogonal random variables in the SEP-H models are presented as random orthogonal functions of elementary random variables. Meanwhile, the number theoretical method (NTM) is conveniently adopted to select representative points set of the elementary random variables. The POD-FFT (Fast Fourier transform) technique is introduced in frequency to give full play to the computational efficiency of the SEP-H models. Finally, taking a long-span bridge as the engineering background, the SEP-H models are compared with the dimension-reduction DPOD (DR-DPOD) model to verify the effectiveness and superiority of the proposed models.

• 대한인간공학회지
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• 제33권2호
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• pp.125-134
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• 2014

Objective: The purpose of this study is to evaluate integral seat desk used in universities through comparison of real dimension values of the desk with KS/ISO standard and questionnaire survey. Background: School furniture that helps students sit comfortably for longer periods of time and allows for better concentration on learning is important. However, seat and desk have been generally designed based on the industry practice rather than user's anthropometry, and seats and desks used in universities of Korea have not been ergonomically evaluated. Method: Real 13 dimensions of the desk used in K University were measured using tape measure and inclinometer, and the dimension values were compared to the KS standard of desk and chair for lecture room (KS G 4210) and ergonomic design principles found in relevant references. Subjective appropriacies and preference for the desk were investigated based on questionnaire survey, in which 121 (male: 91, female: 30) college students participated. Results: Several dimensions for the desk and chair investigated except desk depth and width, leg room width, seat width have not met the KS standard, but all dimensions satisfied ergonomic design principles available in references. The questionnaire survey revealed that appropriacies for desk surface size, seat pan depth, seat pan cushion and backrest curvature were under middle point of 3.0, and that those for the other dimensions showed higher scores exceeding 3.0. Conclusion: The integral seat desk widely used in universities showed some design problems in terms of standards of KS G 2010 and KS G 4210, and ergonomic design principles. Compared to the general desk with separated desk and seat, subjective preference on the integral seat desk was low. Application: This would be used as a valuable guideline when designing or choosing new integral seat desk with high satisfaction of students.

• 한국공간정보시스템학회 논문지
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• 제9권3호
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• pp.1-16
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• 2007

공간 데이터 웨어하우스는 공간 의사결정을 지원하는 시스템으로 공간 데이터 큐브를 이용한다. 공간 데이터 큐브에는 분석의 기준이 되는 공간 차원테이블과 분석의 대상이 되는 공간 사실테이블들로 구성되는데 의사결정 지원을 위해서는 공간 차원테이블의 개념계층 지원과 공간 사실테이블의 요약정보 제공이 필요하다. 그러나 기존의 연구들은 공간 개념계층에 대해서만 연구하였을 뿐 공간 요약정보에 대한 연구가 미비하였다. 따라서 본 논문에서는 공간 데이터 웨어하우스에서 공간 공간 요약정보를 위한 공간 집계연산에 대하여 제안한다. 본 논문에서는 공간 집계연산을 숫자화 집계연산과 객체화 집계연산으로 나누어 제안한다. 숫자화 집계연산은 공간 분석의 결과로 숫자 형태의 데이터를 반환하며, 객체화 집계연산은 공간 객체 형태로 결과를 반환한다. 본 논문에서는 확장된 공간 데이터 자료구조를 제공하여 공간 집계연산의 효율성을 높인다.

• Korean Journal of Acupuncture
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• 제26권2호
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• pp.1-13
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• 2009

Objective: Optical Coherence Tomography (OCT) has emerged as an important optical imaging modality in non-invasive medical diagnostics. Hence, the aim of this study is to measure the similarity of the diagnosis by a traditional method using doctor's hand for feeling of pulse and by the non-contact/non-invasive pulse analyzing system using OCT on Chon(寸), Kwan(關), Chuk(尺). Method: Four korean medical doctors and the non-contact/non-invasive pulse analyzing system using OCT have measured the rapidity, the dimension, and the power of pulse waves of 25 volunteers. First, four korean medical doctors measured pulse waves of volunteers. During measuring, four doctors were separated from each other and so were volunteers. And then, the pulse waves of volunteers were measured by OCT. This was performed on the right Chon(寸), Kwan(關), Chuk(尺). Results: The study showed that the traditional method and the OCT based method had the 88% matches on the values of the slow and rapid pulse condition (遲數), 64% matches on the values of the small and big pulse condition(微細弱緩大[洪]), and 72% matches on the values of the weak and strong pulse condition(虛實). Conclusions: Based on the high similarities of the measurements of two approaches, we suggest that the OCT based pulse diagnosis method is useful for compensating the traditional method for the pulse diagnosis.

• International Journal of Industrial Entomology and Biomaterials
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• 제5권2호
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• pp.163-170
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• 2002

In this paper, silk fibroin (SF)/polyurethane (PU) blend films were fabricated to develop a new biomaterial for biomedical applications. These blend films were prepared using formic acid as a cosolvent, and structural characteristics and properties of blend films were investigated. FTIR results suggested that there was no specific interaction between SF and PU, implying molecular immiscibility in SF/PU blend films. Furthermore, it was revealed by XRD method that the crystalline region of blend components was not perturbed by counterpart polymers. The degree of phase separation of SF/PU blend films was diminished by increasing PU content in blend. Especially, the blend with 70% content of PU showed no evidence of macro-phase separation in SEM observation. However, SF/PU blend (70/30) was revealed to be phase-separated in a lower dimension confirmed by DMTA measurement. TGA result showed that thermal decomposition temperature of blend film was slightly decreased compared to those of SF and PU polymer itself, Though mechanical properties of SF/PU blend films were not good enough due to the solvent, blood compatibility of PU can be enhanced markedly by mixing with SF for SF/PU blend film.

• Steel and Composite Structures
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• 제31권3호
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• pp.217-232
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• 2019

Modular steel buildings consist of prefabricated room-sized structural units that are manufactured offsite and installed onsite. The inter-module connections must fulfill the assembly construction requirements and soundly transfer the external loads. This work proposes an innovative assembled connection suitable for modular buildings with concrete-filled steel tube columns. The connection uses pretensioned strands and plugin bars to vertically connect the adjacent modular columns. The moment-transferring performance of this inter-module connection was studied through monotonic and cyclic loading tests. The results showed that because of the assembly construction, the connected sections were separated under lateral bending, and the prestressed inter-module connection performed as a weak semirigid connection. The moment strength at the early loading stage originated primarily from the contact bonding mechanism with the infilled concrete, and the postyield strength depended mainly on the tensioned strands. The connection displayed a self-centering-like behavior that the induced deformation was reversed during unloading. The energy dissipation originated primarily from frictional slipping of the plugin bars and steel strands. The moment transferring ability was closely related to the section dimension and the arrangements of the plugin bars and steel strands. A simplified strength calculation and evaluation method was also proposed, and the effectiveness was validated with the test data.