• Title/Summary/Keyword: Diffraction angle

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The Crystal and Molecular Structure of Maltitol

  • Park, Young-Ja;Shin, Jung-Mi;Shin, Whan-Chul;Suh, Il-Hwan
    • Bulletin of the Korean Chemical Society
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    • v.10 no.4
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    • pp.352-356
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    • 1989
  • The crystal structure of maltitol, 4-O-${\alpha}$ -D-glucopyranosyl-D-glucitol, has been determined by X-ray diffraction method. The crystal is orthorhombic with cell parameters of a = 8.170(1), b = 12.731(1), c = 13.679(3) ${\AA}$, space group $P2_12_12_1$ and z = 4. The structure was solved by direct methods and refined to R = 0.030 for 1181 observed reflections measured on a diffractometer. The ${\alpha}$-glucose ring has chair conformation. The carbon atom chain of the glucitol residue has the bent, ap, Psc, Psc conformation. The angle at the ring oxygen atom is $112.6^{\circ}$ and the one at the glucosidic oxygen is $117.1^{\circ}$. The molecules are linked by very complicated hydrogen bonds, and there is an intramolecular hydrogen bond between O(1') and O(2').

Surface-Plasmon Assisted Transmission Through an Ultrasmall Nanohole of ~ 10 nm with a Bull's Eye Groove

  • Kim, Geon Woo;Ko, Jae-Hyeon;Park, Doo Jae;Choi, Seong Soo;Kim, Hyuntae;Choi, Soo Bong
    • Journal of the Korean Physical Society
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    • v.73 no.11
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    • pp.1698-1702
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    • 2018
  • We simulate the light transmission through an extremely small nanoscale aperture having a 10 nm diameter punctured in a metal film positioned at the center of a plasmonic bull's eye grating. A considerable directive emission of transmitted light with a divergence angle of 5.7 degrees was observed at $10{\mu}m$ from the nanohole opening at the frequency of surface plasmon polariton excitation, an confirmed by measuring the distance dependent transmission amplitude. Observations of the electric field in cross-sectional, near-field, and far-field views near-field enhancement associated with the surface plasmon excitation, and the interference of the electric field light through the nanohole in the near-field region is responsible for such a considerable directive emission.

MAGNETIC AND MAGNETO-OPTICAL PROPERTIES OF Co-BASED MULTILAYERED FILMS PREPARED BY ELECTRON-BEAM EVAPORATION

  • Lee, Y.P.;Lee, B.J.;Park, H.K.;Kim, S.K.;Kang, J.S.;Jeong, J.I.
    • Journal of the Korean Vacuum Society
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    • v.4 no.S2
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    • pp.24-29
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    • 1995
  • The magnetic amd magneto-optical(MO)properties of Co-based multilayered(ML)films are known to vary sensitively according to the manufacturing methods and the film microstructures. Co/Pd and Co/Pt ML films with ultrathin layers of Co were prepared by alternating deposition in an ultrahigh-vacuum physical-vapor-deposition system. The individual layer thicknesses of the samples were estimated making use of the angular positions of x-ray diffraction peaks. The magnetic and MO properties were investigated, and correlated systematically to the structural parameters of the films. A Kerr spectrometer was self-manufactured to measure the MO properties such as Kerr rotation angle, ellipticity and reflectivity. The rms surface roughness was also measured using atomic force microscopy. Some of the samples showed good properties for MO medium, such as large perpendicular magnetic anisotropy and Kerr rotation, and perfect squareness of the magnetic hysteresis loop.

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Characteristic of Wave Diffraction and Reflection for Irregular Waves in SWASH Model Around Small Port Structures (소규모 항만 구조물 주변에서 불규칙파에 대한 SWASH 모형의 반사 및 회절)

  • Kwon, Kyong Hwan;Park, Chang Wook;Park, Il Heum;Kim, Jong Hoon
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.31 no.6
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    • pp.468-477
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    • 2019
  • The numerical model of Boussinesq approximation, which is mainly used for evaluating the port calmness due to the irregular waves, has a limit of applicability of lattice size in ports such as marinas with narrow port openings of around 30m. The SWASH model controls the partial reflection according to the depth, porosity coefficient and structure size when applying the reflected wave incident on the structure and terrain. In this study, the partial reflection evaluation at the front of the structure according to the bottom shape and the shape of the structure are examined. In order to evaluate the reproducibility of the model due to the diffraction waves entering the term, the area of incidence at right angles and inclination of the structure is constructed and compared with the diffraction theory suggested by Goda et al. (1978). The experimental results of the sectional structure reflectances calculated as the depth mean show reflectances similar to the approximate values of the reflectances presented by Stelling and Ahrens (1981). It is considered that the reflected wave is well reproduced according to the control of the reflected wave at the boundary and the shape and topography of the structure. Compared with previous studies to examine the diffraction of the wave incident from the breakwater opening, the wave incidence angle and the shape of the diffraction wave are very similar to the theoretical values, but both oblique and rectangular incidence In the case where the direction concentration is small, the diffraction degree is underestimated in some sections with the crest ratio of 0.5 to 0.6.

Fabrication of patterned substrate by wet process for biochip (습식 공정법에 의한 바이오칩 용 패터닝 기판 제조)

  • Kim, Jin-Ho;Lee, Min;Hwang, Jong-Hee;Lim, Tae-Young;Kim, Sae-Hoon
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.19 no.6
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    • pp.288-292
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    • 2009
  • Hydrophobic/hydrophilic patterned substrates were fabricated on a glass substrate by a liquid phase deposition (LPD) method. Hydrophobic surface was obtained by modifying ZnO thin films with a rough surface using a fluoroalkyltrimethoxysilane (FAS) and hydrophilic surface was prepared by decomposing FAS on an exposed to UV light. The hexagonal ZnO rods were perpendicularly grown by LPD method on glass substrates with a ZnO seed layer. The diameter and thickness of hexagonal ZnO rods were increased as a function of increases of immersion time. The surface morphology, thickness, crystal structure, transmittance and contact angle of prepared ZnO thin films were measured by field emission scanning electron microscopy (FE-SEM), X-ray diffraction (XRD), UV-visible spectrophotometer (UV-vis) and contact angle measurement. Hydrophilic ZnO thin films with a contact angle of $20^{\circ}{\sim}30^{\circ}$ were changed to a hydrophobic surface with a contact angle of $145^{\circ}{\sim}161^{\circ}$ by a FAS surface treatment. Prepared hydrophobic surface was pattered by an irradiation of UV light using shadow mask with $300\;{\mu}m$ or 3 mm dot size. Finally, the hydrophobic surface exposed to UV light was changed to a hydrophilic surface.

Nonlinear Diffraction of Incident Waves with Side-band Disturbances by a Thin Wedge (변조된 입사파의 쐐기에 의한 산란)

  • 지원식;최항순
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.3 no.1
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    • pp.45-53
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    • 1991
  • The nonlinear forward diffraction of a modulated wave train by a thin wedge has been studied analytically. Since the physical variables involved in the problem have vastly different scales, the multiple scale expansion method has been used to obtain an approximate solution. To simplify the problem. the wedge is assumed to be thin and the parabolic approximation is utilized. The wave evolution can be described by a kind of the cubic Schrodinger equation. which consists of the linear time evolution. the lateral dispersion and the nonlinearity. Numerical results indicate that the nonlinearity. which it defined by the ratio of the ratio of the incident wave to the wedge angle. governs the amplitude and the stability of diffracted waves. The instability of dirffracted waves becomes more pronounced as the nonlinearity increases and the modulation ratio decreases. It is also found that the stem waves. initially developed along the wedge. can not sustain for a long time.

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Rapid Thermal Annealing of GaN EpiLayer grown by Molecular Beam Epitaxy (MBE로 성장한 GaN 에피층의 급속 열처리)

  • Choi, Sung-Jai;Lee, Won-Sik
    • The Journal of the Institute of Internet, Broadcasting and Communication
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    • v.10 no.1
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    • pp.7-13
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    • 2010
  • We have investigated effects of the rapid thermal annealing of GaN epilayers by molecular beam epitaxy in nitrogen atmosphere. The improvement of structural properties of the samples was observed after rapid thermal annealing under optimum conditions. This improvement in crystal quality is due to a reduction of the spread in the lattice parameter in epilayers. The annealing has been performed in a rapid thermal annealing furnace at $950^{\circ}C$. The effect of rapid thermal annealing on the structural properties of GaN was studied by x-ray diffraction. The Bragg peak shifts toward larger angle as the annealing time increases. As the thermal treatment time increases, FWHM(full width at half maximum) of the peak slightly increase with its decreases followed and it increases again. Results demonstrate that rapid thermal annealing did not always promote qualities of GaN epilayers. However, rapid thermal annealing under optimum conditions improve structural properties of the samples, elevating their crystal quality with a reduction of inaccuracy in the lattice parameter of the epilayers.

Wavelength tunability of XeCl laser pumped double-resonator dye laser for DIAL (DIAL용 XeCl 레이저펌핑 쌍공진기색소레이저의 파장가변특성)

  • 이용우;이주희
    • Korean Journal of Optics and Photonics
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    • v.7 no.3
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    • pp.238-243
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    • 1996
  • We have developed XeCl laser pumped double-resonator Dye laser and two-stage amplifier system, and generated simultaneously of alternatively two wavelengths suitable in DIAL system. The developed double-resonator is composed of 1st and 2nd diffraction orders on light incidence angle in grazing-incidence grating method with 1200 g/mm. We have obtained spectral linewidth below 10 pm and the total efficiency dependent on pump energy over 6%. The tuning ranges dependent on 1st and 2nd diffraction orders are 434~470 nm and 436~468 nm, respectively. The amplification gain and rine-450 dye laser by using the double-resonator laser system and measured the distribution of $NO_2$ concentration over Suwon as the result of transmission of laser output of 6 mJ in this DIAL system. Consequently, we have confirmed that the developed dye laser system is very useful as the tunable source for DIAL.

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Evaluation of the Surface Crack by a Large Aperture Ultrasonic Probe (대구경 초음파 탐촉자를 이용한 표면균열 평가)

  • Cho, Yong-Sang;Kim, Jae-Hoon
    • Journal of the Korean Society for Nondestructive Testing
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    • v.24 no.2
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    • pp.180-185
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    • 2004
  • Conventional ultrasonic examination to detect micro and small surface cracks is based on the pulse-echo technique using a normal immersion focused transducer with high frequency, or an angle-beam transducer generating surface waves. It is difficult to make an automatic ultrasonic system that can detect micro and small surface cracks and position in a large structure like steel and ceramic rolls, because of the huge data of inspection and the ambiguous position data of the transducer. In this study, a high-precision scanning acoustic microscope with a 10MHz large-aperture transducer has been used to assess the existence, position and depth of a surface crack from the real-time A, B, C scans obtained by exploiting the ultrasonic diffraction. The ultrasonic method with large aperture transducer has improved the accuracy of the crack depth assessment and also the scanning speed by ten times, compared with the conventional ultrasonic methods.

Depth Sizing of Notch Fatigue Crack Using Diffracted Ultrasonic Wave (회절초음파를 이용한 노치 피로균열의 균열깊이 평가)

  • Jin, Mei-Ling;Lee, Tae-Hun;Park, Byung-Jun;Jhang, Kyung-Young
    • Journal of the Korean Society for Nondestructive Testing
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    • v.29 no.5
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    • pp.405-414
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    • 2009
  • This paper proposed a methodology based on ultrasonic diffraction technique to inspect the depth of a crack initiated from a notch of CT specimen by fatigue test, and its usefulness was verified by experiments. Especially, in order to identify accurately the diffractive waves from the crack tip in the situation where there are extra diffractive elements such as a notch, we have tried imaging by transducer scan and analyzed the propagation path of diffracted wave. Two specimens with and without a crack were experimented. Higher frequency and larger refractive angle of transducer showed a tendency to decrease the error in the measurements, and the measured crack depth showed an error less than 0.38 mm in case of 4 MHz $60^{\circ}-60^{\circ}$. The proposed methodology is applicable to weak diffractive sources, and so that it would be useful to inspect micro cracks and for their depth sizing.