• Proceedings of the Korean Society of Precision Engineering Conference
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• 1996.11a
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• pp.954-958
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• 1996

An analysis method for the reliability of ceramic structures subjected to thermal shocks is presented, Flaws with the size of given probability distribution function are assumed to be distributed at random with a certain density per unit volume in the structures. Criterions for crack instability are derived for brittle solids under general thermal stresses. A probabilistic failure model is presented to study the probability of crack instability for blittle solids containing cracks with uncertain crack size. The reliabilities of brittle structures are evaluated based on the weakest-link hypothesis, which states that a structure fails when the cracks in any differential volume become unstable. A numerical example is given to demonstrate the application of the proposed method.

• Proceedings of the Korean Vacuum Society Conference
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• 2012.02a
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• pp.555-555
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• 2012

The thermal stability of poly(sodium 4-styrenesulfonate) intercalated graphite oxide has been investigated using a differential scanning calorimeter. The poly(sodium 4-styrenesulfonate) intercalated graphite oxide composite shows a prominent exothermic reaction near $207^{\circ}C$ and an endothermic reaction near $453^{\circ}C$. Graphite oxide is responsible for the exothermic reaction while the endothermic reaction is caused by the poly(sodium 4-styrenesulfonate) used in the synthesis of poly(sodium 4-styrenesulfonate) intercalated graphite oxide. The onset temperature of the exothermic reaction of poly(sodium 4-styrenesulfonate) intercalated graphite oxide decreased by $92^{\circ}C$ in comparison with that of graphite oxide, indicating the addition of poly(sodium 4-styrenesulfonate) in the composite has diminished the thermal stability of graphite oxide.

• Fibers and Polymers
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• v.3 no.3
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• pp.109-112
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• 2002

Polybutadiene(PB) was epoxidized to various extents with m-chloroperbenzoic acid (MCPBA) in homogeneous solution. The thermal properties of the epoxidized PBs were investigated by differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). As a result of epoxidation the glass transition temperature (Tg) of PB increased by approximately $0.8^{\circ}$ for each 1 mol% of epoxidation. The thermal decomposition of the epoxidised PBs occurred in two-step process, while that of PB exhibited apparent one-step degradation process.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 2001.06a
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• pp.114-114
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• 2001

The thermal and friction characteristics of phenolic resin and model friction materials were investigated with the content of acrylonitrilebutadienerubber(NBR). The thermal characteristics of material was performed by dynamic mechanical thermal analysis and differential scanning calorimetry. The friction and wear characteristics of the material were determined by using friction material testing machine. The results show that with the more content of rubber, the loss modulus of friction material was increased. The friction coefficient and the specific wear rate with various NBR contents were reported.

• Structural Engineering and Mechanics
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• v.90 no.3
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• pp.219-232
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• 2024

In current study, for the first time, Nonlinear Bending of a skew microplate made of a laminated composite strengthened with graphene nanosheets is investigated. A mixture of mechanical and thermal stresses is applied to the plate, and the reaction is analyzed using the First Shear Deformation Theory (FSDT). Since different percentages of graphene sheets are included in the multilayer structure of the composite, the characteristics of the composite are functionally graded throughout its thickness. Halpin-Tsai models are used to characterize mechanical qualities, whereas Schapery models are used to characterize thermal properties. The microplate's non-linear strain is first calculated by calculating the plate shear deformation and using the Green-Lagrange tensor and von Karman assumptions. Then the elements of the Couple and Cauchy stress tensors using the Modified Coupled Stress Theory (MCST) are derived. Next, using the Hamilton Principle, the microplate's governing equations and associated boundary conditions are calculated. The nonlinear differential equations are linearized by utilizing auxiliary variables in the nonlinear solution by applying the Frechet approach. The linearized equations are rectified via an iterative loop to precisely solve the problem. For this, the Differential Quadrature Method (DQM) is utilized, and the outcomes are shown for the basic support boundary condition. To ascertain the maximum values of microplate deflection for a range of circumstances-such as skew angles, volume fractions, configurations, temperatures, and length scales-a parametric analysis is carried out. To shed light on how the microplate behaves in these various circumstances, the resulting results are analyzed.

• International Journal of Aeronautical and Space Sciences
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• v.4 no.2
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• pp.17-25
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• 2003

Simple methods are developed to predict temperatures of a satellite box during launch stage. The box is mounted on outer surface of satellite and directly exposed to space thermal environment for the time period from fairing jettison to separation. These simple methods are to solve a 1st order ordinary differential equation (ODE) which is simplified from the governing equation after applying several assumptions. The existence of analytical solution for the 1st order ODE is determined depending on treatment of time-dependent molecular heating term. Even for the case that the analytical solution is not available due to the time dependent term, the 1st order ODE can be solved by relatively simple numerical techniques. The temperature difference between two different approaches (analytical and numerical solutions) is relatively small (Jess than $1^{\circ}C$ along the time line) when they are applied to STSAT-I launch scenario. The present methods can be generally used as tools to quickly check whether a satellite box is safe against space environment during the launch stage for the case that the detailed thermal analysis is not available.

• Journal of the Korean Society of Fisheries and Ocean Technology
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• v.47 no.1
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• pp.46-58
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• 2011

A steady-state analysis and a simple dynamic model as simplified methods are developed, and results of energy consumption loads are compared with results obtained using computer to evaluate the analytical solution. Before obtaining simplified model a mathematical model is formulated for the effect of wall mass on the thermal performance of four different houses having various wall construction. This analytical study was motivated by the experimental work of Burch et al. An analytical solution of one-dimensional, linear, partial differential equation for wall temperature profiles and room air temperatures is obtained using the Laplace transform method. Typical Meteorological Year data are processed to yield hourly average monthly values. This study is conducted using weather data from four different locations in the United States: Albuquerque, New mexico; Miami, Florida; Santa Maria, California; and Washington D.C. for both winter and summer conditions. The steady state analysis that does not include the effect of thermal mass can provide an accurate estimate of energy consumption in most cases except for houses #2 and #4 in mild weather areas. This result shows that there is an effect of mass on the thermal performance of heavily constructed house in mild weather conditions. The simple dynamic model is applicable for high cycling rates and accurate values of inside wall temperature and ambient air temperature.

• Polymer(Korea)
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• v.39 no.2
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• pp.200-209
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• 2015

In this study, the influence of dilauroyl peroxide on mechanical and thermal properties of different polypropylene (PP) matrices was investigated. Polypropylene matrices, different molecular weight isotactic PP containing 0.01, 0.02, 0.04, 0.06, 0.08, and 0.1 wt% of dilauroyl peroxide (DLP) were prepared by using a single-screw extruder. The effect of the visbreaking agent (DLP) on mechanical, physical, thermal and morphological properties of different molecular weight PP had been studied. Mechanical properties (tensile strength at break point, at yield and elongation at break point), melt flow index (MFI), scanning electron microscope (SEM) and differential scanning calorimetric (DSC) analyses of these matrices were examined. Melting ($T_m$) and crystallization ($T_c$) temperatures, crystallinity ratio (%) and enthalpies were determined. The microstructure of isotactic polypropylene matrix was investigated by scanning electron microscopy (SEM). From SEM analysis, it was observed that the surface disorder increased by the increasing amount of DLP. As a result of DSC analyses, the crystallinity ratio of the PP matrices has varied between 1.64-7.27%. Mechanical properties of the matrices have been improved. Particularly, the mechanical tests of PP have given interesting results when compounded with 0.06-0.08 wt% dilauroyl peroxide (DLP). Mechanical properties and thermal decomposition processes were all changed by increasing the amount of DLP in the matrix structure.

• Korean Journal of Metals and Materials
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• v.50 no.9
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• pp.629-636
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• 2012

Volume shrinkage behavior accompanying the cure of resin formulations might be a critical factor when assembly processes using polymer materials are considered. In this study, cure shrinkage behavior with respect to resin formulation type and heating method was measured on sandwich structure samples by a thermomechanical analyzer (TMA). Quartz, used as a cover material for the sandwich structure, indicated the coefficient of thermal expansion close to $0ppm/^{\circ}C$. When a dynamic heating mode was conducted, a squeeze-out region and a cross-linking region for each resin formulation could be separated clearly with overlapping differential scanning calorimeter results on the TMA results. In addition, a cure shrinkage dominant region and a thermal expansion dominant region in the cross-linking region were distinguished. Consequently, the degree of cure at the initiation of the thermal expansion dominant region was successfully measured. Measurement of all resin formulations indicated the thermal expansion behavior exceeded cure shrinkage before full cure.

• Bulletin of the Korean Chemical Society
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• v.30 no.3
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• pp.618-622
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• 2009

The new candidates for OTFTs, which were composed of naphthalene, anthracene, benzo[1,2-b:4,5-b’]dithiophene and 2-decylbithiophene end-capper were synthesized under Suzuki coupling reaction conditions. All of the oligomers were characterized by FT-IR, mass analysis, UV-vis, PL spectrum, cyclic voltametry (CV), differential scanning calorimetry (DSC), thermal gravimetric analysis (TGA), $^1H-NMR\;and\;^{13}C-NMR$. Investigation of physical properties showed that all of the oligomers have higher oxidation potential and good thermal stability. Especially, DBT-DtB-DBT is soluble in common solvents and suitable for low cost processing technologies.