• 제목/요약/키워드: Determination technology

검색결과 3,577건 처리시간 0.028초

On-line Trace Enrichment in High Performance Liquid Chromatography Using XAD-2 Precolumn for the Determination of Lonazolac in Human Plasma

  • Lee, Hye-Suk;Kim, Eun-Joo;Zee, Ok-Pyo;Lee, Yoon-Joong
    • Archives of Pharmacal Research
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    • 제12권2호
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    • pp.108-113
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    • 1989
  • A new column-switching high performance liquid chromatographic method was developed for the determination of lonazolac in plasma. This method was based on the on-line trace enrichment of lonazolac using a precolumn packed with Amberlite XAD-2. The analysis was complete in 20 min. between injections and the limit of detection was $0.1{\mu}g/ml$ using $100{\mu}l$ of plasma. The method was linear in range of $0.1-10{\mu}g/ml$ with a correlation coefficient of 0.9991. Absolute recovery of lonazolac from the spiked plasma samples ranged from 95.6% to 97.1%. The method was shown to be reproducible over the concentration range studied.

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Interpretation of Voltammetric Data by Neural Networks for Simultaneous Determination of Glucose, Fructose, and Ascorbic Acid

  • Susomrith, Paisit;Surareungchai, Werasak;Chaisawat, Ake
    • 대한전자공학회:학술대회논문집
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    • 대한전자공학회 2002년도 ITC-CSCC -1
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    • pp.269-272
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    • 2002
  • This work describes the use of neural networks (NNs) for interpreting voltammetric data, i.e., current-voltage spectra that obtained from the electrochemical reaction of analyte species at a gold electrode. Current-voltage spectra of glucose, fructose and ascorbic acid in mixtures obtained from dual-pulse staircase voltammetry (DPSV) was in the form of the mixed responses contain characteristics of the individual analytes approximately in proportion to their concentration. Extraction of individual analyte concentration from combined data was subsequently achieved using NNs. The combination of DPSV and NNs opens a possibility for simultaneous determination of mixtures of the species for fruit juices quality monitoring.

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습식 분해법을 이용한 해산물 중 총 비소 분석을 위한 전처리 방법 연구 (Study on the Pretreatment of Seafood for the Determination of Total Arsenic using Wet Ashing Method)

  • 김선태;박경수
    • 분석과학
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    • 제16권6호
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    • pp.509-512
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    • 2003
  • Pretreatment method for the determination of total arsenic in seafood sample was studied. NIST SRM 1566a oyster tissue ($14.0{\pm}1.2mg\;As/kg$) as a standard arsenic compound in order to establish the decomposition method. We confirmed that the best way for pretreatment of seafoods to analyze total arsenic content precisely was $HNO_3-H_2SO_4-HCIO_4$ method by comparison of two methods which are dry ashing and wet ashing methods.

새로운 킬레이트 시약을 이용한 금의 원자흡수광도법 정량 (Determination of Gold by Flame Atomic Absorption Spectrophotometry using a New Chelating Agent)

  • 이진식;카츠야 우에스기;나가히로 토루;최원형;김경태;최성용
    • 분석과학
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    • 제8권3호
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    • pp.391-396
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    • 1995
  • A rapid preconcentration method based on solvent extraction is described for the determination of gold by flame atomic absorption spectrophotometry. Trace amounts of gold was extracted as a new chelating agent, 3-thiophenaldehyde-4-phenyl-3-thiosemicarbazone from pH 4.0 in diisobutyl ketone. The method is simple, fast, free from the effect of many interfering ions and has a high sensitivity and a good precision. Gold is quantitatively separated and concentrated from the elements in standard sample, and the value of the recovery was 91.7 and 108.3% by the proposed method.

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An Efficient Anti-collision Algorithm for the EPCglobal Class-1 Generation-2 System under the Dynamic Environment

  • Chen, Yihong;Feng, Quanyuan
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • 제8권11호
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    • pp.3997-4015
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    • 2014
  • Radio frequency identification (RFID) is an emerging wireless communication technology which allows objects to be identified automatically. The tag anti-collision is a significant issue for fast identifying tags due to the shared wireless channel between tags and the reader during communication. The EPCglobal Class-1 Generation-2 which uses Q algorithm for the anti-collision is widely used in many applications such as consumer electronic device and supply chain. However, the increasing application of EPCglobal Class-1 Generation-2 which requires the dynamic environment makes the efficiency decrease critically. Furthermore, its frame length (size) determination and frame termination lead to the suboptimal efficiency. A new anti-collision algorithm is proposed to deal with the two problems for large-scale RFID systems. The algorithm has higher performance than the Q algorithm in the dynamic environment. Some simulations are given to illustrate the performance.

무선측위 기술을 활용한 원전 건설현장 인원 안전관리 시스템 개발 방안 (Development of Safety Management System Based on Location Determination Technology for Construction Workers in Nuclear Power Plant Construction Project)

  • 김우중;이상현
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2016년도 춘계 학술논문 발표대회
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    • pp.239-240
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    • 2016
  • The nuclear power plant construction project is a large-scale project that involved a daily maximum of thousands of workers. many equipment and laborers involved has been required consistently to minimize the need for safety through real-time safety management. But current nuclear power plant construction site is only managed to access of workers and equipments. The purpose of this study is the owner requirements reflects the characteristics of the nuclear power plant construction project integrated safety management system utilizing active RFID and GPS positioning technology.

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Determination of Niflumic Acid in Human Urine by Gas Chromatography/Negative Chemical lonization Mass Spectrometry

  • Myung, Seung-Woon;Kim, Myung-Soo;Cho, Hyun-Woo;Park, Jong-Sei
    • Archives of Pharmacal Research
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    • 제19권6호
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    • pp.566-569
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    • 1996
  • A sensitivity method has been developed for the detection and determination of niflmic acid(NA) in human urine. Samples were extracted with diethylether. Flunixin (FN) was added to the sample prior to extraction as an internal standard. Niflumic acid was converted to its methyl derivative and analyzed by capillary gas chromatography/negative chemical isonization mass spectrometry. Using selected ion monitoring (SIM), the levels of NA down to 5 pg/ml could be detected in 5 ml spiked urine sample. Calibration curve was linear over the range of 0.5 ppm-50 ppm. The recovery of niflumic acid from urine at 40 pg/ml was to be $91.7{\pm}3.8(n=3)$ and the coefficient of variation was 4.1%.

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특허가치 평가지표 선정을 통한 기술 사업화 가능성 판단 : 리튬이온전지분야 (Determination of Commercialization Potential Through Patent Attribute Assessment in Lithium Ion Battery Technology)

  • 김완기
    • 대한산업공학회지
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    • 제40권2호
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    • pp.240-249
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    • 2014
  • This study aims to identify an assessment system based on multiple patent indices that can predict the likelihood of success in the commercialization of a patented technology in advance. In addition, we examine the effectiveness of our predictive model in identifying valuable technologies early on. We analyzed 3,063 secondary battery technologies patented in the US over the past 10 years. Our analysis identified 22 of the 25 most promising patented technologies, corresponding with the top 50% of industry-patented technologies that directly and indirectly succeeded in commercialization. These results support our claim that it is possible to identify attributes for the assessment of patent commercial potential to a significant degree. Our system presents a useful assessment index in the forecasting and determination of potential commercial success of patented technologies.

새로운 전처리 방법과 ICP-AES에 의한 폴리우레탄 중의 중금속 분석 (Determination of Heavy Metal in Polyurethane by New Digestion Method and ICP-AES)

  • 임헌성;이석근
    • 분석과학
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    • 제17권4호
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    • pp.363-367
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    • 2004
  • A simple and convenient digestion method was developed for the determination of heavy metal in polyurethane sample using only nitric acid in open system without heating. This digestion method had prevented loss of volatile elements of Hg and As and reduced the pretreatment time for the sample digestion. The detection limit is lowered over 10 times than that of microwave digestion method. Recoveries in polyurethane material were 108% for As, 96 ~ 99% for Hg, 102 ~ 103% for Cr, 98 ~ 102% for Pb, 86 ~ 90% for Cd, and 90 ~ 93% for Cu.