• Title/Summary/Keyword: Determination of Parameters

Search Result 1,536, Processing Time 0.026 seconds

Determination of Trace Metals in Waters by FAAS after Enrichment as Metal-HMDTC Complexes Using Solid Phase Extraction

  • Tokalioglu, Serife;Kartal, Senol;Elci, Latif
    • Bulletin of the Korean Chemical Society
    • /
    • v.23 no.5
    • /
    • pp.693-698
    • /
    • 2002
  • A method has been described for the determination of Cu(Ⅱ), Pb(Ⅱ), Ni(Ⅱ), Cd(Ⅱ), Mn(Ⅱ) and Fe(Ⅲ) by flame atomic absorption spectrometry (FAAS) after preconcentration on Amberlite XAD-16 resin, using hexamethyleneammonium-hexamethylenedithiocarbamate (HMA-HMDTC) as a chelating agent, and NH3/NH4Cl buffer solution (pH 9). Influences of various analytical parameters such as pH, concentration of nitric acid, amount of analytes, diverse ions and sample volume were investigated. The relative standard deviation (RSD) and the detection limit (LOD) were found in the range of 0.8-2.9% and 0.006-0.277 ㎍/mL,respectively. Recoveries obtained by the column method were quantitative ( >95%) at optimum conditions.The method was applied to the determination of some metal ions in seawater and wastewater samples. A high preconcentration factor (about 150 for seawater and 75 for wastewater samples) and simplicity are the main advantages of this suggested method.

A Study on Determination of Fallout Pu in the Environment

  • Lee, Myung-Ho;Park, Young-Hyun;Do Won park;Park, Gun-Sik;Kim, Sang-Bog;Lee, Chang-Woo
    • Proceedings of the Korean Nuclear Society Conference
    • /
    • 1998.05b
    • /
    • pp.627-632
    • /
    • 1998
  • Using an ammonium oxalate-ammonium sulfate electrolyte, a simple, quantitative, and fast technique for preparing sources for analytical alpha spectrometry was developed. To determine the optimum conditions for plating plutonium, parameters such as current density .and pH of electrolyte affacting the electrodeposition of the plutonium have been investigated. An optimized electrodeposition step for the determination of plutonium has been validated with a result of application to IAEA-Reference Soils. The new method of fallout Pu determination has been applied to environmental samples such as soil, sediment and moss samples in Korea.

  • PDF

Miniaturized Rectangular Slotted Nameplate Antenna Design for Satellite and Radio Determination Applications

  • Shanmuganantham, Thangavelu;Kaushal, Deepanshu
    • ETRI Journal
    • /
    • v.39 no.6
    • /
    • pp.813-819
    • /
    • 2017
  • A slotted rectangular nameplate antenna design with a patch bearing the name of the first author is presented. A $6.8mm{\times}26mm{\times}1.6mm$ substrate of FR-4 epoxy material having a relative permittivity of 4.4 and a dielectric loss tangent of 0.02 is used. Additionally, the feeding technique used is a coaxial mechanism. The standard antenna design parameters, including the reflection coefficient, bandwidth, radiation pattern, gain, directivity, and voltage standing wave radio (VSWR) for the proposed prototype are analyzed using a high-frequency structure simulator (HFSS) v-15, and are compared to the measured results. The designed structure may be considered for different satellite- and radio-determination applications at the respective resonant frequencies.

Determination of Design Parameters of Stockbridge Damper (스톡브리지 댐퍼 설계 파라미터 선정)

  • Kim, Chan-Jung
    • Transactions of the Korean Society for Noise and Vibration Engineering
    • /
    • v.26 no.7
    • /
    • pp.814-819
    • /
    • 2016
  • The Stockbridge damper is used to control the aeolian vibration of a overhead transmission line due to the natural wind under a low velocity, between 1 m/s to 7 m/s. The damper model can be simply derived with several design parameters and the location of eigenvalues of design parameters are important to determine the efficiency of energy dissipation by excitation itself with two counterweights. First, the importance of resonance frequencies of Stockbridge damper was reviewed through the analysis of frequency response function of damper system. Then, the best selection of design parameters was investigated with the introduction of objected function that minimize the distance between the calculated eigenvalues and target frequency points. The best choice of design parameters was reviewed using the simulated results from the objective function and the effectiveness of selected design case was discussed at the point view of practical implementation.

Model Parameter Determination of Industrial Co-generator Model Parameters through Filed Measurement (현장 계측을 통한 산업용 열병합 발전설비 모델 파라미터 결정)

  • Kim, Hak-Man
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
    • /
    • v.21 no.10
    • /
    • pp.159-165
    • /
    • 2007
  • This paper presents a method for the derivation of model parameters of a co-generation system using data measured through on-site generator characteristic testing and validates its model parameters. Dynamic models such as generator, excitation system, and turbine/governor are mainly dealt in this paper. For the purpose of validation of derived model parameters, the measured results are compared with simulation results. The comparisons between measured results and simulation results show good match.

A Study on the Determination of Optimum Parameter Level using Genetic Algorithms (유전자 알고리즘을 이용한 최적 파라미터 수준 결정에 관한 연구)

  • 김용범;김우열
    • Journal of the military operations research society of Korea
    • /
    • v.23 no.1
    • /
    • pp.88-99
    • /
    • 1997
  • Due to the various requests from consumers and rapidly changing market, the product design is continuously changing and the new products are manufactured in various forms. To satisfy this condition, companies must make the product design robust with better quality. However, considering many parameters and increasing the level of each parameter in product design can lead us to a difficult situation. In order to solve this problem, this paper attempts to develop an algorithm that takes into account more parameters and increased level of parameters using Genetic Algorithms. As a result of this study, we can use this algorithm for designing the parameters of new product since it can search the level of parameters in more detail and wider range.

  • PDF

A study on determination of HTS power devices' parameters (초전도기기 주요 파라미터 선정에 관한 연구)

  • Lee, Seung-Ryul;Kim, Jong-Yul;Yoon, Jae-Young
    • Progress in Superconductivity and Cryogenics
    • /
    • v.8 no.1
    • /
    • pp.34-38
    • /
    • 2006
  • There are many parameters that should be considered from the viewpoint of real power system operation and planning in designing HTS power devices. Especially, in the power system with HTS-FCL(fault current limiter) and TR(transformer), there is close correlation between parameters of the HTS power devices. This paper describes some considerations in determining parameters of HTS power devices, which are related to technical and economical aspects. The main parameters in this study are the quench resistance of HTS-FCL and the % impedance of HTS-TR. The results may give basic information for developing the devices.

Determination of Machining Parameters Considering Current Density in Three Dimensional Electrical Discharge Machining (3차원 방전가공에서 전류밀도를 고려한 방전가공조건 결정)

  • 이건범;김정두;최병훈;송희덕
    • Journal of the Korean Society of Manufacturing Technology Engineers
    • /
    • v.8 no.3
    • /
    • pp.100-106
    • /
    • 1999
  • Owing to the complexity of electrical discharge machining (EDM) phenomenon, it is very difficult to determine optimal machining parameters fer improving machining performance. This paper proposes a methodology for determining optimal electrical discharge machining parameters, which is maintaining suitable current density for increasing productivity or improving surface roughness. Machining area is closely related on optimal machining parameters in electrical discharge machining process, so calculation of machining area is needed in order to determine optimal machining parameters. In this study machining area, which is corresponding to the machining position, is calculated from intersection curves between the tool surface and a horizontal plane.

  • PDF

A Study on the Statistical Determination of Design Parameters Considering the Original Distribution Characteristics (원분포 특성을 고려한 설계정수의 통계적 신정에 관한 연구)

  • Kim, Jong-Gwan;Yang, Hyung-Sik
    • Tunnel and Underground Space
    • /
    • v.17 no.3 s.68
    • /
    • pp.197-202
    • /
    • 2007
  • In this study, design parameters were determined statistically with and without consideration of original distribution characteristics. Obtained parameters were applied to test numerical analysis and the results were compared. Distribution characteristics of statistically treated parameters show the similar characteristics of original distribution. Mean values show more than 19% of errors between the two cases. Regarding the characteristics as normal distribution can cause distorted results, it is proper to consider the original distribution characteristics of the parameters.

Determination of Parameters for 3-Dimensional Electrical Discharge Machining by a Tool Electrode Surface (공구전극곡면에 의한 3차원 방전가공조건의 결정)

  • 주상윤;이건범
    • Journal of the Korean Society for Precision Engineering
    • /
    • v.17 no.1
    • /
    • pp.27-33
    • /
    • 2000
  • This paper presents a method for determining machining parameters in 3-dimentional electrical discharge machining(EDM). The parameters are the peak value of currents, the pulse-on time, and the pulse-off time. It is known that they influence the performance of EDM more than the other else. The parameters are determined from the discharge area between a tool electrode and a work piece. The discharge area is directly influenced by the geometry of a tool surface and the tool discharge position. The discharge area on a tool discharge position is calculated from intersection curves between the tool surface and a horizontal plane. The grid search method is applied to determine the intersection curves. An example is introduced to show that the machining parameters are obtained from the surface geometry of a tool electrode.

  • PDF