• Title/Summary/Keyword: Deposition time

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Development and Application of Anti-Corrosive Steel Using Electro-Deposition of Sea Water (1) -Development of Electro-Deposition System Using Sea Water (해수전착 코팅을 이용한 내부식성 철근의 개발 및 적용성에 대한 연구 (1) -해수전착 코팅 시스템 개발)

  • Kwon, Seung Jun;Lee, Myeong Hoon;Park, Sang Soon
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.16 no.5
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    • pp.78-87
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    • 2012
  • This study is for developing a system for electro-deposition utilizing sea water containing various ions like calcium and magnesium. This is the first step research for the final goal which is a development of anti-corrosive steel for RC structure, so that this paper is mainly focused on the development for electro-deposition system. Optimum conditions for steel coating is obtained through various tests considering anode type, temperature, duration time, and current density. The composition of electro-deposition is analyzed through SEM, EDS, and XRD and it is evaluated to be $CaCO_3$ and $Mg(OH)_2$. Through measuring polarization potential and current density in the coated steel, the coating layer from the developed system is evaluated to have high resistance to steel corrosion. Additional tests and discussions on durability and structural performance in the coated steel from this work will be performed for the second step research.

Synthesis of Single Crystal Diamond by Variation of Deposition Pressure by HFCVD (HFCVD에 의한 증착압력 변화에 따른 Single Crystal Diamond 합성)

  • Kim, Min Su;Bae, Mun Ki;Kim, Seong-Woo;Kim, Tae Gyu
    • Journal of the Korean Society for Heat Treatment
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    • v.33 no.1
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    • pp.20-24
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    • 2020
  • Single crystal diamonds are in great demand in such fields as mechanical, electronic applications and optoelectronics. Large area single crystal diamonds are attracting attention in future industries for mass production and low cost. In this study, hot filament CVD (HFCVD) is used to grow large area single crystal diamond. However, the growth rate of large area single crystal diamond using HFCVD is known to be very low. The goal of this study is to use single crystal diamond substrates in HFCVD with methane-hydrogen gas mixtures to increase the growth rate of single crystal diamond and to optimize the conditions by analysing the effects of deposition conditions for high quality crystallinity. The deposition pressure, the ratio of CH4/H2 gas, the substrate temperature and the distance between the filament and the substrate were optimized. The sample used a 4×4 (mm2) size single crystal diamond substrate (100), the CH4/H2 gas ratio was fixed at 5%, the substrate temperature was synthesized to about 1000℃. At this time, the deposition pressure was changed to three types of 50, 75, 85 Torr and deposited. Finally, optimization was investigated under pressure conditions to analyse the growth rate and quality of single crystal diamond.

In-situ magnetization measurements and ex-situ morphological analysis of electrodeposited cobalt onto chemical vapor deposition graphene/SiO2/Si

  • Franco, Vinicius C. De;Castro, Gustavo M.B.;Corredor, Jeaneth;Mendes, Daniel;Schmidt, Joao E.
    • Carbon letters
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    • v.21
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    • pp.16-22
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    • 2017
  • Cobalt was electrodeposited onto chemical vapor deposition (CVD) graphene/Si/$SiO_2$ substrates, during different time intervals, using an electrolyte solution containing a low concentration of cobalt sulfate. The intention was to investigate the details of the deposition process (and the dissolution process) and the resulting magnetic properties of the Co deposits on graphene. During and after electrodeposition, in-situ magnetic measurements were performed using an (AGFM). These were followed by ex situ morphological analysis of the samples with ${\Delta}t_{DEP}$ 30 and 100 s by atomic force microscopy in the non-contact mode on pristine CVD graphene/$SiO_2$/Si. We demonstrate that it is possible to electrodeposit Co onto graphene, and that in-situ magnetic measurements can also help in understanding details of the deposition process itself. The results show that the Co deposits are ferromagnetic with decreasing coercivity ($H_C$) and demonstrate increasing magnetization on saturation ($M_{SAT}$) and electric signal proportional to remanence ($M_r$), as a function of the amount of the electrodeposited Co. It was also found that, after the end of the dissolution process, a certain amount of cobalt remains on the graphene in oxide form (this was confirmed by X-ray photoelectron spectroscopy), as suggested by the magnetic measurements. This oxide tends to exhibit a limited asymptotic amount when cycling through the deposition/dissolution process for increasing deposition times, possibly indicating that the oxidation process is similar to the graphene surface chemistry.

Field measurement study on snow accumulation process around a cube during snowdrift

  • Wenyong Ma;Sai Li;Xuanyi Zhou;Yuanchun Sun;Zihan Cui;Ziqi Tang
    • Wind and Structures
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    • v.37 no.1
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    • pp.25-38
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    • 2023
  • Due to the complexity and difficulty in meeting the multiphase flow complexity, similarity, and multiscale characteristics, the mechanism of snow drift is so complicated that the snow deposition prediction is still inaccurate and needs to be far improved. Meanwhile, the validation of prediction methods is also limited due to a lack of field-measured data about snow deposition. To this end, a field measurement activity about snow deposition around a cube with time was carried out, and the snow accumulation process was measured under blowing snow conditions in northwest China. The maximum snow depth, snow profile, and variation in snow depth around the cube were discussed and analyzed. The measured results indicated three stages of snow accumulation around the cube. First, snow is deposited in windward, lateral and leeward regions, and then the snow depth in windward and lateral regions increases. Secondly, when the snow in the windward region reaches its maximum, the downwash flow erodes the snow against the front wall. Meanwhile, snow range and depth in lateral regions have a significant increase. Thirdly, a narrow road in the leeward region is formed with the increase in snow range and depth, which results in higher wind speed and reforming snow deposition there. The field measurement study in this paper not only furthers understanding of the snow accumulation process instead of final deposition under complex conditions but also provides an important benchmark for validating prediction methods.

Real-time Contaminant Particle Monitoring for Chemical Vapor Deposition of Borophosphosilicate and Phosphosilicate Glass Film by using In-situ Particle Monitor and Particle Beam Mass Spectrometer (ISPM 및 PBMS를 이용한 BPSG 및 PSG CVD 공정 중 발생하는 오염입자의 실시간 측정)

  • Na, Jeong Gil;Choi, Jae Boong;Moon, Ji Hoon;Lim, Sung Kyu;Park, Sang Hyun;Yi, Hun Jung;Chae, Seung Ki;Yun, Ju Young;Kang, Sang Woo;Kim, Tae Sung
    • Particle and aerosol research
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    • v.6 no.3
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    • pp.139-145
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    • 2010
  • In this study, we investigated the particle formation during the deposition of borophosphosilicate glass (BPSG) and phosphosilicate glass (PSG) films in thermal chemical vapor deposition reactor using in-situ particle monitor (ISPM) and particle beam mass spectrometer (PBMS) which installed in the reactor exhaust line. The particle current and number count are monitored at set-up, stabilize, deposition, purge and pumping process step in real-time. The particle number distribution at stabilize step was measured using PBMS and compared with SEM image data. The PBMS and SEM analysis data shows the 110 nm and 80 nm of mode diameter for BPSG and PSG process, respectively.

Addition Effect of the Deposition and Buoyancy Terms in Modeling Turbulence Diffusion of Hazardous Air Pollutants (유해 대기오염물질의 난류확산 수치모의에서 침적한과 부력항 추가에 따른 효과)

  • Won, Gyeong-Mee;Lee, Hwa-Woon;Ji, Hyo-Eun;Kim, Cheol-Hee;Song, Chang-Keun
    • Journal of Korean Society for Atmospheric Environment
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    • v.22 no.1
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    • pp.73-84
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    • 2006
  • Hazardous Air Pollutants (HAPs) are characterized by being relatively heavier and denser than that of ambient air due to the various reasons such as higher molecular weight, low temperature and other complicated chemical transformations (Witlox, 1994). In an effort to investigate transport and diffusion from instantaneous emission of heavy gas, Lagrangian Particle Dispersion Model (LPDM) coupled with the RAMS output was employed. Both deposition process and buoyancy term were added on the atmospheric diffusion equations of LPDM, and the locations and concentrations of dense gas particle released from instantaneous single point source (emitting initially for 10 minutes only) were analyzed. The result overall shows that adding deposition process and buoyancy terms on the diffusion equation of LPDM has very small but detectable effect on the vertical and horizontal distribution of Lagrangian particles that especially transported for a fairly long traveling time. Also the slumping of dense gas can be found to be ignored horizontally compared to the advection by the horizontal wind suggesting that it was essential to couple the Lagrangian particle dispersion model coupled with the RAMS model in order to explain the dispersion of HAPs more accurately. However, during the initial time of instantaneous emission, buoyancy term play an important role on the vertical locations of dense particles for near surface atmosphere and around source area, indicating the importance of densities of HAPs in the beginning stage or short duration for the risk assessment of HAPs or management of heavy vapors during the explosive accidents.

A Study on the Assessment of Derived Intervention Levels in Foodstuffs Using the Dynamic Ingestion Pathway Model (동적 섭식경로모델을 이용한 음식물에 대한 유도 방사능 개입준위의 산정에 관한 연구)

  • Hwang, Won-Tae;Han, Moon-Hee;Kim, Byung-Woo
    • Journal of Radiation Protection and Research
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    • v.19 no.3
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    • pp.199-208
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    • 1994
  • The derived intervention levels in Korean foodstuffs were estimated using the dynamic ingestion pathway model which was developed considering Korean environment. The derived intervention levels were estimated from the intervention level of dose based on the thyroid committed dose equivalent of infant in the case of I-131, and the whole body committed dose equivalent for age groups and 13 kinds foodstuffs in the cases of Cs-137 and Sr-90. The derived intervention levels were shown as a considerable variation with deposition time and radionuclide. The adult was the most important age group in the estimation of derived intervention levels for Cs-137 and Sr-90. In the adult, the derived intervention levels for rice were 2390 and 47 Bq/kg for Cs-137 and Sr-90 in the case of deposition in summer, respectively, and 198 and 79 Bq/kg in the case of deposition in winter, respectively.

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A Study on the Temperature Distribution Change of the Spent Nuclear Fuel Disposal Canister and its Surrounding Structures due to the Spent Fuel Heat according to the Deposition Time Elapse (고준위폐기물 열에 의한 처분용기 및 처분용기 주위 구조물의 시간경과에 따른 온도분포 변화)

  • Choi, Jong-Won;Kwon, Young-Joo
    • Journal of the Computational Structural Engineering Institute of Korea
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    • v.20 no.2
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    • pp.157-164
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    • 2007
  • The prediction of the temperature distribution change of the spent nuclear fuel disposal canister and its surrounding structures (bentonite buffer, granitic rock etc.) due to the spent fuel heat is very important for the design of the 500m deep granitic repository for the spent nuclear fuel disposal canister (about 10,000 years long) deposition. In this study, the temperature distribution change of the composite structure which comprises the canister, the bentonite buffer, the deposition tunnel due to the spent fuel heat is computed using the numerical analysis method. Specially, the temperature distribution change of the composite structure is analysed as the deposition time elapses up to m years. The analysis result shows that the temperature of each part of the repository increases slowly in different way but the latest part temperature increases slowly up to 150 years and thereafter decreases slowly.

A Study on the Sediment Volume Change and Two-dimensional Deposited Characteristics of Pumping-dredged Soil (준설토의 체적변화 및 2차원 퇴적특성에 관한 연구)

  • 김형주;이민선;이용주;김대우
    • Journal of the Korean Geotechnical Society
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    • v.19 no.4
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    • pp.155-165
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    • 2003
  • A series of one-dimensional cylinder sedimentation test, seepage consolidation test and two-dimensional deposition model test were conducted to examine the characteristics of deposition and volume change of dredged soils containing the high water content, and these experimental results were compared with the sedimentary conditions of actual dredged-reclaimed fields to obtain the relations of a volume change by settling what is required for design. In addition, the change of water content and the distribution of fine grained soils after sedimentation were investigated. Thus, it was concluded that deposition height increased lineary as substantial soil volume increased, and also the elevation of interface increasea proportionately at both the starting time and the finishing time of virtual self-weight consolidation in one-dimensional sedimentation. Furthermore, the two-dimensional model test results were shown to describe the plain distribution of water content and fine grained silt where dredged soil was deposited by two dimensional flowing, and the water content was distributed to wide range from the minimum water content 30% to maximum 180% according to the passed amount of №200 sieve percentage.

An Experimental Study on Depositional Parameters of Cohesive Sediments in Semi-closed Bay (준 폐만 점착성 퇴적물의 퇴적매개변수 산정에 관한 실험적 연구)

  • Jung, Eui-Taek;Kim, Yong-Muk;Kim, Dong-Ho;Hwang, Kyu-Nam
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.24 no.3
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    • pp.159-165
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    • 2012
  • In this study, a series of deposition tests have been performed using an annular flume and depositional parameters of natural cohesive sediments have been estimated domestically for the first time. The natural cohesive sediments for deposition tests have been collected from Kwangyang Bay and total 18 deposition tests have been carried out on different bed shear stress respectively but with the same initial concentration. Test results for natural cohesive sediments of Kwangyang bay show that minimum bed shear stress ${\tau}_{bmin}$, standard deviation ${\sigma}_1$, and time scale parameter $({\tau}_b^*-1)_{50}$ are $0.11N/m^2$, 0.68 and 0.85, respectively. Through the comparison with results of previous studies for other sediments, the results of this study are shown to be good enough to verify.