• 제목/요약/키워드: Deposition methods

검색결과 844건 처리시간 0.049초

분말소재의 표면처리를 위한 회전형 CVD 공정 (Rotary CVD Process for Surface Treatment of Powders)

  • 이종환;정구환
    • 한국표면공학회지
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    • 제56권6호
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    • pp.341-352
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    • 2023
  • This paper reviews the potentials of a rotary chemical vapor deposition (RCVD) process for nanomaterial synthesis and coating on powder-based materials. The rotary reactor offers a significant improvement over traditional CVD methods having horizontal and fixed reaction chambers. The RCVD system yields enhanced productivity and surface coating uniformity of nanoparticles applied in various purposes, such as efficient heat dissipation, surface hardness enhancement, and enhanced energy storage performances. The effectiveness of the RCVD system would open up new possibilities in various applications because uniform coating on powder-based materials with massive productivity is inevitable to develop multi-functional materials with high reliability.

탄소나노튜브 박막 제조를 위한 분무공정에서의 증착 두께 분포 예측 모델 개발 (Development of Numerical Model for Predicting Deposition Thickness Distribution during Spray Process for Carbon Nanotube Thin Films)

  • 최두순;김덕종;장동환
    • 대한기계학회논문집B
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    • 제35권9호
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    • pp.969-974
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    • 2011
  • 탄소나노튜브(CNT)는 원통형의 탄소나노 구조물로서, 뛰어난 전도특성과 열전도율을 갖는다. 이러한 특성을 이용한 다양한 응용 분야의 하나로 CNT 를 박막형태의 그물망으로 제작하여 전도성 필름으로 응용하는 방안이 연구되고 있다. 이러한 CNT 의 박막 제조 방법 중, 분무 코팅 방식은 대면적 박막 제조에 널리 사용되나, 박막 두께를 균일하게 제작하는 점에 어려움이 있다. 이러한 문제점을 해결하려면 분무시의 공정조건이 증착 두께 분포에 미치는 효과를 잘 분석해야 한다. 본 연구에서는 분무 공정에서의 증착두께분포를 예측하기 위한 수치해석 모델을 개발하였다. 또한, 개발된 모델을 이용하여 여러가지 노즐 경로에 따른 증착 두께 분포를 분석하였다.

열처리방법에 따른 ${K_3}{Li_2}{Nb_5}{O_{15}}$(KLN)박막의 제작 (Preparation of ${K_3}{Li_2}{Nb_5}{O_{15}}$(KLN) Thin Films by Heat Treatment Methods)

  • 김광태;박명식;이동욱;조상희
    • 한국세라믹학회지
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    • 제37권8호
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    • pp.731-738
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    • 2000
  • KLN(K3Li2Nb5O15) has attracted a great deal of attention for their potential usefulness in piezoelectric, electro-optic, nonlinear optic, and pyroelectirc devices. Especially, the KLN single crystal has been studied in the field of optics and electronics. However it is hard to produce good quality single crystals due to the crack propagation during crystal growing. One of the solutions of this problem is prepartion of thin film. But the intensive study has not been conducted so far. In this study, after the KLN thin film were prepared by R.F. magnetron Sputtering method on SiO2/Si substrate, the post-annealing methods of RTA(rapid thermal annealin) and IPA(insitu post annealing) were employed. The deposition condition of KLN thin film was RF power(100 W), Working pressure(100 mtorr). The commonness of both RAT and IPA was that the higher were deposition and post annealing temperature, the higher was the intensity of XRD but the less surface roughness. The difference of post-annealing methods affected XRD phase and surface condition very much. And in IPA process, the influence of O2 had much effect on the formation of KLN phase.

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진공아크 증착법과 다른 공정에 의해 증착된 MgO 박막 특성 비교 (Comparison of characteristics of MgO films deposited by vacuum arc method with other methods.)

  • 이은성;김종국;이성훈;이건환
    • 한국진공학회지
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    • 제12권2호
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    • pp.112-117
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    • 2003
  • MgO 박막은 PDP(plasma display panels)분야에서 널리 사용되어 왔다. 본 연구에서는, 기존에 사용되고 있는 e-beam evaporation, reactive magnetron sputtering법과 arc deposition법으로 MgO 보호막을 증착하여 구조적 · 광학적 특성을 비교하였다. 반응 가스인 산소 가스의 유입량을 변화시켜 Mg metal target을 이용하여 vacuum arc deposition equipment 의해 유리 기판 위에 증착하였다. Ellipsometer를 이용하여 치밀도를 측정하고, MgO보호막의 마모율(erosion rate)를 측정하기 위해 가속 실험 방법을 도입, Ar+ 이온빔에 의한 erosion test를 시행하여 내마모성을 알아보았다. 또한, XPS와 UV test를 사용하여 MgO보호막의 광투과도에 미치는 수분의 영향을 조사한 결과, arc evaporation 법이 광투과도 90%이상을 유지하여 수분의 영향에 둔감한 것을 알 수 있었다. 한편, XRD와 AFM을 이용하여 MgO 박막의 구조와 표면 형상에 대해 조사하였다.

Chemical Vapor Deposition of Tantalum Carbide from TaCl5-C3H6-Ar-H2 System

  • Kim, Daejong;Jeong, Sang Min;Yoon, Soon Gil;Woo, Chang Hyun;Kim, Joung Il;Lee, Hyun-Geun;Park, Ji Yeon;Kim, Weon-Ju
    • 한국세라믹학회지
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    • 제53권6호
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    • pp.597-603
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    • 2016
  • Tantalum carbide, which is one of the ultra-high temperature ceramics, was deposited on graphite by low pressure chemical vapor deposition from a $TaCl_5-C_3H_6-Ar-H_2$ mixture. To maintain a constant $TaCl_5/C_3H_6$ ratio during the deposition process, $TaCl_5$ powders were continuously fed into the sublimation chamber using a screw-driven feeder. Sublimation behavior of $TaCl_5$ powder was measured by thermogravimetric analysis. TaC coatings have various phases such as $Ta+{\alpha}-Ta_2C$, ${\alpha}-Ta_2C+TaC_{1-x}$, and $TaC_{1-x}$ depending on the powder feeding methods, the $C_3H_6/TaCl_5$ ratio, and the deposition temperatures. Near-stoichiometric TaC was obtained by optimizing the deposition parameters. Phase compositions were analyzed by XRD, XPS, and Raman analysis.

젊은 여자환자에서 발생한 특발성 칼슘 피로 인산염 침착질환 - 증례보고 - (Idiopathic Calcium Pyrophosphate Dihydrate (CPPD) Crystal Deposition Disease in a Young Female Patient - A Case Report -)

  • 최의성;박경진;김용민;김동수;손현철;조병기;이현철
    • Clinics in Shoulder and Elbow
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    • 제12권1호
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    • pp.84-88
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    • 2009
  • 목적: 칼슘 피로 인산염 침착질환은 노인에게서 호발하며 젊은 성인에서의 발병은 극히 드문 것으로 인식되어 왔다. 대상 및 방법: 젊은 성인에서 발병한다면 혈색소증, 부갑상선 기능항진증, 저인산혈증, 저마그네슘혈증, 윌슨병, 갑상선 기능저하증, 통풍 등과 관련될 수 있으므로 젊은 성인에서 발병하는 다관절성 칼슘 피로 인산염 침착질환은 대사성 질환에 대한 검사가 이루어져야 한다. 결론: 저자들은 대사성 질환이 없는 25세 젊은 여성에서 발병한 특발성 칼슘 피로 인산염 침착질환 1례를 경험하였기에 보고하는 바이다.

Effect of Agricultural Countermeasures on Ingestion Dose Following a Nuclear Accident

  • Keum, Dong-Kwon;Jeong, Hyojoon;Jun, In;Lim, Kwang-Muk;Choi, Yong-Ho;Lee, So-Hyeon;Jung, Tae-Jong
    • Journal of Radiation Protection and Research
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    • 제44권1호
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    • pp.8-14
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    • 2019
  • Background: Management of an agricultural food product system following a nuclear accident is indispensable for reducing radiation exposure due to ingestion of contaminated food. The present study analyzes the effect of agricultural countermeasures on ingestion dose following a nuclear accident. Materials and Methods: Agricultural countermeasures suitable for domestic farming environments were selected by referring to the countermeasures applied after the Fukushima accident in Japan. The avertable ingestion doses that could be obtained by implementing the selected countermeasures were calculated using the Korean Agricultural Countermeasure Analysis Program (K-ACAP) to investigate the efficiency of each countermeasure. Results and Discussion: Of the selected countermeasures, the management of crops was effective when radionuclide deposition occurred during the growing season of plants. Treatment by soil additive and topsoil removal was effective when deposition occurred during the nongrowing season of plants. The disposal of milk was not effective owing to the small contribution of milk to the overall ingestion dose. Clean feeding of livestock was effective when deposition occurred during the growing season of fodder plants such as pasture and rice-straw. Finally, the effect of food restriction increased with the soil deposition density of radionuclide. The practical effect of countermeasures was very small when the avertable ingestion dose was absolutely low. Conclusion: The agricultural countermeasures selected to reduce the radionuclide ingestion dose after a nuclear accident must be made appropriate by considering the accident situation, such as the soil deposition density of the radionuclide and the deposition date in relation to farming cycles.

$CoSi_2$ 전극 구조의 증착법에 따른 특성 변화 연구 (Study on Property Variations of $CoSi_2$ Electrode with Its Preparation Methods)

  • 남형진
    • 반도체디스플레이기술학회지
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    • 제6권4호
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    • pp.5-9
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    • 2007
  • Phase transition and dopant redistribution during silicidation of $CoSi_2$ thin films were characterized depending on their preparation methods. Our results indicated that cleanness of the substrate surface played an important role in the formation of the final phase. This effect was found to be reduced by addition of W resulting in the formation of $CoSi_2$. However, even in this case, the formation of the final phase was achieved at the cost of extra thermal energy, which induced rough interface between the substrate and the silicide film. As for the dopant redistribution, the deposition sequence of Co and Si on SiGe was observed to induce significant differences in the dopant profiles. It was found that co-deposition of Co and Si resulted in the least redistribution of dopants thus maintaining the original dopant profile.

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무전도 금속 증착을 위한 하전 입자빔 전처리 공정의 타당성 연구 (On Feasibility Study of the Charged Particle Beam Pretreatment Process for Non-conducting Metal Coating)

  • 나명환;박영식;심하몽;전영호
    • 품질경영학회지
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    • 제42권2호
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    • pp.179-187
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    • 2014
  • Purpose: Since several problems were found when present non-conducting metal coating process was applied to mass production, we study and develop to improve those problems. Methods: In this paper, a couple of analysis methods such as surface hardness, XPS spectrum analysis, morphology, and reflection ratio were used. Results: This paper suggest a new possibility of Non-conducting thin metal coating method that has quality of mass production phase without UV coating process. Conclusion: By the result of analysis, we can set optimized process conditions of the electro deposition coating using electron beam.

다양한 방법에 의해 성장된 탄소 나노튜브의 전계방출 특성 (Field emission properties of carbon nanotubes grown by various methods)

  • 김부종;장한빛;김종필;박진석
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2011년도 제42회 하계학술대회
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    • pp.1408-1409
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    • 2011
  • Carbon nanotubes (CNTs) were grown on conical tip substrates by using various methods such as electrophoretic deposition, dip-coating, and spray. The scanning electron microscope measurement showed that the spray method ascertained the most uniform deposition of CNTs. The CNT-emitter that was fabricated by the spray method revealed the lowest turn on voltage of electron emission and the highest emission current. In addition, the spray-produced CNT emitter showed the most stable long-term emission characteristics.

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