• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2000.10a
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• pp.66-69
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• 2000

In order to analyze the densification behaviour of stainless steel powder compacts during hot isostatic pressing (HIP) at elevated temperatures, a power-law creep constitutive model based on the plastic deformation theory for porous materials was applied to the densification. Various densification mechanisms including interparticle boundary diffusion, grain boundary diffusion and lattice diffusion mechanisms were incorporated in the constitutive model, as well. The power-law creep model in conjunction with various diffusion models was applied to the HIP process of 316L stainless steel powder compacts under 50 and 100 MPa at 1125 $!`\acute{\dot{E}}$. The results of the calculations were verified using literature data It could be found that the contribution of the diffusional mechanisms is not significant under the current process conditions.

• Journal of Powder Materials
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• v.7 no.3
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• pp.137-142
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• 2000

In order to analyze the densification behaviour of stainless steel powder compacts during hot isostatic pressing (HIP) at elevated temperatures, a power-law creep constitutive model based on the plastic deformation theory for porous materials was applied to the densification. Various densification mechanisms including interparticle boundary diffusion, grain boundary diffusion and lattice diffusion mechanisms were incorporated in the constitutive model, as well. The power-law creep model in conjunction with various diffusion models was applied to the HIP process of 316L stainless steel powder compacts under 50 and 100 MPa at $1125^{\circ}C$. The results of the calculations were verified using literature data. It could be found that the contribution of the diffusional mechanisms is not significant under the current process conditions.

• Metals and materials international
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• v.24 no.6
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• pp.1303-1308
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• 2018

A new sintering technique for enhancing a densification and hardness of sintered titanium body by supplying hydrogen was developed (Hydrogen Sintering Process, HSP). The HSP was developed by only injecting hydrogen into an argon atmosphere during the core time. As a result, sound titanium sintered bodies with high density and hardness were obtained by the HSP. In addition, a pore size and number of the HSP specimens were smaller than those of the argon atmosphere specimen. It was found that the injecting hydrogen into the argon atmosphere by HSP can prevent the formation of oxide layers, resulting in enhanced densification and hardness.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.32 no.4
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• pp.333-339
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• 2008

Densification behavior of copper powder was investigated to study the effect of an aluminum mold under warm pressing. The low flow stress of an aluminum mold is appropriate to apply hydrostatic stress to powder compacts during compaction under high temperature. The suggested powder metallurgy process is very useful under high temperature since copper powder compacts have higher relative density over axial stress of 100 MPa and show more homogeneity as compared with conventional warm pressing. Elastoplastic constitutive equation proposed by Shima and Oyane was implemented into a finite element program (ABAQUS) for densification behavior under warn pressing by using a metal mold. Finite element results agreed well with experimental data for densification and deformation of copper powder compacts in the mold.

• Journal of the Korean Wood Science and Technology
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• v.51 no.2
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• pp.133-144
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• 2023

Densification is an effective method for improving the physical and mechanical properties of low-density wood. However, the set-recovery of dimensions was found to be the problem of densified wood due to low fixation during the densification process. Alkali pretreatment before densification is thought to be a modification process to improve the dimensional stability of densified wood. In this research, the wood samples used were boiled in a 1.25 N sodium hydroxide (NaOH) solution at different times, followed by densification for 5 h at 100℃. The alkali pretreatment for 1, 3, and 5 h of boiling increased the dimensional stability of densified woods and anti-swelling efficiency values were 8.52%, 63.24%, and 48.94%, respectively. The boiling of wood in NaOH solution decreased the holocellulose content, as well as lignin to a lesser degree, and a lower crystallinity index was observed. The lower hydroxyl groups and a higher proportion of lignin in treated samples seem to have contributed to the high dimensional stability detected.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.36 no.10
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• pp.1255-1260
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• 2012

The densification behavior of titanium powder in the direct powder rolling process was investigated. An analytical model for the roll-backlash phenomenon during this process was proposed to conduct a realistic finite element analysis. Furthermore, the roll-backlash was quantitatively analyzed, and the relative densities of the greenstrip along the rolling direction were precisely estimated. Finally, the slip and nip phenomena were identified by calculating the contact pressure and shear stress between the titanium powder and the roller in order to understand the densification behavior of the powder during the rolling process.

• Transactions of Materials Processing
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• v.7 no.5
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• pp.426-431
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• 1998

This study is concerned with cold repressing of sintered preforms by the rotary forging process. An experiment has been carried out using the rotary powder forging press(500kN) which was designed and constructed in the authors' laboratory. The effect of process variables and aspect ration of sintered preform on the densification behavior during the rotary repressing was studied by several mechanical test such as working force hardness distribution density and microstructures of the specimens. Since a higher densification can be achieved by applying the rotary repressing on presinted preforms it was successively demonstrated that the cold rotary powder forging is an effective operation to improve quality of P/M parts.

• Journal of Powder Materials
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• v.20 no.1
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• pp.1-6
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• 2013

The key concept of nanopowder agglomerate sintering (NAS) is to enhance material transport by controlling the powder interface volume of nanopowder agglomerates. Using this concept, we developed a new approach to full density processing for the fabrication of pure iron nanomaterial using Fe nanopowder agglomerates from oxide powders. Full density processing of pure iron nanopowders was introduced in which the powder interface volume is manipulated in order to control the densification process and its corresponding microstructures. The full density sintering behavior of Fe nanopowders optimally size-controlled by wet-milling treatment was discussed in terms of densification process and microstructures.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.14 no.10
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• pp.779-784
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• 2001

In this work, we studied the characteristics of nitride films for the optimization of PMD(pro-metal dielectric) linear process, which can be applied to the recent semiconductor manufacturing process. We split the deposit condition of nitride films into four parts such as PO(protect overcoat) nitride, baseline, low hydrogen and high stress and low hydrogen, respectively. We tried to find out correlation between BPSG deposition and densification. In order to analyze the changes of Si-H and Si-NH-Si bonding density, we used FTIR area method. We also investigated the crack generation on wafer edge after BPSG densification, and the changes of nitride film stress as a function of RF power variation to judge whether the deposited films.

• Journal of the Korean Ceramic Society
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• v.32 no.1
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• pp.51-56
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• 1995

Variation of sintered density of BaTiO3 powder calcined at 120$0^{\circ}C$ and 135$0^{\circ}C$ was investigated with respect to the grain growth behavior. It was found that BaTiO3 powder, which was calcined at 120$0^{\circ}C$, showed abnormal grain growth behavior during sintering process. At initial stage of sintering process, the densification rate of specimen was accelerated with rapid grain growth caused by the abnormal grain growth. But with the increase of sintering time, abnormally grown grain met each other and the density of specimen decreased drastically due to coalescence of pores located in triple junction. On the contrary, BaTiO3 powder calcined at 135$0^{\circ}C$ showed normal grain growth behavior and gradually densified with the increase of sintering time.